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1. 发明申请

US20100124522A1 Process for the extraction of technetium from uranium 有权
公开(公告)号：US20100124522A1
公开(公告)日：2010-05-20
申请号：US12313354
申请日：2008-11-19
申请人： Cynthia-May S. Gong , Frederic Poineau , Kenneth R. Czerwinski
发明人： Cynthia-May S. Gong , Frederic Poineau , Kenneth R. Czerwinski
IPC分类号： C01G43/00 , B01D11/04 , C22B61/00
CPC分类号： C22B3/0024 , C01G43/003 , C01G99/003 , C22B7/007 , C22B61/00 , G21C19/46 , Y02P10/234 , Y02W30/883
摘要： A spent fuel reprocessing method contacts an aqueous solution containing Technetium(V) and uranyl with an acidic solution comprising hydroxylamine hydrochloride or acetohydroxamic acid to reduce Tc(V) to Tc(II, and then extracts the uranyl with an organic phase, leaving technetium(II) in aqueous solution.

2. 发明授权

US07452703B1 Uranium enrichment using microorganisms 失效
标题翻译：使用微生物的铀浓缩
公开(公告)号：US07452703B1
公开(公告)日：2008-11-18
申请号：US10802637
申请日：2004-03-17
申请人： Kenneth R. Czerwinski , Martin F. Polz
发明人： Kenneth R. Czerwinski , Martin F. Polz
IPC分类号： C12P3/00 , C12P41/00
CPC分类号： B01D59/36
摘要： The present invention provides methods for separating isotopes of actinide elements such as uranium using microorganisms, e.g., metal or sulfate reducing bacteria. The microorganisms reduce the actinide element to form a precipitate, which contains a greater proportion of the lighter isotope relative to the heavier isotope than the starting material. The precipitate may be collected, re-oxidized, and subjected to multiple rounds of enrichment. Alternately, separation processes not requiring formation of a precipitate may be used. The invention also features cell-free systems for isotope separation. The invention further provides compositions produced according to the foregoing methods, including compositions comprising enriched uraninite.
摘要翻译：本发明提供使用微生物例如金属或硫酸盐还原细菌分离锕系元素如铀的同位素的方法。微生物减少锕系元素以形成沉淀物，其比起始原料含有比重的同位素更大比例的较轻的同位素。可以收集沉淀物，再次氧化并进行多轮富集。或者，可以使用不需要形成沉淀物的分离方法。本发明还具有用于同位素分离的无细胞系统。本发明还提供了根据前述方法制备的组合物，包括含有浓缩的尿烷的组合物。

3. 发明申请

US20130087464A1 ROOM TEMPERATURE ELECTRODEPOSITION OF ACTINIDES FROM IONIC SOLUTIONS 审中-公开
标题翻译：来自离子解决方案的室温室温电沉积
公开(公告)号：US20130087464A1
公开(公告)日：2013-04-11
申请号：US13268138
申请日：2011-10-07
申请人： David W. Hatchett , Wendy Pemberton , Kenneth R. Czerwinski
发明人： David W. Hatchett , Wendy Pemberton , Kenneth R. Czerwinski
IPC分类号： C25D3/54
CPC分类号： C25D3/54 , C25D3/665
摘要： Uranium metal can be electrochemical deposited from room temperature ionic liquid (RTIL), tri-methyl-n-butyl ammonium n-bis(trifluoromethansulfonylimide) [Me3NnBu][TFSI] providing an alternative non-aqueous system for the extraction and reclamation of actinides from reprocessed fuel materials. Deposition of U metal is achieved using TFSI complexes of U(III) and U(IV) containing the anion common to the RTIL. TFSI complexes of uranium were produced to ensure solubility of the species in the ionic liquid. The methods provide a first measure of the thermodynamic properties of U metal deposition using Uranium complexes with different oxidation states from RTIL solution at room temperature.
摘要翻译：铀金属可以从室温离子液体（RTIL），三 - 甲基 - 正丁基铵正 - 双（三氟甲烷磺酰亚胺）[Me3NnBu] [TFSI]进行电化学沉积，提供了一种替代非水系统，用于从锕系元素中提取和回收锕系元素再加工燃料。使用含有与RTIL共有的阴离子的U（III）和U（IV）的TFSI复合物实现U金属的沉积。制备铀的TFSI络合物以确保物质在离子液体中的溶解度。该方法提供了使用在室温下从RTIL溶液中具有不同氧化态的铀络合物的U金属沉积的热力学性质的第一测量。

4. 发明授权

US07854907B2 Process for the extraction of technetium from uranium 有权
标题翻译：从铀提取锝的工艺
公开(公告)号：US07854907B2
公开(公告)日：2010-12-21
申请号：US12313354
申请日：2008-11-19
申请人： Cynthia-May S. Gong , Frederic Poineau , Kenneth R. Czerwinski
发明人： Cynthia-May S. Gong , Frederic Poineau , Kenneth R. Czerwinski
IPC分类号： B01D11/00
CPC分类号： C22B3/0024 , C01G43/003 , C01G99/003 , C22B7/007 , C22B61/00 , G21C19/46 , Y02P10/234 , Y02W30/883
摘要： A spent fuel reprocessing method contacts an aqueous solution containing Technetium(V) and uranyl with an acidic solution comprising hydroxylamine hydrochloride or acetohydroxamic acid to reduce Tc(V) to Tc(II, and then extracts the uranyl with an organic phase, leaving technetium(II) in aqueous solution.
摘要翻译：乏燃料再处理方法将含有锝（V）和铀酰的水溶液与包含羟胺盐酸盐或乙酰肟酸的酸性溶液接触以将Tc（V）降低至Tc（II），然后用有机相萃取铀酰，留下锝 II）在水溶液中。

5. 发明授权

US10399077B2 Dual flask 有权
公开(公告)号：US10399077B2
公开(公告)日：2019-09-03
申请号：US14659241
申请日：2015-03-16
申请人： Daniel Rego , Kenneth R. Czerwinski
发明人： Daniel Rego , Kenneth R. Czerwinski
IPC分类号： B01L3/00 , B01L3/08
摘要： This document provides a dual flask for laboratory use, methods of using a dual flask, and systems including a dual flask. A dual flask can include a first flask structure and a second flask structure. Each flask structure can include a body and a neck. The first body and the second body in a dual flask provided herein can be connected together and have a filter there between such that fluids can be filtered between said first and second bodies.

6. 发明授权

US07582232B1 Low temperature route to uranium nitride 有权
标题翻译：低温铀氮化物路线
公开(公告)号：US07582232B1
公开(公告)日：2009-09-01
申请号：US11739147
申请日：2007-04-24
申请人： Anthony K. Burrell , Alfred P. Sattelberger , Charles Yeamans , Thomas Hartmann , G. W. Chinthaka Silva , Gary Cerefice , Kenneth R. Czerwinski
发明人： Anthony K. Burrell , Alfred P. Sattelberger , Charles Yeamans , Thomas Hartmann , G. W. Chinthaka Silva , Gary Cerefice , Kenneth R. Czerwinski
IPC分类号： G21C3/02 , G21C3/42 , C01G43/00 , C01B21/06
CPC分类号： C01B21/063 , C01B21/0602 , C01B21/076 , C01G43/06 , C01P2002/60 , C01P2002/72 , C01P2002/77 , C01P2002/80 , C01P2002/85 , C01P2006/10 , G21C3/42 , G21C3/58 , Y02E30/38
摘要： A method of preparing an actinide nitride fuel for nuclear reactors is provided. The method comprises the steps of a) providing at least one actinide oxide and optionally zirconium oxide; b) mixing the oxide with a source of hydrogen fluoride for a period of time and at a temperature sufficient to convert the oxide to a fluoride salt; c) heating the fluoride salt to remove water; d) heating the fluoride salt in a nitrogen atmosphere for a period of time and at a temperature sufficient to convert the fluorides to nitrides; and e) heating the nitrides under vacuum and/or inert atmosphere for a period of time sufficient to convert the nitrides to mononitrides.
摘要翻译：提供了制备用于核反应堆的锕系氮化物燃料的方法。该方法包括以下步骤：a）提供至少一种锕系氧化物和任选的氧化锆; b）将氧化物与氟化氢源混合一段时间并在足以将氧化物转化成氟化物盐的温度下进行; c）加热氟化物盐以除去水; d）在氮气气氛中加热氟化盐一段时间并在足以将氟化物转化为氮化物的温度下加热; 以及e）在真空和/或惰性气氛下加热氮化物一段足以将氮化物转化为一氮化物的时间。

7. 发明申请

US20150258541A1 DUAL FLASK 审中-公开
标题翻译：双重FLASK
公开(公告)号：US20150258541A1
公开(公告)日：2015-09-17
申请号：US14659241
申请日：2015-03-16
申请人： Daniel Rego , Kenneth R. Czerwinski
发明人： Daniel Rego , Kenneth R. Czerwinski
IPC分类号： B01L3/08
CPC分类号： B01L3/08 , B01L3/569 , B01L2300/0681 , B01L2300/0861 , B01L2400/0644
摘要： This document provides a dual flask for laboratory use, methods of using a dual flask, and systems including a dual flask. A dual flask can include a first flask structure and a second flask structure. Each flask structure can include a body and a neck. The first body and the second body in a dual flask provided herein can be connected together and have a filter there between such that fluids can be filtered between said first and second bodies.
摘要翻译：本文件提供实验室使用的双烧瓶，使用双烧瓶的方法和包括双烧瓶的系统。双烧瓶可以包括第一烧瓶结构和第二烧瓶结构。每个烧瓶结构可以包括身体和颈部。本文提供的双烧瓶中的第一主体和第二主体可以连接在一起，并且其间具有过滤器，使得流体可以在所述第一和第二主体之间过滤。

8. 发明申请

US20080268513A1 URANIUM ENRICHMENT USING MICROORGANISMS 失效
标题翻译：铀浓缩使用微生物
公开(公告)号：US20080268513A1
公开(公告)日：2008-10-30
申请号：US10802637
申请日：2004-03-17
申请人： Kenneth R. Czerwinski , Martin F. Polz
发明人： Kenneth R. Czerwinski , Martin F. Polz
IPC分类号： C12P3/00 , C12N1/21 , C07F5/00
CPC分类号： B01D59/36
摘要： The present invention provides methods for separating isotopes of actinide elements such as uranium using microorganisms, e.g., metal or sulfate reducing bacteria. The microorganisms reduce the actinide element to form a precipitate, which contains a greater proportion of the lighter isotope relative to the heavier isotope than the starting material. The precipitate may be collected, re-oxidized, and subjected to multiple rounds of enrichment. Alternately, separation processes not requiring formation of a precipitate may be used. The invention also features cell-free systems for isotope separation. The invention further provides compositions produced according
摘要翻译：本发明提供使用微生物例如金属或硫酸盐还原细菌分离锕系元素如铀的同位素的方法。微生物减少锕系元素以形成沉淀物，其比起始原料含有比重的同位素更大比例的较轻的同位素。可以收集沉淀物，再次氧化并进行多轮富集。或者，可以使用不需要形成沉淀物的分离方法。本发明还具有用于同位素分离的无细胞系统。本发明还提供了根据本发明生产的组合物

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