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1. 发明授权

US08709705B2 Metal-containing compositions and method of making same 有权
标题翻译：含金属的组合物及其制备方法
公开(公告)号：US08709705B2
公开(公告)日：2014-04-29
申请号：US13543071
申请日：2012-07-06
申请人： Mangala Malik , Joseph J Schwab
发明人： Mangala Malik , Joseph J Schwab
IPC分类号： G03F7/26
CPC分类号： C08F4/12 , C08F4/06 , C08F4/16
摘要： The present invention relates to a process for forming metal-containing films by applying a photosensitive metal-containing composition on a substrate, drying the photosensitive metal-containing composition, exposing the photosensitive metal-containing composition to a source of actinic radiation and applying a post-treatment to the metal-containing composition. The process also includes exposing the photosensitive metal-containing composition to a source of actinic radiation through a mask or mold and developing the unexposed portion of the composition. Another embodiment of the invention is a metal-containing film, three-dimensional object or article formed by the process. The invention is useful in producing a directly patterned metal-containing film and a microdevice.
摘要翻译：本发明涉及通过将含感光性金属的组合物涂布在基材上，干燥含有感光性金属的组合物，将含有感光性金属的组合物曝露于光化辐射源并施加柱对含金属组合物的处理。该方法还包括将含感光金属的组合物暴露于光化辐射源通过掩模或模具并显影组合物的未曝光部分。本发明的另一个实施方案是通过该方法形成的含金属膜，三维物体或制品。本发明可用于生产直接图案化的含金属膜和微型设备。

2. 发明申请

US20100137464A1 POROSITY CONTROL WITH POLYHEDRAL OLIGOMERIC SILSESQUIOXANES 审中-公开
标题翻译：多孔低密度硅藻土的多孔性控制
公开(公告)号：US20100137464A1
公开(公告)日：2010-06-03
申请号：US12698931
申请日：2010-02-02
申请人： Joseph D. Lichtenhan , Joseph J. Schwab , Yi-Zhong An , Jack Sammons
发明人： Joseph D. Lichtenhan , Joseph J. Schwab , Yi-Zhong An , Jack Sammons
IPC分类号： C08J9/40
CPC分类号： C08J3/203 , B82Y30/00 , C08J5/005 , C08J2201/038 , C08K5/549 , Y10T428/2995 , Y10T428/31663
摘要： The use of nanostructured chemicals based on polyhedral oligomeric silsesquioxanes (POSS) and polyhedral oligomeric silicates (POS) are used to control porosity in organic and inorganic media. The precisely defined nanoscopic dimensions of this class of chemicals enables porosity to be both created (increased) or reduced (decreased) as desired. The thermal and chemical stability of the POSS/POS nanostructures and the ability of these nano-building blocks to be selectively placed or rationally assembled with both inorganic and organic material mediums allow tailoring of porosity.
摘要翻译：使用基于多面体低聚倍半硅氧烷（POSS）和多面体低聚硅酸盐（POS）的纳米结构化学品用于控制有机和无机介质中的孔隙率。这类化学品的精确定义的纳米尺寸尺寸可以根据需要产生（增加）或减少（减少）孔隙度。 POSS / POS纳米结构的热和化学稳定性以及这些纳米结构单元与无机和有机材料介质选择性地放置或合理组装的能力允许调整孔隙度。

3. 发明授权

US07629424B2 Metal-containing compositions and method of making same 有权
标题翻译：含金属组合物及其制备方法
公开(公告)号：US07629424B2
公开(公告)日：2009-12-08
申请号：US11792739
申请日：2006-06-12
申请人： Mangala Malik , Joseph J Schwab
发明人： Mangala Malik , Joseph J Schwab
IPC分类号： C08F30/04
CPC分类号： C08J3/28 , C08F230/04
摘要： The present invention relates to metal-containing compositions with refractive indices of at least 1.5 comprising a metal-containing precursor unit (MU), a prepolymer unit (PU), and a catalyst or an initiator capable of inducing a combining reaction of ethylenically unsaturated functional groups of the metal-containing precursor unit and reactive functional groups of the prepolymer unit. In another embodiment, the composition comprises MU and a catalyst or initiator capable of inducing a combining reaction of the metal-containing precursor units. Both MU and PU contain additional functional groups, which may be selected to impart compatibility with each other and to produce optically clear films. The metal-containing compositions can be used to produce films or articles having a transmittance of at least 90% and index of refraction in the range of 1.5 to 1.8 in the 400-700 nm range of light and 1.5 to 2.4 in the 150-400 nm range of light.
摘要翻译：本发明涉及具有至少1.5的折射率的含金属组合物，其包含含金属的前体单元（MU），预聚物单元（PU），以及能够诱导烯属不饱和官能团的组合反应的催化剂或引发剂含金属的前体单元的基团和预聚物单元的反应性官能团。在另一个实施方案中，组合物包含MU和能够诱导含金属的前体单元的组合反应的催化剂或引发剂。 MU和PU都包含另外的官能团，其可以被选择以赋予彼此的相容性并产生光学透明的膜。含金属的组合物可用于生产具有至少90％的透光率和在400-700nm光范围内的1.5至1.8范围内的折射率和在150-400中的1.5至2.4的膜或制品 nm范围的光。

4. 发明授权

US07265194B1 Polyhedral oligomeric silsesquinoxanes and polyhedral oligomeric silicates bearing surfactant functionalities 失效
标题翻译：具有表面活性剂功能的多面体低聚硅氧烷喹啉和多面体低聚硅酸盐
公开(公告)号：US07265194B1
公开(公告)日：2007-09-04
申请号：US10968370
申请日：2004-10-18
申请人： Joseph D. Lichtenhan , Joseph J. Schwab
发明人： Joseph D. Lichtenhan , Joseph J. Schwab
IPC分类号： C08G77/38
CPC分类号： C08G77/04 , C08G77/382
摘要： This invention teaches the preparation and compositions of POSS nanostructured chemicals bearing a variety of onium-type surfactants. The surfactants serve as low-cost compatibilizing groups for polyhedral oligomeric silsesquioxane and polyhedral oligomeric silicate nanostructures with man-made polymer and biological systems. Variations of the surfactants also provide reactivity for the nanostructured chemicals with man-made and biological materials. The surfactant bearing nanostructured chemicals are useful as alloying agents is for controlling the structure and bulk physical properties of materials from the nanoscopic length scale. Alternately, the surfactants can be eliminated from the nanostructures to render the formation of nanoscopically dispersed silica particles.
摘要翻译：本发明教导了具有各种鎓型表面活性剂的POSS纳米结构化学品的制备和组成。表面活性剂作为多面体低聚倍半硅氧烷和具有人造聚合物和生物体系的多面体低聚硅酸盐纳米结构的低成本相容性基团。表面活性剂的变化也为人造和生物材料的纳米结构化学品提供反应性。具有表面活性剂的纳米结构化学品可用作合金化剂用于从纳米尺度尺度控制材料的结构和体积物理性质。或者，可以从纳米结构中去除表面活性剂以形成纳米尺度分散的二氧化硅颗粒。

5. 发明授权

US07193015B1 Nanostructured chemicals as alloying agents in fluorinated polymers 有权
标题翻译：纳米结构化学品作为氟化聚合物中的合金剂
公开(公告)号：US07193015B1
公开(公告)日：2007-03-20
申请号：US10815544
申请日：2004-03-31
申请人： Joseph M. Mabry , Rene I. Gonzalez , Rusty L. Blanski , Patrick N. Ruth , Brent D. Viers , Joseph J. Schwab , Joseph D. Lichtenhan
发明人： Joseph M. Mabry , Rene I. Gonzalez , Rusty L. Blanski , Patrick N. Ruth , Brent D. Viers , Joseph J. Schwab , Joseph D. Lichtenhan
IPC分类号： C08F8/00
CPC分类号： C08K5/549 , B82Y30/00 , C08G77/045 , C08K2201/011 , C08L27/12 , C08L27/16 , C08L83/06
摘要： A method of using nanostructured chemicals as alloying agents for the reinforcement of flouropolymer microstructures, including polymer coils, domains, chains, and segments, at the molecular level. Because of their tailorable compatibility with fluorinated polymers, nanostructured chemicals can be readily and selectively incorporated into polymers by direct blending processes. Properties most favorably improved are time dependent mechanical and thermal properties such as heat distortion, creep, compression set, shrinkage, modulus, hardness and abrasion resistance. In addition to mechanical properties, other physical properties are favorably improved, including lower thermal conductivity, fire resistance, and improved oxygen permeability. These improved properties may be useful in a number of applications, including space-survivable materials and creep resistant seals and gaskets. Improved surface properties may be useful for applications such as anti-icing or non-wetting surfaces or as low friction surfaces.
摘要翻译：一种使用纳米结构化学药品作为合成剂的方法，用于在分子水平上加强含氟聚合物微观结构，包括聚合物线圈，结构域，链和链段。由于其与氟化聚合物的可定制的相容性，纳米结构化学物质可以通过直接共混方法容易且选择性地引入到聚合物中。最有利地改善的性能是时间相关的机械和热性能，如热变形，蠕变，压缩永久变形，收缩率，模量，硬度和耐磨性。除了机械性能之外，其他物理性能得到有利改善，包括较低的导热性，耐火性和改善的氧气渗透性。这些改进的性能可用于许多应用，包括空间存活材料和抗蠕变密封件和垫圈。改进的表面性质可用于诸如防冰或不润湿表面或作为低摩擦表面的应用。

6. 发明授权

US06933345B1 Reactive grafting and compatibilization of polyhedral oligomeric silsesquioxanes 失效
标题翻译：多面体低聚倍半硅氧烷的反应性接枝和增容
公开(公告)号：US06933345B1
公开(公告)日：2005-08-23
申请号：US10351292
申请日：2003-01-23
申请人： Joseph D. Lichtenhan , Frank J. Feher , Joseph J. Schwab , Sixun Zheng
发明人： Joseph D. Lichtenhan , Frank J. Feher , Joseph J. Schwab , Sixun Zheng
IPC分类号： C08F8/00 , C08K5/5419 , C08K7/00 , C08L83/00
CPC分类号： B82Y30/00 , C08K5/5419 , C08K7/00 , C08K2201/011 , C08L2205/14 , C08L23/10
摘要： The nanoscopic dimensions of polyhedral oligomeric silsesquioxanes (POSS) and polyhedral oligomeric silicates (POS) materials ranges from 0.7 nm to 5.0 nm and enables the thermomechanical and physical properties of polymeric materials to be improved by providing nanoscopic reinforcement of polymer chains at a length scale that is not possible by physically smaller aromatic chemical systems or larger fillers and fibers. A simple and cost effective method for incorporating POSS/POS nanoreinforcements onto polymers via the reactive grafting of suitably functionalized POSS/POS entities with polymeric systems amenable to such processes is described. The method teaches that the resulting POSS-grafted-polymers are particularly well suited for alloying agents by nongrafted POSS entitles such as molecular silicas. The successful alloying of POSS-polymers is aided because their interfacial tensions are reduced relative to non-POSS containing systems.
摘要翻译：多面体低聚倍半硅氧烷（POSS）和多面体低聚硅酸盐（POS）材料的纳米尺寸范围为0.7nm至5.0nm，并且通过以长度尺度提供聚合物链的纳米级增强，可以改善聚合物材料的热机械和物理性能，通过物理上较小的芳族化学体系或较大的填料和纤维是不可能的。描述了通过适当功能化的POSS / POS实体与适合于这种方法的聚合物体系的反应性接枝将POSS / POS纳米增强剂结合到聚合物上的简单且成本有效的方法。该方法教导得到的POSS接枝聚合物特别适用于通过非接枝POSS权利如分子二氧化硅的合金化剂。有助于POSS聚合物的成功合金化，因为它们的界面张力相对于不含POSS的体系而降低。

7. 发明授权

US06911518B2 Polyhedral oligomeric -silsesquioxanes, -silicates and -siloxanes bearing ring-strained olefinic functionalities 有权
公开(公告)号：US06911518B2
公开(公告)日：2005-06-28
申请号：US09747762
申请日：2000-12-21
申请人： Joseph D. Lichtenhan , Joseph J. Schwab , Yi-Zong An , William Reinerth , Frank J. Feher
发明人： Joseph D. Lichtenhan , Joseph J. Schwab , Yi-Zong An , William Reinerth , Frank J. Feher
IPC分类号： C07F7/08 , C07F7/18 , C07F7/21 , C07F11/00 , C08G77/20 , C08G77/08
CPC分类号： C08G77/20 , C07F7/0829 , C07F7/0874 , C07F7/0879 , C07F7/1876 , C07F7/188 , C07F7/21 , C07F11/005
摘要： Processes have been developed for the manufacture of polyhedral oligomeric silsesquioxanes (POSS), polysilsesquioxanes, polyhedral oligomeric silicates (POS), and siloxane molecules bearing reactive ring-strained cyclic olefins (e.g. norbornenyl, cyclopentenyl, etc. functionalities). The preferred manufacturing processes employ the silation of siloxides (Si—OA, where A=H, alkaline or alkaline earth metals) with silane reagents that contain at least one reactive ring-strained cyclic olefin functionality [e.g., X3-ySi(CH3)y(CH2)2 where y=1-2 and X=OH, Cl, Br, I, alkoxide OR, acetate OOCR, peroxide OOR, amine NR2, isocyanate NCO, and R]. Alternatively, similar products can be prepared through hydrosilation reactions between silanes containing at least one silicon-hydrogen bond (Si—H) with ring-strained cyclic olefin reagents [e.g., 5-vinyl, 2 norbornene CH2═CH, cyclopentadiene]. The two processes can be effectively practiced using polymeric silsesquioxanes [RSiO1.5]∞ where ∞=1-1,000,000 or higher and which contain unreacted silanol or silane groups at chain terminus or branch points, on POSS nanostructures of formulas [(RSiO1.5)n]Σ#, homoleptic, [(RSiO1.5)m(R′SiO1.5)n]Σ#, heteroleptic, and {(RSiO1.5)m(RXSiO1.0)n}Σ#, functionalized heteroleptic nanostructures, on silanes RSiX3, linear, cyclic, oligomeric and polymeric siloxanes (polymeric formula RX2Si—(OSiRX)m—OSiRX2 where m=0-1000, X=OH, Cl, Br, I, alkoxide OR, acetate OOCR, peroxide OOR, amine NR2, isocyanate NCO, and R). Each of the processes result in new chemical species bearing one or more ring strained olefins that can undergo polymerization, grafting, or other desirable chemical reactions to form polymeric products. These polymeric systems are most desirably utilized in polymerizations for the modification of properties of thermoplastic or thermoset resin systems or for the preparation of polymers with utility in electronics, medical devices, sporting goods, and aerospace as coatings and structural components.

8. 发明授权

US06716919B2 Nanostructured chemicals as alloying agents in polymers 有权
标题翻译：纳米结构化学品作为聚合物中的合金剂
公开(公告)号：US06716919B2
公开(公告)日：2004-04-06
申请号：US09818265
申请日：2001-03-26
申请人： Joseph D. Lichtenhan , Joseph J. Schwab , Andre Lee , Shawn Phillips
发明人： Joseph D. Lichtenhan , Joseph J. Schwab , Andre Lee , Shawn Phillips
IPC分类号： C08F800
CPC分类号： B82Y30/00 , C08K5/5419 , C08K7/00 , C08K2201/011 , C08L2205/14 , C08L23/10
摘要： A method of using nanostructured chemicals as alloying agents for the reinforcement of polymer microstructures, including polymer coils, domains, chains, and segments, at the molecular level. Because of their tailorable compatibility with polymers, nanostructured chemicals can be readily and selectively incorporated into polymers by direct blending processes. The incorporation of a nanostructured chemical into a polymer favorably impacts a multitude of polymer physical properties. Properties most favorably improved are time dependent mechanical and thermal properties such as heat distortion, creep, compression set, shrinkage, modulus, hardness and abrasion resistance. In addition to mechanical properties, other physical properties are favorably improved, including lower thermal conductivity, fire resistance, and improved oxygen permeability.
摘要翻译：使用纳米结构化学品作为合成剂的方法，用于在分子水平上增强聚合物微结构，包括聚合物线圈，结构域，链和链段。由于其与聚合物的可兼容的相容性，纳米结构化学品可以通过直接共混方法容易且有选择地并入聚合物中。将纳米结构化学物质掺入聚合物有利地影响了许多聚合物的物理性质。最有利地改善的性能是时间相关的机械和热性能，如热变形，蠕变，压缩永久变形，收缩率，模量，硬度和耐磨性。除了机械性能之外，其他物理性能得到有利改善，包括较低的导热性，耐火性和改善的氧气渗透性。

9. 发明申请

US20110201827A1 PROCESS FOR CONTINUOUS PRODUCTION OF OXIDIZED OLEFIN POLYHEDRAL OLIGOMERIC SILSESQUIOXANE CAGES 审中-公开
标题翻译：连续生产氧化烯烃聚氧乙烯低聚硅氧烷的方法
公开(公告)号：US20110201827A1
公开(公告)日：2011-08-18
申请号：US13026529
申请日：2011-02-14
申请人： Joseph D. Lichtenhan , Sukhendu Bikash Hait , Joseph J. Schwab , Michael J. Carr
发明人： Joseph D. Lichtenhan , Sukhendu Bikash Hait , Joseph J. Schwab , Michael J. Carr
IPC分类号： C07F7/18
CPC分类号： A61K8/895 , A61Q19/00 , C07F7/0874 , C07F7/21
摘要： Methods for continuous bulk production of polyolefin polyhedral oligomeric silsesquioxanes and their amino, isocyanate, and alcohol derivatives using silane coupling agents as precursors.
摘要翻译：使用硅烷偶联剂作为前体的连续大量生产聚烯烃多面体低聚倍半硅氧烷及其氨基，异氰酸酯和醇衍生物的方法。

10. 发明申请

US20110184139A1 METAL COMPOSITIONS AND METHODS OF MAKING SAME 有权
标题翻译：金属组合物及其制备方法
公开(公告)号：US20110184139A1
公开(公告)日：2011-07-28
申请号：US12737694
申请日：2009-06-27
申请人： Mangala Malik , Joseph J. Schwab
发明人： Mangala Malik , Joseph J. Schwab
IPC分类号： C08F230/04 , B32B3/10 , G03F7/20
CPC分类号： C23C18/14 , C23C18/06 , H05K3/105 , Y10T428/24802
摘要： The present invention relates to a process for forming metal-containing films by applying a photosensitive metal-containing composition on a substrate, drying the photosensitive metal-containing composition, exposing the photosensitive metal-containing composition to a source of actinic radiation and applying a post- treatment to the metal-containing composition. The process also includes exposing the photosensitive metal-containing composition to a source of actinic radiation through a mask or mold and developing the unexposed portion of the composition. Another embodiment of the invention is a metal-containing film, three-dimensional object or article formed by the process. The invention is useful in producing a directly patterned metal-containing film and a microdevice.
摘要翻译：本发明涉及通过将含感光性金属的组合物涂布在基材上，干燥含有感光性金属的组合物，将含有感光性金属的组合物曝露于光化辐射源并施加柱 - 对含金属组合物的处理。该方法还包括将含感光金属的组合物暴露于光化辐射源通过掩模或模具并显影组合物的未曝光部分。本发明的另一个实施方案是通过该方法形成的含金属膜，三维物体或制品。本发明可用于生产直接图案化的含金属膜和微型设备。

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