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1. 发明申请

US20090297854A1 AA STACKED GRAPHENE-DIAMOND HYBRID MATERIAL BY HIGH TEMPERATURE TREATMENT OF DIAMOND AND THE FABRICATION METHOD THEREOF 审中-公开
标题翻译： AA钻石高温处理堆积石墨 - 金刚石混合材料及其制造方法
公开(公告)号：US20090297854A1
公开(公告)日：2009-12-03
申请号：US12437838
申请日：2009-05-08
申请人： Jae-Kap LEE , So-Hyung LEE , Seung-Cheol LEE , Jae-Pyoung AHN , Jeon-Kook LEE , Wook-Seong LEE
发明人： Jae-Kap LEE , So-Hyung LEE , Seung-Cheol LEE , Jae-Pyoung AHN , Jeon-Kook LEE , Wook-Seong LEE
IPC分类号： B32B9/00 , B01J19/12 , B82B1/00 , B82B3/00
CPC分类号： B01J3/006 , B01J19/088 , B01J2219/0809 , B01J2219/0879 , B01J2219/0894 , C01B32/20 , C01B32/25 , C01B32/28 , C30B29/04 , C30B33/02 , Y10T428/30
摘要： There is provided a fabrication method for an AA stacked graphene-diamond hybrid material by converting, through a high temperature treatment on diamond, a diamond surface into graphene. According to the present invention, if various types of diamond are maintained at a certain temperature having a stable graphene phase (approximately greater than 1200° C.) in a hydrogen gas atmosphere, two diamond {111} lattice planes are converted into one graphene plate (2:1 conversion), whereby the diamond surface is converted into graphene in a certain thickness, thus to fabricate the AA stacked graphene-diamond hybrid material.
摘要翻译：通过将金刚石上的高温处理，金刚石表面转化成石墨烯，提供了一种用于AA堆叠的石墨烯 - 金刚石混合材料的制造方法。根据本发明，如果各种类型的金刚石在氢气气氛中保持在稳定的石墨烯相（大约大于1200℃）的一定温度下，则将两个菱形{111}晶格面转换为一个石墨烯板（2:1转化），由此将金刚石表面转化成一定厚度的石墨烯，从而制造AA堆叠的石墨烯 - 金刚石混合材料。

2. 发明授权

US08672246B2 Method for purifying graphene powder 有权
标题翻译：石墨烯粉末的净化方法
公开(公告)号：US08672246B2
公开(公告)日：2014-03-18
申请号：US13211609
申请日：2011-08-17
申请人： Jae Kap Lee , Kyoung-Il Lee
发明人： Jae Kap Lee , Kyoung-Il Lee
IPC分类号： B02C19/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/196 , C01P2004/64
摘要： An easy and effective method for purifying graphene powder by removing magnetic impurities, wherein magnetic impurities are incorporated during the process of fabricating the graphene powder, is provided. The method for purifying graphene powder, the method including: (1) ball-milling a graphite material to form graphene powder; (2) dispersing the graphene powder in a solvent to form a suspension; and (3) separating magnetic impurities during stirring the suspension, by using a magnet, Wherein the magnetic impurities were incorporated into the graphene powder during ball-milling from the balls and dispersed in the suspension.
摘要翻译：提供了一种通过去除在制造石墨烯粉末的过程中并入磁性杂质的磁性杂质来净化石墨烯粉末的简单有效的方法。石墨烯粉末的净化方法，该方法包括：（1）对石墨材料进行球磨以形成石墨烯粉末; （2）将石墨烯粉末分散在溶剂中以形成悬浮液; 和（3）通过使用磁体在搅拌悬浮液期间分离磁性杂质，其中在从球中球磨过程中将磁性杂质掺入石墨烯粉末中并分散在悬浮液中。

3. 发明申请

US20110097258A1 METHOD FOR PREPARING GRAPHENE RIBBONS WHERE STRUCTURE IS CONTROLLED 审中-公开
标题翻译：用于制备结构控制的石墨纤维的方法
公开(公告)号：US20110097258A1
公开(公告)日：2011-04-28
申请号：US12909958
申请日：2010-10-22
申请人： Jae-Kap LEE , Kyoung-Il LEE , So-Hyung LEE
发明人： Jae-Kap LEE , Kyoung-Il LEE , So-Hyung LEE
IPC分类号： C01B31/04 , B82Y40/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/186 , C01B32/194 , C01B2204/065
摘要： Disclosed is a method for fabricating graphene ribbons which are high-functional carbon materials. Provided a method of fabricating graphene ribbons, including (a) preparing a carbon structure in which a graphene ribbon is spirally grown (a graphene helix), revealing a tube shape, and (b) applying energy to unroll the graphene helix into the graphene ribbons.
摘要翻译：公开了一种制造高功能碳材料的石墨烯带的方法。提供了一种制造石墨烯带的方法，包括（a）制备其中石墨烯带螺旋生长（石墨烯螺旋）的碳结构，露出管状，和（b）施加能量以将石墨烯螺旋展开到石墨烯带。

4. 发明授权

US07776445B2 Graphene-diamond hybrid material and method for preparing same using chemical vapor deposition 有权
标题翻译：石墨烯 - 金刚石杂化材料及其使用化学气相沉积的方法
公开(公告)号：US07776445B2
公开(公告)日：2010-08-17
申请号：US12191801
申请日：2008-08-14
申请人： Jae Kap Lee , Seung Cheol Lee , Phillip John , Wook Seong Lee , Jeon Kook Lee
发明人： Jae Kap Lee , Seung Cheol Lee , Phillip John , Wook Seong Lee , Jeon Kook Lee
IPC分类号： B32B9/00 , C23C16/26
CPC分类号： C30B29/02 , B82Y15/00 , B82Y30/00 , B82Y40/00 , C01B32/188 , C23C16/01 , C23C16/26 , C30B25/02 , C30B29/04 , Y10S977/742 , Y10T428/30
摘要： Disclosed herein are a graphene hybrid material and a method for preparing the graphene hybrid material, the graphene hybrid material comprising: a matrix having lattice planes disconnected on a surface thereof; and layers of graphene which are epitaxially grown along the lattice planes disconnected on the surface of the matrix such that the layers of graphene are oriented perpendicularly to the matrix, and which are spaced apart from each other and layered on the matrix in the same shape. The graphene hybrid material can be usefully used in the fields of next-generation semiconductor devices, biosensors, electrochemical electrodes and the like.
摘要翻译：本发明公开了石墨烯混合材料和石墨烯混合材料的制备方法，所述石墨烯混合材料包括：具有在其表面上断开晶格面的矩阵; 以及沿着在基体表面上断开的晶格面外延生长的石墨烯层，使得石墨烯层垂直于矩阵定向，并且彼此间隔开并以相同形状层叠在基体上。石墨烯混合材料可用于下一代半导体器件，生物传感器，电化学电极等领域。

5. 发明申请

US20100028573A1 AA' STACKED GRAPHITE AND FABRICATION METHOD THEREOF 有权
标题翻译： AA'堆积石墨及其制造方法
公开(公告)号：US20100028573A1
公开(公告)日：2010-02-04
申请号：US12512942
申请日：2009-07-30
申请人： Jae-Kap LEE , So-Hyung Lee , Jae-Pyoung Ahn , Seung-Cheol Lee , Wook-Seong Lee
发明人： Jae-Kap LEE , So-Hyung Lee , Jae-Pyoung Ahn , Seung-Cheol Lee , Wook-Seong Lee
IPC分类号： B32B9/00 , B32B1/08 , B32B1/00 , C23C16/26
CPC分类号： C23C16/26 , B82Y30/00 , C01B32/20 , C01P2002/78 , Y10T428/13 , Y10T428/261 , Y10T428/298 , Y10T428/2982
摘要： Disclosed is AA′ graphite with a new stacking feature of graphene, and a fabrication method thereof. Graphene is stacked in the sequence of AA′ where alternate graphene layers exhibiting the AA′ stacking are translated by a half hexagon (1.23 Å). AA′ graphite has an interplanar spacing of about 3.44 Å larger than that of the conventional AB stacked graphite (3.35 Å) that has been known as the only crystal of pure graphite. This may allow the AA′ stacked graphite to have unique physical and chemical characteristics.
摘要翻译：公开了具有石墨烯的新堆叠特征的AA'石墨及其制造方法。石墨烯以AA'的顺序堆叠，其中呈现AA'层叠的交替石墨烯层被半六边形（1.23）平移。 AA'石墨具有比已知为纯石墨的唯一晶体的常规AB堆叠石墨（3.35埃）的面间距大约3.44埃。这可能使AA的堆积石墨具有独特的物理和化学特性。

6. 发明申请

US20090047520A1 GRAPHENE HYBRID MATERIAL AND METHOD FOR PREPARING SAME USING CHEMICAL VAPOR DEPOSITION 有权
标题翻译：石墨混合材料及其使用化学蒸气沉积法制备其的方法
公开(公告)号：US20090047520A1
公开(公告)日：2009-02-19
申请号：US12191801
申请日：2008-08-14
申请人： Jae Kap LEE , Seung Cheol LEE , Phillip JOHN , Wook Seong LEE , Jeon Kook LEE
发明人： Jae Kap LEE , Seung Cheol LEE , Phillip JOHN , Wook Seong LEE , Jeon Kook LEE
IPC分类号： B32B9/00 , C23C16/26
CPC分类号： C30B29/02 , B82Y15/00 , B82Y30/00 , B82Y40/00 , C01B32/188 , C23C16/01 , C23C16/26 , C30B25/02 , C30B29/04 , Y10S977/742 , Y10T428/30
摘要： Disclosed herein are a graphene hybrid material and a method for preparing the graphene hybrid material, the graphene hybrid material comprising: a matrix having lattice planes disconnected on a surface thereof; and layers of graphene which are epitaxially grown along the lattice planes disconnected on the surface of the matrix such that the layers of graphene are oriented perpendicularly to the matrix, and which are spaced apart from each other and layered on the matrix in the same shape. The graphene hybrid material can be usefully used in the fields of next-generation semiconductor devices, biosensors, electrochemical electrodes and the like.
摘要翻译：本发明公开了石墨烯混合材料和石墨烯混合材料的制备方法，所述石墨烯混合材料包括：具有在其表面上断开晶格面的矩阵; 以及沿着在基体表面上断开的晶格面外延生长的石墨烯层，使得石墨烯层垂直于矩阵定向，并且彼此间隔开并以相同形状层叠在基体上。石墨烯混合材料可用于下一代半导体器件，生物传感器，电化学电极等领域。

7. 发明申请

US20080166479A1 Diamond Shell with a Geometrical Figure and Method for Fabrication Thereof 有权
标题翻译：具有几何图形的金刚石外壳及其制造方法
公开(公告)号：US20080166479A1
公开(公告)日：2008-07-10
申请号：US10574264
申请日：2005-10-19
申请人： Jae Kap Lee , Philip John
发明人： Jae Kap Lee , Philip John
IPC分类号： C23C16/27
CPC分类号： C23C16/0254 , C23C16/01 , C23C16/042 , C23C16/272 , C23C16/274 , C30B25/18 , C30B29/04
摘要： This invention provides a method for fabricating geometrical diamond/matrix composites where all or a part of surfaces of the matrix are covered with a diamond film, and to fabricate hollow diamond shells using the composites where a part is uncoated with a diamond film. Hollow diamond shells were prepared by etching out of the matrix soluble with chemicals through an opening, a zone on the matrix, uncoated with diamond film. By changing the shape and the size of the geometrical matrixes, various kinds of diamond/matrix composites and diamond shells in shape and in size can be fabricated. The sizes available are between 200 nm and 2 mm.
摘要翻译：本发明提供了一种用于制造几何金刚石/基体复合材料的方法，其中基体的全部或一部分表面被金刚石膜覆盖，并且使用复合材料制造中空的金刚石壳体，其中一部分未被金刚石膜涂覆。通过蚀刻出可溶于基质的基质，通过开孔，基体上的区域，用金刚石薄膜未涂覆来制备空心金刚石壳。通过改变几何矩阵的形状和尺寸，可以制造各种形状和尺寸的金刚石/基体复合材料和金刚石壳。可用的尺寸在200nm和2mm之间。

8. 发明授权

US06319439B1 Method of synthesizing even diamond film without cracks 失效
标题翻译：偶合金刚石薄膜无裂纹的方法
公开(公告)号：US06319439B1
公开(公告)日：2001-11-20
申请号：US09513319
申请日：2000-02-25
申请人： Jae-Kap Lee , Young Joon Baik , Kwang Yong Eun
发明人： Jae-Kap Lee , Young Joon Baik , Kwang Yong Eun
IPC分类号： C30B2500
CPC分类号： C23C16/272 , C23C16/27 , C30B25/105 , C30B29/04
摘要： A method of synthesizing an even free-standing diamond film without growth cracks is disclosed. The intrinsic tensile stress of a diamond film is compensated by an artificial compressive stress with a step down control of the deposition temperature during deposition. After a diamond film is deposited with a predetermined thickness at a deposition temperature, the deposition temperature is decreased in multiple steps during the deposition. The bending of the diamond wafer is minimized by using a tungsten substrate with higher elastic modulus than molybdenum.
摘要翻译：公开了一种合成均匀自立金刚石膜而没有生长裂纹的方法。金刚石膜的固有拉伸应力通过人造压缩应力补偿，同时降低沉积期间沉积温度的控制。在沉积温度下以预定厚度沉积金刚石膜之后，在沉积期间沉积温度以多个步骤降低。通过使用具有比钼更高的弹性模量的钨基材，使金刚石晶片的弯曲最小化。

9. 发明授权

US09200363B2 AA' stacked graphite and fabrication method thereof 有权
标题翻译： AA'堆石墨及其制造方法
公开(公告)号：US09200363B2
公开(公告)日：2015-12-01
申请号：US12512942
申请日：2009-07-30
申请人： Jae-Kap Lee , So-Hyung Lee , Jae-Pyoung Ahn , Seung-Cheol Lee , Wook-Seong Lee
发明人： Jae-Kap Lee , So-Hyung Lee , Jae-Pyoung Ahn , Seung-Cheol Lee , Wook-Seong Lee
IPC分类号： C01B31/04 , C23C16/26 , B82Y30/00
CPC分类号： C23C16/26 , B82Y30/00 , C01B32/20 , C01P2002/78 , Y10T428/13 , Y10T428/261 , Y10T428/298 , Y10T428/2982
摘要： Disclosed is AA′ graphite with a new stacking feature of graphene, and a fabrication method thereof. Graphene is stacked in the sequence of AA′ where alternate graphene layers exhibiting the AA′ stacking are translated by a half hexagon (1.23 Å). AA′ graphite has an interplanar spacing of about 3.44 Å larger than that of the conventional AB stacked graphite (3.35 Å) that has been known as the only crystal of pure graphite. This may allow the AA′ stacked graphite to have unique physical and chemical characteristics.
摘要翻译：公开了具有石墨烯的新堆叠特征的AA'石墨及其制造方法。石墨烯以AA'的顺序堆叠，其中呈现AA'层叠的交替石墨烯层被半六边形（1.23）平移。 AA'石墨具有比已知为纯石墨的唯一晶体的常规AB堆叠石墨（3.35埃）的面间距大约3.44埃。这可能使AA的堆积石墨具有独特的物理和化学特性。

10. 发明授权

US08597607B2 Method for preparing graphene ribbons 有权
标题翻译：制备石墨烯带的方法
公开(公告)号：US08597607B2
公开(公告)日：2013-12-03
申请号：US12545740
申请日：2009-08-21
申请人： Jae-Kap Lee , So-Hyung Lee , Wook-Seong Lee
发明人： Jae-Kap Lee , So-Hyung Lee , Wook-Seong Lee
IPC分类号： C09C1/44
CPC分类号： C09C1/44 , B82Y30/00 , B82Y40/00 , C01B32/184 , C01B32/19 , C01B2204/04 , C01B2204/06 , C01P2002/77
摘要： Disclosed is a method for fabricating graphene ribbons, comprising: preparing a graphitic material comprising stacked graphene helices; and cutting the graphitic material in a short form by applying energy to the graphitic material; and simultaneously or afterward, decomposing the graphitic material into short graphene ribbons. This method provides a mass production route to graphene ribbons.
摘要翻译：公开了一种制造石墨烯带的方法，包括：制备包括堆积的石墨烯螺旋的石墨材料; 并通过向石墨材料施加能量来以短形式切割石墨材料; 同时或之后，将石墨材料分解成短的石墨烯带。这种方法提供了石墨烯带的大规模生产路线。

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