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1. 发明申请

US20040164439A1 Process for removing volatile components in polyarylene sulfide 失效
标题翻译：去除聚芳硫醚中挥发性成分的方法
公开(公告)号：US20040164439A1
公开(公告)日：2004-08-26
申请号：US10368564
申请日：2003-02-20
申请人： IDEMITSU PETROCHEMICAL CO., LTD. , PETROLEUM ENERGY CENTER
发明人： Yoshinari Koyama
IPC分类号： B29C047/60 , B29C047/76
CPC分类号： B29C47/767 , B29C47/0009 , B29C47/40 , B29C47/6056 , B29C47/64 , B29C47/763
摘要： There is disclosed a process for removing volatile components in a polyarylene sulfide resin which is produced by subjecting a sulfur source and a dihalogenated aromatic compound to polymerization reaction in an aprotic organic solvent, comprising using an extruder which is equipped with front vent having an opening length in the range of 4D to 11D (D: screw diameter) and which has a distance between a terminal position of a screw in a kneading portion and the opening portion of the front vent being in the range of 4D to 15D. The process is capable of steadily and economically removing volatile components in the polyarylene sulfide resin without necessitating expensive machinery or equipment such as a dryer without plugging up the opening portion of a vent even in the case of degassing a PAS resin having a low molecular weight and further, thus enabling a long-term continuous stable running.
摘要翻译：公开了一种除去聚亚芳基硫醚树脂中的挥发性组分的方法，该方法是通过使硫源和二卤代芳族化合物在非质子性有机溶剂中进行聚合反应而制备的，其包括使用挤出机，该挤出机配备有具有开口长度在4D至11D（D：螺杆直径）的范围内，并且其具有揉捏部分中的螺杆的终端位置与前排气孔的开口部分之间的距离在4D至15D的范围内。该方法能够稳定且经济地除去聚芳硫醚树脂中的挥发性组分，而不需要昂贵的机械或设备如干燥机，而不会堵塞排气孔的开口部分，即使在脱气低分子量的PAS树脂的情况下，从而能够长期持续稳定运行。

2. 发明申请

US20030120014A1 Propylenic random copolymer and composition comprising it, and film comprising the copolymer or composition 失效
标题翻译：丙烯酸无规共聚物和包含它的组合物，以及包含共聚物或组合物的膜
公开(公告)号：US20030120014A1
公开(公告)日：2003-06-26
申请号：US10301708
申请日：2002-11-22
申请人： Idemitsu Petrochemical Co., Ltd.
发明人： Yasushi Seta , Satoshi Nakatsuka , Michihiro Sawada , Ryoichi Tsunori
IPC分类号： C08F010/00
CPC分类号： B32B27/08 , B32B27/32 , B32B2250/24 , B32B2307/514 , C08F210/06 , C08F210/16 , C08J5/18 , C08J2323/14 , C08L23/04 , C08L23/142 , Y10T428/1328 , Y10T428/1334 , Y10T428/1352 , Y10T428/31909 , Y10T428/31913 , Y10T428/31938 , C08F4/6565 , C08F4/6465 , C08L2666/04 , C08F2500/15 , C08F2500/26
摘要： Provided are a propylenic random copolymer of propylene and ethylene satisfying the following (1) to (5), a composition comprising the copolymer, a film and a stretched film of the copolymer or its composition, and a laminate film and a stretched laminate film comprising at least one layer of the copolymer or its composition. (1) The ethylene unit content (x, wt. %) of the copolymer is from 0.2 to 10 wt. %. (2) The copolymer has a melt index (MI, g/10 min) of from 0.1 to 4 g/10 min. (3) The relation between the boiling diethyl ether extraction (E, wt. %) of the copolymer and x satisfies the following (I) or (II);Enull0.253xnull1.1 (0.2nullx
摘要翻译：提供一种丙烯和乙烯的丙烯和乙烯的丙烯无规共聚物，其满足以下（1）至（5），包括共聚物或其组合物的共聚物，膜和拉伸膜的组合物，以及层压膜和拉伸层压膜，至少一层共聚物或其组合物。（1）共聚物的乙烯单元含量（x，重量％）为0.2〜10重量％。％。（2）共聚物的熔融指数（MI，g / 10分钟）为0.1〜4g / 10分钟。（3）共聚物的沸腾二乙醚萃取（E，wt。％）与x的关系满足下列（I）或（II）：E <= 0.253x + 1.1（0.2 <= x <6） I）E <= 2.6（6 <= x <= 10）（II）（4）用差示扫描量热计测量的共聚物的熔点（Tm，℃）与x之间的关系满足以下（ III）：Tm <= 165-5x（III）（5）在13 C-NMR中测定的共聚物的PPP序列中的全同立构三单元组分数（mm，摩尔％）不小于98.0摩尔％。该薄膜具有良好的刚度，低温热封性，热收缩性，热滑性，防粘连性和冷滑性，并且有利地用作包装或包装收缩膜。

3. 发明申请

US20030022990A1 Aromatic vinyl polymer resin composition and its molding 失效
标题翻译：芳香族乙烯基聚合物树脂组合物及其成型
公开(公告)号：US20030022990A1
公开(公告)日：2003-01-30
申请号：US10196195
申请日：2002-07-17
申请人： IDEMITSU PETROCHEMICAL CO., LTD.
发明人： Shogo Hirota , Ryozo Okumura , Makoto Wakabayashi
IPC分类号： C08L053/00
CPC分类号： C08J9/0061 , C08J9/122 , C08J2201/03 , C08J2325/06 , C08J2453/00 , C08L25/06 , C08L53/02 , C08L2666/24
摘要： Provided are an aromatic vinyl polymer resin composition capable of being molded into resin foam sheets having good surface smoothness and glossiness well balanced with the mechanical strength thereof even when the expansion ratio in molding is increased, and resin foam sheets and containers of the composition. The resin composition comprises (A) from 80 to 98% by mass of an aromatic vinyl polymer resin having a weight-average molecular weight measured through GPC of from 200,000 to 400,000, a ratio of weight-average molecular weight to number-average molecular weight ranging from 2.2 to 3.6, a number of branches of from 0.1 to 1.0 in one molecule having an absolute molecular weight of 1,190,000 measured through GPC-MALLS, and a melt flow rate of from 1.5 to 3.5 g/10 min, and (B) from 2 to 20% by mass of a styrene-diene block copolymer or its hydrogenate. This is molded into a resin foam sheet through extrusion foaming, and the sheet is thermoformed into containers.
摘要翻译：提供一种芳族乙烯基聚合物树脂组合物，其即使当成型时的膨胀比增加时，也可以模塑成具有良好的表面光滑度和光泽度的树脂发泡体片材，并且其组合物的树脂发泡片材和容器。树脂组合物包含（A）80〜98质量％的通过GPC测定的重均分子量为20万〜40万的芳族乙烯基聚合物树脂，重均分子量与数均分子量的比例范围为2.2至3.6，通过GPC-MALLS测量的绝对分子量为1,190,000的一个分子中的分支数为0.1至1.0，熔体流动速率为1.5-3.5g / 10min，（B） 2〜20质量％的苯乙烯 - 二烯嵌段共聚物或其氢化物。通过挤出发泡将其模制成树脂发泡片材，并将片材热成型为容器。

4. 发明申请

US20020187267A1 Method of producing the plated molded articles by non-electrode plating, and the resin compositions for that use 失效
标题翻译：通过非电极电镀制造电镀模制品的方法和用于该用途的树脂组合物
公开(公告)号：US20020187267A1
公开(公告)日：2002-12-12
申请号：US10157883
申请日：2002-05-31
申请人： IDEMITSU PETROCHEMICAL CO., LTD.
发明人： Eiji Tamura , Wataru Kosaka , Toshimi Arashi
IPC分类号： B05D003/12 , C08L067/00
CPC分类号： H05K3/381 , C23C18/1653 , C23C18/2013 , C23C18/285 , C23C18/30 , C23C18/34 , C23C18/40 , H05K1/0373 , H05K3/181 , H05K2201/0129 , H05K2201/0209 , H05K2201/0248 , H05K2201/09118 , H05K2203/025
摘要： A process for producing an electrolessly plated molded article, which includes molding a resin composition made of a thermoplastic resin having a specific Izod impact strength and a Rockwell surface hardness and an inorganic filler, then treating the surface of the molded article with air blast using an abrasive having a sharp granular shape, and then conducting catalyst coating, activation treatment and electroless plating. It has been possible to apply the electroless plating with a high adhesion strength to the molded article of the thermoplastic resin composition without conducting the chemical etching treatment.
摘要翻译：一种无电镀模塑制品的制造方法，其包括将具有特定艾佐德冲击强度的热塑性树脂和洛氏硬度的无机填料制成的树脂组合物成型，然后使用空气吹扫处理模制品的表面研磨剂具有尖锐的颗粒形状，然后进行催化剂涂覆，活化处理和化学镀。可以对热塑性树脂组合物的成型体施加高粘合强度的无电镀，而不进行化学蚀刻处理。

5. 发明申请

US20020115802A1 Ethylene copolymer and aromatic vinyl graft copolymer and method for producing the same 审中-公开
公开(公告)号：US20020115802A1
公开(公告)日：2002-08-22
申请号：US10072994
申请日：2002-02-12
申请人： IDEMITSU PETROCHEMICAL CO., LTD.
发明人： Hideo Teshima , Masanori Sera
IPC分类号： C08F004/44
CPC分类号： C08F290/042 , C08F10/00 , C08F10/02 , C08F210/02 , C08F4/65912 , C08F4/6592 , C08F212/08 , C08F212/36 , C08F2500/03 , C08F2500/17
摘要： The present invention provides resin materials endowed with excellent heat resistance, solvent resistance, tensile elongation, toughness, and transparency. Specifically, there are provided an ethylene copolymer having a vinyl group attributed to a diene monomer in the molecular chain and comprising an aromatic vinyl monomer (A), ethylene (B) and a diene monomer (C), and an aromatic vinyl graft copolymer which is a graft copolymerization product of an aromatic vinyl monomer (H) and an ethylene copolymer macromer (I).

6. 发明申请

US20020010290A1 Process for producing a polymer of an alpha-olefin and lubricant 有权
标题翻译：制备α-烯烃和润滑剂的聚合物的方法
公开(公告)号：US20020010290A1
公开(公告)日：2002-01-24
申请号：US09860912
申请日：2001-05-21
申请人： Idemitsu Petrochemical Co., Ltd.
发明人： Yutaka Minami , Tatsuya Egawa
IPC分类号： C08F004/44
CPC分类号： C10M143/08 , C08F4/65912 , C08F10/00 , C08F110/14 , C10M107/10 , C10M2205/028 , C10N2220/02 , Y10S526/905 , C08F4/63927 , C08F2500/03 , C08F2500/17
摘要： A process for producing a polymer of an null-olefin which comprises polymerizing an null-olefin having at least 4 carbon atoms in the presence of a catalyst for producing polymers of olefins which comprises (A) a specific metal compound and (B) at least one compound selected from (b-1) an organoaluminum oxy compound and (b-2) an ionic compound. The polymer of an null-olefin is useful as a component of lubricant.
摘要翻译：一种制备α-烯烃聚合物的方法，其包括在用于制备烯烃聚合物的催化剂存在下聚合具有至少4个碳原子的α-烯烃，所述催化剂包含（A）特定金属化合物和（B）至少一种选自（b-1）有机铝氧化合物和（b-2）离子化合物的化合物。 α-烯烃的聚合物可用作润滑剂的组分。

7. 发明申请

US20010025085A1 Aromatic vinyl resin material and molded products thereof 失效
标题翻译：芳族乙烯基树脂材料及其成型品
公开(公告)号：US20010025085A1
公开(公告)日：2001-09-27
申请号：US09773904
申请日：2001-02-02
申请人： IDEMITSU PETROCHEMICAL CO., LTD.
发明人： Hideo Teshima , Tomoaki Takebe , Masanori Sera
IPC分类号： C08F255/02 , C08F210/02 , C08F212/06 , C08F212/08 , C08F279/00 , C08F279/02
CPC分类号： C08F290/04 , C08F290/044
摘要： The present invention provides resin materials for producing molded products endowed with excellent heat resistance, solvent resistance, toughness, tensile elongation, and transparency. Specifically, there are provided aromatic vinyl resin materials which have the following properties: Storage elasticity values Gnull(1.0) and Gnull(0.1) as measured at 300null C., a strain null of 20%, and a frequency of 1.0 Hz or 0.1 Hz satisfy the expression, lognullGnull(1.0)/Gnull(0.1)nullnull0.6, the heat of fusion nullH as measured over the range 200-295null C. is 8 to 50 (J/g), and the 1H-NMR peak integrated values for the fraction corresponding to the temperature range of not lower than 50null C., as collected from temperature rising election fraction on the Soxhlet extraction residue by use of cyclohexane or o-dichlorobenzene, satisfy the relation null1.8-2.1 (ppm)null/null1.0-1.7(ppm))
摘要翻译：本发明提供了具有优异的耐热性，耐溶剂性，韧性，拉伸伸长率和透明性的用于生产模塑制品的树脂材料。具体地说，提供具有以下特性的芳香族乙烯基树脂材料：在300℃下测定的储存弹性值G'（1.0）和G'（0.1），20％的应变γ和1.0Hz的频率或0.1Hz满足log [G'（1.0）/ G'（0.1）] <= 0.6的表达式，在200-295℃范围内测量的熔融热DELTAH为8〜50（J / g），并且通过使用环己烷或邻二氯苯从索格利特提取残渣的升温选择分数收集的对应于不低于50℃的温度范围的馏分的1 H-NMR峰积分值满足关系式 [1.8-2.1（ppm）] / [1.0-1.7（ppm））<0.49。

8. 发明申请

US20040259720A1 Catalyst for vinyl compound polymerization and process for producing vinyl polymer 失效
标题翻译：用于乙烯基化合物聚合的催化剂和用于生产乙烯基聚合物的方法
公开(公告)号：US20040259720A1
公开(公告)日：2004-12-23
申请号：US10889117
申请日：2004-07-13
申请人： IDEMITSU PETROCHEMICAL CO., LTD.
发明人： Haruhito Sato , Masami Watanabe , Masahiko Kuramoto
IPC分类号： B01J031/00
CPC分类号： C07C2/32 , C07C2/04 , C07C2521/16 , C07C2531/14 , C07C2531/16 , C08F10/00 , Y10S526/943 , C08F4/7042 , C08F4/7006
摘要： The catalyst for polymerizing vinyl compounds according to the present invention comprises (A) a complex of Group 4 to 10 transition metal of the Periodic Table, (B) a clay, clay mineral or ion-exchangeable layered compound, and (C) at least one aluminoxy compound represented by Formula (1): 1 wherein a plurality of R groups are each independently C1-10 hydrocarbon group and at least one of the R groups is a hydrocarbon group having 2 or more carbon atoms; and x is an integer of 2 or more. By using the Group 4 to 10 transition metal complex and the clay, clay mineral or ion-exchangeable layered compound in combination with the specific aluminoxy compound, vinyl polymers are produced at a high efficiency. Also, the catalyst for producing null-olefins according to the present invention comprises (Anull) a complex of Group 8 to 10 transition metal of the Periodic Table, (Bnull) an organic compound-modified clay, clay mineral or ion-exchangeable layered compound, and (Cnull) at least one aluminoxy compound represented by Formula (2): 2 wherein a plurality of R groups are each independently C1-10 hydrocarbon group and at least one of the R groups is a hydrocarbon group having 2 or more carbon atoms; and y is an integer of 2 to 4. Since the organic compound-modified clay, clay mineral or ion-exchangeable layered compound absorbs other catalyst components between layers thereof, the elution of the catalyst components into liquid phase is effectively prevented, thereby facilitating the separation of the catalyst from a reaction product.
摘要翻译：根据本发明的用于聚合乙烯基化合物的催化剂包含（A）元素周期表第4至10族过渡金属的络合物，（B）粘土，粘土矿物或可离子交换层状化合物，和（C）至少一种由式（1）表示的铝氧化合物：其中多个R基团各自独立地为C 1-10烃基，并且至少一个R基团为具有2个或更多个碳原子的烃基; x为2以上的整数。通过使用4至10族过渡金属络合物和粘土，粘土矿物或可离子交换的层状化合物与特定的铝氧化合物的组合，以高效率生产乙烯基聚合物。此外，根据本发明的用于制备α-烯烃的催化剂包含（A'）元素周期表第8-10族过渡金属的络合物，（B'）有机化合物改性的粘土，粘土矿物或可离子交换的层状化合物和（C'）至少一种由式（2）表示的铝氧化合物：其中多个R基团各自独立地为C1-10烃基，并且至少一个R基团为具有2个或更多个的烃基碳原子 y为2〜4的整数。由于有机化合物改性粘土，粘土矿物或离子交换性层状化合物在其层之间吸收其他催化剂成分，因此有效地防止了催化剂成分向液相的溶出，催化剂与反应产物的分离。

9. 发明申请

US20040198931A1 Magnesium compound, olefin polymerization catalyst, and method for producing olefin polymer 有权
公开(公告)号：US20040198931A1
公开(公告)日：2004-10-07
申请号：US10831327
申请日：2004-04-26
申请人： IDEMITSU PETROCHEMICAL CO., LTD.
发明人： Shohjiroh Tanase , Takehiro Tsuda , Tsuyoshi Ota , Hideo Funabashi
IPC分类号： C08F004/44 , B01J031/00
CPC分类号： C08F110/06 , C08F4/6565 , C08F2500/18 , C08F2500/24
摘要： The invention relates to a magnesium compound effective in producing olefin polymers having an increased bulk density and a narrowed particle size distribution, not lowering the stereospecificity of the polymers produced and not lowering the polymerization activity in producing the polymers, to an olefin polymerization catalyst comprising the compound, and to a method for producing such olefin polymers. The olefin polymerization catalyst comprises (A) a solid catalyst component prepared by contacting a magnesium compound having a specific particle size distribution index (P), a titanium compound and an electron donor compound with each other, (B) an organometallic compound, and (C) an electron donor. The olefin polymerization method comprises polymerizing an olefin in the presence of the catalyst to give olefin polymers.

10. 发明申请

US20040192975A1 Process for producing bisphenol A 失效
公开(公告)号：US20040192975A1
公开(公告)日：2004-09-30
申请号：US10822703
申请日：2004-04-13
申请人： IDEMITSU PETROCHEMICAL CO., LTD.
发明人： Masahiro Iwahara , Tetsuya Saruwatari
IPC分类号： C07C039/16
CPC分类号： C07C37/20 , Y02P20/52 , C07C39/16
摘要： There is disclosed a process for producing bisphenol A by subjecting phenol and acetone to condensation reaction in the presence of a catalyst composed of an acid type ion exchange resin which is modified in part with a sulfur-containing amine compound, wherein the ion exchange resin having a modification rate of 10 to less than 20 mol % is used for a methanol concentration in acetone of lower than 250 ppm by weight, and the ion exchange resin having a modification rate of 20 to 65 mol % is used for a methanol concentration in acetone of 250 to 8000 ppm by weight. The above process is capable of producing bisphenol A at high conversion and selectivity by suppressing deterioration of catalytic activity due to methanol as an impurity in acetone.

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