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1. 发明申请

US20110065913A1 PROCESS FOR PRODUCING LAUROLACTAM 有权
标题翻译：生产乳酸菌的方法
公开(公告)号：US20110065913A1
公开(公告)日：2011-03-17
申请号：US12993451
申请日：2009-05-19
申请人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
发明人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention relates to a process for producing laurolactam from cyclododecanone oxime by liquid-phase rearrangement reaction using trichlorotriazine as a rearrangement catalyst. The present invention can provide a process which can solve the problem of termination of the reaction at a certain conversion, can prevent an inactive precipitate generated from trichlorotriazine from precipitating in the course of the reaction process, and can remove an inactive precipitate, an active intermediate and a residual catalyst.
摘要翻译：本发明涉及使用三氯三嗪作为重排催化剂通过液相重排反应从环十二酮肟生产十二内酰胺的方法。本发明可以提供能够解决在一定转化时终止反应的问题的方法，可以防止三氯三嗪在反应过程中产生的不活泼的沉淀物沉淀，并且可以除去无活性的沉淀物，活性中间体和残留催化剂。

2. 发明授权

US06649757B2 Process for producing laurolactam from cyclododecanone 有权
标题翻译：从环十二酮生产十二内酰胺的方法
公开(公告)号：US06649757B2
公开(公告)日：2003-11-18
申请号：US10345548
申请日：2003-01-16
申请人： Nobuyuki Kuroda , Joji Kawai , Hideo Shimomura
发明人： Nobuyuki Kuroda , Joji Kawai , Hideo Shimomura
IPC分类号： C07D22502
CPC分类号： C07D201/06 , C07D201/04
摘要： Laurolactam having high quality is produced by reacting cyclododecanone with a hydroxylamine salt of a mineral acid, and converting the resultant cyclododecanoneoxime to laurolactam through the Beckmann rearrangement reaction, wherein a content of each of oxygen atom-containing C12 organic compounds, for example, cyclododecenone or epoxycyclododecane, and cycloaliphatic unsaturated C12 hydrocarbon compounds, contained, as an impurity, in the staring cyclododecanone material, is controlled to 1,000 ppm or less.
摘要翻译：通过使环十二酮与无机酸的羟胺盐反应，通过贝克曼重排反应将所得的环十二烷酮肟转化为十二内酰胺，生成具有高品质的月桂内酰胺，其中各含氧原子的C12有机化合物，例如环十二酮或环氧环十二烷和环脂肪族不饱和C12烃化合物被控制在1000ppm以下，作为杂质，在起始环十二烷酮材料中。

3. 发明授权

US4697397A Trussed girder, roof framing using the trussed girder and method of constructing the roof framing of a building using the trussed girder 失效
标题翻译：桁架梁，采用桁梁的屋顶框架及使用桁架梁构筑建筑物屋顶框架的方法
公开(公告)号：US4697397A
公开(公告)日：1987-10-06
申请号：US893625
申请日：1986-08-06
申请人： Shuji Okuda , Hideo Shimomura , Kusuo Honda , Masato Kawaguchi , Yasuo Kuno , Takenori Kumagai , Nobuo Kato
发明人： Shuji Okuda , Hideo Shimomura , Kusuo Honda , Masato Kawaguchi , Yasuo Kuno , Takenori Kumagai , Nobuo Kato
IPC分类号： E04B7/00 , E04C3/04 , E04C3/08 , E04C3/10 , E04B1/24
CPC分类号： E04B7/00 , E04C3/08 , E04C3/10 , E04C2003/0486 , E04C2003/0491
摘要： Trussed girder, roof framing using the trussed girder and method of constructing the roof framing of a building using the trussed girder. In the trussed girder, an upper chord and a lower chord are jointed through lattice members. The trussed girder includes: a prestressing steel member; and an attaching mechanism for attaching the prestressing steel member to at least one of both the upper and lower chords to longitudinally extend under tension for providing prestress to the trussed girder.
摘要翻译：使用桁架梁的桁架梁，屋顶框架和使用桁架梁构建建筑物屋顶框架的方法。在桁架梁中，上弦和下弦通过格子构件连接起来。桁架梁包括：预应力钢构件; 以及用于将预应力钢构件附接到上和下两个弦中的至少一个的附接机构，以在张力下纵向延伸以向桁架梁提供预应力。

4. 发明授权

US08309714B2 Process for producing laurolactam 有权
标题翻译：生产月桂内酰胺的方法
公开(公告)号：US08309714B2
公开(公告)日：2012-11-13
申请号：US12744675
申请日：2008-11-19
申请人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro Ii
发明人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro Ii
IPC分类号： C07D201/04 , C07D225/02
CPC分类号： C07D201/04 , C07D225/02 , Y02P20/582
摘要： Provided is a process for efficiently producing laurolactam by simple steps from cyclododecanone and hydroxylamine. This production process comprises the steps of: (a) reacting cyclododecanone with hydroxylamine in an aqueous solution in the presence of an oxime-formation solvent to produce cyclododecanone oxime; (b) separating the reaction mixture obtained after the oxime-forming step into an oil and an aqueous phases and collecting a solution of cyclododecanone oxime of the oil phase; (c) removing a part or all of the oxime-formation solvent and dissolved water from the solution of cyclododecanone oxime which is collected as an oil phase in the oil/aqueous phase separation step, whereby preparing a solution containing a rearrangement solvent to be used in a rearrangement reaction in a later step and the cyclododecanone oxime; (d) producing laurolactam from cyclododecanone oxime by rearrangement reaction using an aromatic-ring containing compound as a rearrangement catalyst; and (e) separating and removing the rearrangement solvent and the rearrangement catalyst from the reaction mixture after the rearrangement step, and purifying the laurolactam.
摘要翻译：提供一种通过简单的步骤从环十二酮和羟胺有效地生产十二内酰胺的方法。该制备方法包括以下步骤：（a）在肟形成溶剂存在下，使环十二酮与羟胺在水溶液中反应，生成环十二烷酮肟; （b）将在肟形成步骤后获得的反应混合物分离成油相和水相，并收集油相的环十二烷酮肟溶液; （c）从油/水相分离步骤中以油相收集的环十二烷酮肟溶液中除去部分或全部肟形成溶剂和溶解的水，由此制备含有使用的重排溶剂的溶液在后续步骤中的重排反应和环十二酮肟; （d）使用含芳环的化合物作为重排催化剂，通过重排反应从环十二酮肟生产月桂内酰胺; 和（e）在重排步骤之后从反应混合物中分离和除去重排溶剂和重排催化剂，并纯化月桂内酰胺。

5. 发明授权

US08624021B2 Compound and process for producing amide compound therewith 有权
标题翻译：用于生产酰胺化合物的化合物和方法
公开(公告)号：US08624021B2
公开(公告)日：2014-01-07
申请号：US13497687
申请日：2010-09-24
申请人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
发明人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
IPC分类号： C07D225/02 , C07D201/04
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention provides novel cyclododecanone-O-azacyclotridecen-2-yloxime and cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride. The invention also provides a process for producing an amide compound wherein cyclododecanone-O-azacyclotridecen-2-yloxime, hydrogen chloride and/or Lewis acid or cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride are used as a rearrangement catalyst and/or a reaction starting material in a reaction step.
摘要翻译：本发明提供了新的环十二烷酮-O-氮杂环十二烯-2-基肟和环十二酮-O-氮杂环十二烯-2-基肟酸盐酸盐。本发明还提供一种制备酰胺化合物的方法，其中使用环十二酮-O-氮杂环十二碳-2-肟，氯化氢和/或路易斯酸或环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐作为重排催化剂和/或反应步骤中的反应原料。

6. 发明申请

US20130005961A1 NOVEL COMPOUND AND PROCESS FOR PRODUCING AMIDE COMPOUND THEREWITH 有权
标题翻译：新型化合物及其生产方法
公开(公告)号：US20130005961A1
公开(公告)日：2013-01-03
申请号：US13497687
申请日：2010-09-24
申请人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
发明人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention provides novel cyclododecanone-O-azacyclotridecen-2-yloxime and cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride. The invention also provides a process for producing an amide compound wherein cyclododecanone-O-azacyclotridecen-2-yloxime, hydrogen chloride and/or Lewis acid or cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride are used as a rearrangement catalyst and/or a reaction starting material in a reaction step.
摘要翻译：本发明提供新的环十二烷酮-O-氮杂环十二烷-2-基肟和环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐。本发明还提供一种制备酰胺化合物的方法，其中使用环十二酮-O-氮杂环十二碳-2-肟，氯化氢和/或路易斯酸或环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐作为重排催化剂和/或反应步骤中的反应原料。

7. 发明授权

US08338589B2 Process for producing laurolactam 有权
标题翻译：生产月桂内酰胺的方法
公开(公告)号：US08338589B2
公开(公告)日：2012-12-25
申请号：US12993451
申请日：2009-05-19
申请人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
发明人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
IPC分类号： C07D201/04 , C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention relates to a process for producing laurolactam from cyclododecanone oxime by liquid-phase rearrangement reaction using trichlorotriazine as a rearrangement catalyst. The present invention can provide a process which can solve the problem of termination of the reaction at a certain conversion, can prevent an inactive precipitate generated from trichlorotriazine from precipitating in the course of the reaction process, and can remove an inactive precipitate, an active intermediate and a residual catalyst.
摘要翻译：本发明涉及使用三氯三嗪作为重排催化剂通过液相重排反应从环十二酮肟生产十二内酰胺的方法。本发明可以提供能够解决在一定转化时终止反应的问题的方法，可以防止三氯三嗪在反应过程中产生的不活泼的沉淀物沉淀，并且可以除去无活性的沉淀物，活性中间体和残留催化剂。

8. 发明申请

US20100267944A1 PROCESS FOR PRODUCING LAUROLACTAM 有权
标题翻译：生产乳酸菌的方法
公开(公告)号：US20100267944A1
公开(公告)日：2010-10-21
申请号：US12744675
申请日：2008-11-19
申请人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro II
发明人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro II
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02 , Y02P20/582
摘要： Provided is a process for efficiently producing laurolactam by simple steps from cyclododecanone and hydroxylamine. This production process comprises the steps of: (a) reacting cyclododecanone with hydroxylamine in an aqueous solution in the presence of an oxime-formation solvent to produce cyclododecanone oxime; (b) separating the reaction mixture obtained after the oxime-forming step into an oil and an aqueous phases and collecting a solution of cyclododecanone oxime of the oil phase; (c) removing a part or all of the oxime-formation solvent and dissolved water from the solution of cyclododecanone oxime which is collected as an oil phase in the oil/aqueous phase separation step, whereby preparing a solution containing a rearrangement solvent to be used in a rearrangement reaction in a later step and the cyclododecanone oxime; (d) producing laurolactam from cyclododecanone oxime by rearrangement reaction using an aromatic-ring containing compound as a rearrangement catalyst; and (e) separating and removing the rearrangement solvent and the rearrangement catalyst from the reaction mixture after the rearrangement step, and purifying the laurolactam.
摘要翻译：提供一种通过简单的步骤从环十二酮和羟胺有效地生产十二内酰胺的方法。该制备方法包括以下步骤：（a）在肟形成溶剂存在下，使环十二酮与羟胺在水溶液中反应，生成环十二酮肟; （b）将在肟形成步骤后获得的反应混合物分离成油相和水相，并收集油相的环十二烷酮肟溶液; （c）从油/水相分离步骤中以油相收集的环十二酮肟溶液中除去部分或全部肟形成溶剂和溶解的水，由此制备含有使用的重排溶剂的溶液在后续步骤中的重排反应和环十二酮肟; （d）使用含芳环的化合物作为重排催化剂，通过重排反应从环十二酮肟生产月桂内酰胺; 和（e）在重排步骤之后从反应混合物中分离和除去重排溶剂和重排催化剂，并纯化月桂内酰胺。

9. 发明授权

US6043383A Process for producing 1,2-epoxy-5,9-cyclododecadiene 有权
标题翻译： 1,2-环氧-5,9-环十二烯的生产方法
公开(公告)号：US6043383A
公开(公告)日：2000-03-28
申请号：US290500
申请日：1999-04-12
申请人： Nobuyuki Kuroda , Mitsuo Yamanaka , Osamu Yamazaki , Hirofumi Takemoto , Kohei Ninomiya , Junichi Kugimoto , Koji Kaiso , Hideo Shimomura
发明人： Nobuyuki Kuroda , Mitsuo Yamanaka , Osamu Yamazaki , Hirofumi Takemoto , Kohei Ninomiya , Junichi Kugimoto , Koji Kaiso , Hideo Shimomura
IPC分类号： C07D303/04 , C07D303/06 , C07D301/12 , C07D301/16
CPC分类号： C07D303/04
摘要： 1,2-epoxy-5,9-cyclododecadiene is produced with a high selectivity thereto by epoxidizing 1,5,9-cyclododecatriene in a continuous multi-stage oxidation apparatus having a plurality of reactors connected to each other in series in such a manner that (1) in a first reactor, 1,5,9-cyclododecatriene, hydrogen peroxide, catalyst components and optionally a mineral acid are subjected to an epoxidation reaction; (2) the resultant reaction mixture delivered from the first reactor is passed through one or more succeeding reactors to further epoxidize the non-reacted 1,5,9-cyclododecatriene with the non-reacted hydrogen peroxide; and (3) the final reaction mixture produced in a rearend reactor is delivered from the oxidation apparatus, and optionally subjected to an isolation-refining procedure wherein the target 1,2-epoxy-5,9-cyclododecadiene is refined and collected and the non-reacted 1,5,9-cyclododecatriene is recovered and recycled to the epoxidation procedure.
摘要翻译：通过在连续的多级氧化装置中环氧化1,5,9-环十二碳三烯以高选择性制备1,2-环氧-5,9-环十二烯，其中多个反应器以这种方式相互串联连接（1）在第一反应器，1,5,9-环十二碳三烯，过氧化氢，催化剂组分和任选的无机酸中进行环氧化反应; （2）将从第一反应器输送的所得反应混合物通过一个或多个后续反应器，以用未反应的过氧化氢进一步环氧化未反应的1,5,9-环十二碳三烯; 和（3）在再循环反应器中产生的最终反应混合物从氧化装置输送，并任选地进行分离精制程序，其中精制和收集目标1,2-环氧-5,9-环十二烷二烯， - 回收的1,5,9-环十二碳三烯被回收并再循环至环氧化方法。

10. 发明授权

US5775625A Cover strip for facilitating pay off of line from a spool 失效
标题翻译：盖条，便于从线轴上取下线
公开(公告)号：US5775625A
公开(公告)日：1998-07-07
申请号：US798776
申请日：1997-02-11
申请人： Hideo Shimomura
发明人： Hideo Shimomura
IPC分类号： B65H49/20 , B65H57/18 , B65H75/14 , B65H75/26 , B65H59/02 , B65H49/00 , B65H75/28
CPC分类号： B65H75/285 , B65H49/205 , B65H57/18 , B65H75/141
摘要： The combination of a spool having a core with a central axis, a supply of flexible line with a plurality of turns wrapped over the core around the central axis, and a control strip having a body which in an operative state on the core extends around the core over the supply of flexible line to prevent the flexible line from inadvertently unwrapping. The core is movable relative to the control strip around the central axis. A gripping portion on the control strip is graspable to hold the control strip substantially stationary while rotating the core around the core axis. An opening is provided through the control strip, with the flexible line extending from one of the turns of the flexible line through the control strip opening to a useable portion of the flexible line that projects outwardly from the control strip. The control strip opening is located so that with the user simultaneously grasping the gripping portion of the control strip and the useable portion of the flexible line and exerting oppositely directed forces thereon in a first line, the useable portion of the flexible line projects from the one turn in a second line that is substantially tangent to the one turn and parallel to the first line.
摘要翻译：具有芯部与中心轴线的卷轴的组合，围绕中心轴线缠绕在芯上的多个匝的柔性线的供应以及在芯上处于操作状态的主体的控制条围绕芯线供应柔性线，防止弹性线无意中展开。芯可绕中心轴线相对于控制条移动。控制条上的抓握部分是可握住的，以在使芯部绕芯轴线旋转的同时将控制条基本上固定。通过控制带提供开口，柔性线从柔性线的匝之一通过控制条开口延伸到从控制带向外突出的柔性线的可用部分。控制带开口定位成使得用户同时抓住控制带的夹持部分和柔性线的可用部分并且在第一线上施加相反的力，柔性线的可用部分从一个转动基本上与一匝相切并且平行于第一条线的第二条线。

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