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1. 发明授权

US4349526A Process for the production of hydrogen peroxide 失效
标题翻译：过氧化氢生产工艺
公开(公告)号：US4349526A
公开(公告)日：1982-09-14
申请号：US283194
申请日：1981-07-14
申请人： Gustaaf Goor , Wolfgang Kunkel
发明人： Gustaaf Goor , Wolfgang Kunkel
IPC分类号： C01B15/023 , C07C67/00 , C07C239/00 , C07C275/28 , C01B15/02
CPC分类号： C01B15/023
摘要： Tetra substituted ureas wherein at least one substituent is an aryl group have proven very oxidation resistant in the anthraquinone process for making hydrogen peroxide. The urea nitrogen is directly attached to the aryl group. These ureas can be used as a single solvent or as a component of a mixture of solvents.
摘要翻译：其中至少一个取代基是芳基的四取代脲已被证明在用于制备过氧化氢的蒽醌方法中非常耐氧化。尿素氮直接连接到芳基上。这些脲可用作单一溶剂或作为溶剂混合物的组分。

2. 发明授权

US6106803A Granulates which contain titanium silicalite-1 失效
标题翻译：含钛硅沸石-1的颗粒
公开(公告)号：US6106803A
公开(公告)日：2000-08-22
申请号：US121309
申请日：1998-07-23
申请人： Steffen Hasenzahl , Georg Markowz , Mathias Viandt , Eckehart E. Roland , Georg Thiele , Gustaaf Goor , Alexander Moller
发明人： Steffen Hasenzahl , Georg Markowz , Mathias Viandt , Eckehart E. Roland , Georg Thiele , Gustaaf Goor , Alexander Moller
IPC分类号： B01J29/89 , B01J37/00 , C01B37/00 , C01B34/08 , B01J29/40 , C01B39/36 , C07D301/12 , B01J29/30
CPC分类号： B01J37/0045 , B01J29/89 , C01B37/005 , Y10S423/22
摘要： Granulates which contain titanium silicalite-1 are composed of silicon dioxide, titanium dioxide and titanium silicalite-1 crystals. The granulates can be prepared by spray-drying or spray granulating the crystallization suspension. The granulates may be used as suspension catalysts, such as for the epoxidation of olefins using hydrogen peroxide.
摘要翻译：含钛硅沸石-1的颗粒由二氧化硅，二氧化钛和钛硅沸石-1晶体组成。颗粒可以通过喷雾干燥或喷雾造粒结晶悬浮液来制备。颗粒可以用作悬浮催化剂，例如用于使用过氧化氢的烯烃的环氧化。

3. 发明授权

US5534149A Method of separating catalyst-free working solution from the hydrogenation cycle of the anthraquinone method for the production of hydrogen peroxide 失效
标题翻译：从催化剂工作溶液中分离用于生产过氧化氢的蒽醌方法的氢化循环的方法
公开(公告)号：US5534149A
公开(公告)日：1996-07-09
申请号：US406519
申请日：1995-03-20
申请人： Hans Birkenbeil , Ulrich Brand , Gustaaf Goor , Wolfgang Kunkel
发明人： Hans Birkenbeil , Ulrich Brand , Gustaaf Goor , Wolfgang Kunkel
IPC分类号： B01D71/02 , B01D61/14 , B01J19/24 , B01J23/44 , B01J23/96 , B01J37/00 , B01J38/00 , C01B15/023 , B01D61/00 , C02F1/44
CPC分类号： B01D61/147 , B01J19/243 , B01J23/96 , B01J37/009 , C01B15/023 , Y02P20/584
摘要： A method is shown for the separation of catalyst-free working solution from working solution, containing noble-metal black, especially palladium black as catalyst, of the hydrogenation cycle of the so-called anthraquinone method for the production of hydrogen peroxide by filtration of the catalyst-containing working solution using filter candles. The filter candles are formed of an open-pore support body based on a carbon material or metallic or ceramic material with an average pore width in a range of 5 to 100 .mu.m and of a single-layer or multi-layer membrane of ceramic material with an average pore width in a range of at least about 1 up to 10 .mu.m located on the outside surface of the support body.
摘要翻译：示出了用于将不含催化剂的工作溶液从包含贵金属黑，特别是钯黑作为催化剂的工作溶液中分离出用于通过过滤生成过氧化氢的所谓的蒽醌方法的氢化循环的方法含有催化剂的工作液使用过滤蜡烛。过滤蜡烛由基于碳材料或平均孔宽在5至100μm范围内的金属或陶瓷材料的开孔支撑体和陶瓷材料的单层或多层膜形成其平均孔宽在位于支撑体的外表面上的至少约1至10μm的范围内。

4. 发明授权

US5286885A Process for preparing glycide by epoxidation using polymeric organosiloxane ammonium salts of oxoacids of the elements V, Nb, Ta, Mo, and W 失效
标题翻译：使用元素V，Nb，Ta，Mo和W的含氧酸的聚合有机硅氧烷铵盐通过环氧化制备糖苷的方法
公开(公告)号：US5286885A
公开(公告)日：1994-02-15
申请号：US53248
申请日：1993-04-28
申请人： Peter Goetz , Stefan Wieland , Peter Panster , Gustaaf Goor , Rainer Siegmeier
发明人： Peter Goetz , Stefan Wieland , Peter Panster , Gustaaf Goor , Rainer Siegmeier
IPC分类号： C08G77/54 , C08G77/58 , C07D301/12 , C07D303/14
CPC分类号： C08G77/54 , C08G77/58
摘要： The invention relates to polymeric organosiloxane ammonium salts having a silica-like skeleton and including units of Formula (I): ##STR1## wherein R.sup.1 and R.sup.2 are identical or different and signify a group of Formula (II): ##STR2## wherein R.sup.5 is an alkylene group and the oxygen atoms are saturated by silicon atoms of additional groups corresponding to Formula (II), optionally with the insertion of cross-linking agents; R.sup.3 represents groups corresponding to R.sup.1 or R.sup.2, or hydrogen or an alkyl group; R.sup.4 represents hydrogen or an alkyl group; x is the charge number of an oxo anion of a monooxo-, isopolyoxo- or heteropolyoxo acid of the elements vanadium, niobium, tantalum, molybdenum or tungsten; and oxo groups of the X anion also may be replaced by peroxo groups. The invention also includes methods of preparing the salts of Formula (I) from salts of the type (R.sup.1 R.sup.2 R.sup.3 R.sup.4 N.sup.+).sub.y Y wherein Y is different from X. The invention further includes the use of the salts of Formula (I) as catalyst for oxidation reactions using peroxo compounds as an oxidation agent.
摘要翻译：本发明涉及具有二氧化硅样骨架并包括式（I）的单元的聚合有机硅氧烷铵盐：（*化学结构*）（I）其中R1和R2相同或不同并且表示式（II）的基团：（*化学结构*）（II）其中R5是亚烷基并且氧原子被对应于式（II）的另外的基团的硅原子饱和，任选地插入交联剂; R3表示对应于R1或R2的基团，或氢或烷基; R4表示氢或烷基; x是元素钒，铌，钽，钼或钨元素的单氧，异羟基或杂多酸的氧阴离子的电荷数; X阴离子的氧基也可以被过氧基取代。本发明还包括从其中Y不同于X的类型（R 1 R 2 R 3 R 4 N +）y Y的盐制备式（I）的盐的方法。本发明还包括使用式（I）的盐作为氧化反应的催化剂，其使用过氧化合物作为氧化剂。

5. 发明授权

US4759921A Method of preparing hydrogen peroxide 失效
标题翻译：制备过氧化氢的方法
公开(公告)号：US4759921A
公开(公告)日：1988-07-26
申请号：US103215
申请日：1987-10-01
申请人： Wolfgang Kunkel , Gustaaf Goor , Jorg Kemnade
发明人： Wolfgang Kunkel , Gustaaf Goor , Jorg Kemnade
IPC分类号： C01B15/013 , C01B15/023 , C01B15/02
CPC分类号： C01B15/013 , C01B15/023
摘要： An aqueous hydrogen peroxide extract which contains small amounts of dispersed working solution and a working solution which contains small amounts of dispersed aqueous hydrogen peroxide are collected in the extraction stage of the anthraquinone method for preparing hydrogen peroxide. In order to purify these solutions, the working solution is compounded with aqueous hydrogen peroxide or preferably with water and the hydrogen peroxide extract is compounded with an organic dissolving mixture, preferably a quinone dissolver, and the respective dispersed phase is separated out with the aid of coalescers in a separator unit. It is especially preferable to add 1-3% by volume water or 1-3% quinone dissolver before the coalescer stages and to use coalescers with a drop-enlarging design and filter layers consisting of thermally desized glass filament yarn.The after-purification in accordance with the method results in a hydrogen peroxide which is improved as regards carbon content and color index as well as in an increase in yield of hydrogen peroxide and in a working solution with constant rel. moisture.
摘要翻译：在用于制备过氧化氢的蒽醌方法的萃取阶段中收集含有少量分散的工作溶液和含有少量分散的过氧化氢水的工作溶液的过氧化氢水提取物。为了纯化这些溶液，将工作溶液与过氧化氢水溶液或优选与水混合，并将过氧化氢提取物与有机溶解混合物（优选醌溶解器）混合，并将相应的分散相借助于分离器单元中的聚结器。特别优选在聚结器阶段之前加入1-3体积％水或1-3％醌溶解剂，并使用滴加扩大设计的聚结器和由热退浆玻璃丝线组成的过滤层。根据该方法的后净化产生了关于碳含量和颜色指数以及过氧化氢产率的增加和具有恒定相关性的工作溶液中改善的过氧化氢。湿气。

6. 发明授权

US07238335B2 Process for the preparation of hydrogen peroxide by the anthraquinone cyclic process 失效
标题翻译：通过蒽醌循环法制备过氧化氢的方法
公开(公告)号：US07238335B2
公开(公告)日：2007-07-03
申请号：US10912757
申请日：2004-08-06
申请人： Gustaaf Goor , Eugen Staab , Jürgen Glenneberg
发明人： Gustaaf Goor , Eugen Staab , Jürgen Glenneberg
IPC分类号： C01B15/023
CPC分类号： C01B15/023
摘要： The invention concerns a process for the preparation of hydrogen peroxide by the anthraquinone cyclic process. The process includes a regeneration stage in which working solution is regenerated by being brought into contact with an aqueous solution containing an alkyl anthrahydroquinone and/or an alkyl tetrahydroanthrahydroquinone in deprotonated form. The working solution regenerated in the regeneration stage is returned to the cyclic process.
摘要翻译：本发明涉及一种通过蒽醌循环法制备过氧化氢的方法。该方法包括再生阶段，其中工作溶液通过与含有去质子化形式的含有烷基蒽氢醌和/或烷基四氢蒽氢醌的水溶液接触而再生。在再生阶段再生的工作溶液返回循环过程。

7. 发明申请

US20050069483A1 Process for the preparation of hydrogen peroxide by the anthraquinone cyclic process 失效
标题翻译：通过蒽醌循环法制备过氧化氢的方法
公开(公告)号：US20050069483A1
公开(公告)日：2005-03-31
申请号：US10912757
申请日：2004-08-06
申请人： Gustaaf Goor , Eugen Staab , Jurgen Glenneberg
发明人： Gustaaf Goor , Eugen Staab , Jurgen Glenneberg
IPC分类号： C01B15/023
CPC分类号： C01B15/023
摘要： The invention concerns a process for the preparation of hydrogen peroxide by the anthraquinone cyclic process. The process includes a regeneration stage in which working solution is regenerated by being brought into contact with an aqueous solution containing an alkyl anthrahydroquinone and/or an alkyl tetrahydroanthrahydroquinone in deprotonated form. The working solution regenerated in the regeneration stage is returned to the cyclic process.
摘要翻译：本发明涉及一种通过蒽醌循环法制备过氧化氢的方法。该方法包括再生阶段，其中工作溶液通过与含有去质子化形式的含有烷基蒽氢醌和/或烷基四氢蒽氢醌的水溶液接触而再生。在再生阶段再生的工作溶液返回循环过程。

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