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1. 发明授权

US5071809A Tertiary amine catalysts for polyurethanes 失效
标题翻译：用于聚氨酯的仲胺催化剂
公开(公告)号：US5071809A
公开(公告)日：1991-12-10
申请号：US519711
申请日：1990-05-07
申请人： Jeremiah P. Casey , Richard V. C. Carr , George J. Wasilczyk , Robert G. Petrella
发明人： Jeremiah P. Casey , Richard V. C. Carr , George J. Wasilczyk , Robert G. Petrella
IPC分类号： C07C217/08 , C07D295/088 , C08G18/18 , C08G18/20
CPC分类号： C07D295/088 , C07C217/08 , C08G18/1825 , C08G18/1833 , C08G18/2009
摘要： The invention pertains to tertiary amines used as catalysts for the preparation of polyurethane foams prepared via the catalytic reaction of a polyisocyanate with a polyol in the presence of blowing agents, etc. The tertiary amine catalysts are prepared by reacting an olefinic nitrile with aliphatic polyol having at least secondary hydroxyl functionality in a ratio less than stoichiometric for providing cyanoalkylated polyol having residual hydroxyl functionality. The resulting cyanoalkylated polyol then is reacted with a secondary amine under conditions for effective reductive alkylation.The tertiary amine catalysts, because of residual secondary hydroxyl functionality, provide for uniform dispersion within a polyurethane formulation; they provide for additional or extended pot life in polyurethane formulations at temperatures below reaction condition, and they are bound by reaction on cure.

2. 发明授权

US4067831A Process for the preparation of polyurethane foams 失效
标题翻译：制备聚氨酯泡沫的方法
公开(公告)号：US4067831A
公开(公告)日：1978-01-10
申请号：US581174
申请日：1975-05-27
申请人： George J. Wasilczyk
发明人： George J. Wasilczyk
IPC分类号： C08G18/20 , C08G18/24 , C08J9/00
CPC分类号： C08J9/0066 , C08G18/2027 , C08G18/242 , C08K3/0033 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083 , C08J2375/04
摘要： An improved process for the preparation of flexible polyurethane foams which comprise conducting the foaming in the presence of a delayed action catalyst and an inorganic filler having a pH 5 to 10, preferably 6 to 8, and an average particle size of 2-30 microns, preferably 5-15 microns. The process is suitable for slabstock and molded foams.
摘要翻译：用于制备柔性聚氨酯泡沫的改进方法，其包括在延迟作用催化剂和pH5至10，优选6至8，平均粒度为2-30微米的存在下进行发泡，优选5-15微米。该方法适用于块料和模塑泡沫。

3. 发明授权

US5091583A Tertiary amine catalysts for polurethanes 失效
标题翻译：聚氨酯的叔胺催化剂
公开(公告)号：US5091583A
公开(公告)日：1992-02-25
申请号：US697859
申请日：1991-05-09
申请人： Jeremiah P. Casey , Richard V. C. Carr , George J. Wasilczyk , Robert G. Petrella
发明人： Jeremiah P. Casey , Richard V. C. Carr , George J. Wasilczyk , Robert G. Petrella
IPC分类号： C07C217/08 , C07D295/088 , C08G18/18 , C08G18/20
CPC分类号： C07D295/088 , C07C217/08 , C08G18/1825 , C08G18/1833 , C08G18/2009
摘要： The invention pertains to tertiary amines used as catalysts for the preparation of polyurethane foams prepared via the catalytic reaction of a polyisocyanate with a polyol in the presence of blowing agents, etc. The tertiary amine catalysts are prepared by reacting an olefinic nitrile with aliphatic polyol having at least secondary hydroxyl functionality in a ratio less than stoichiometric for providing cyanoalkylated polyol having residual hydroxyl functionality. The resulting cyanoalkylated polyol then is reacted with a secondary amine under conditions for effective reductive alkylation.The tertiary amine catalysts, because of residual secondary hydroxyl functionality, provide for uniform dispersion within a polyurethane, formulation; they provude for additional or extended pot life in polyurethane formulations at temperature below reaction condition, and they are bound by reaction on cure.
摘要翻译：本发明涉及用于制备通过多异氰酸酯与多元醇在发泡剂等的催化反应制备的聚氨酯泡沫的催化剂的叔胺。叔胺催化剂是通过烯烃腈与具有至少具有小于化学计量比的仲羟基官能团以提供具有残余羟基官能团的氰基烷基化多元醇。然后将所得的氰基烷基化多元醇与仲胺在有效还原烷基化的条件下反应。由于残留的仲羟基官能团，叔胺催化剂在聚氨酯，配方中均匀分散; 它们在低于反应条件的温度下在聚氨酯配方中增加或延长适用期，并且它们通过固化反应而结合。

4. 发明授权

US5028366A Water based mold release compositions for making molded polyurethane foam 失效
标题翻译：用于制造模塑聚氨酯泡沫的水基脱模组合物
公开(公告)号：US5028366A
公开(公告)日：1991-07-02
申请号：US142970
申请日：1988-01-12
申请人： Mark E. Harakal , George J. Wasilczyk , Gary D. Andrew , Zdizslaw Makus , Michael Scarpati
发明人： Mark E. Harakal , George J. Wasilczyk , Gary D. Andrew , Zdizslaw Makus , Michael Scarpati
IPC分类号： B29C33/60
CPC分类号： B29C33/60
摘要： A method for preparing a polyurethane foam article in a mold by applying to a mold surface a water-based mold release composition which includes a release effective system which is in a solid (hardened) state at the mold pour temperature and a liquid state at the demold temperature, pouring a polyurethane foam composition into the mold, curing the foam composition and demolding the foam article. The use of such release effective system in the aqueous mold release composition provides for a reduction in surface defects of the polyurethane foam article.Also disclosed is the incorporation of a poly(siloxane-glycol) surfactant having a cloud point ranging from 25.degree.-50.degree. C. into a water-based mold release composition including an aqueous emulsion or dispersion of at least one release effective substance and desirably at least one emulsifying agent provides for improved surface quality of the foam product.
摘要翻译：一种通过向模具表面施加水性脱模组合物来制备聚氨酯泡沫塑料制品的方法，所述水性脱模组合物包括在模具浇注温度处于固体（硬化）状态的释放有效系统和在脱模温度，将聚氨酯泡沫组合物倒入模具中，固化泡沫组合物并脱模泡沫制品。在水性脱模组合物中使用这种释放有效系统提供了聚氨酯泡沫制品的表面缺陷的减少。还公开了将具有25℃-50℃的浊点的聚（硅氧烷 - 二醇）表面活性剂掺入包含至少一种释放有效物质的水性乳液或分散体的水性脱模组合物中，至少一种乳化剂提供改善泡沫产品的表面质量。

5. 发明授权

US4936917A Water based mold release compositions containing poly(siloxane-glycol) surfactants for making polyurethane foam article in a mold 失效
标题翻译：含有用于在模具中制备聚氨酯泡沫制品的聚（硅氧烷 - 二醇）表面活性剂的水基脱模组合物
公开(公告)号：US4936917A
公开(公告)日：1990-06-26
申请号：US142971
申请日：1988-01-12
申请人： Mark E. Harakal , George J. Wasilczyk , Gary D. Andrew , Zdzislaw Makus , Michael Scarpati
发明人： Mark E. Harakal , George J. Wasilczyk , Gary D. Andrew , Zdzislaw Makus , Michael Scarpati
IPC分类号： B29C33/62 , B29C33/64 , B29K75/00 , B29K105/04 , C08L83/04
CPC分类号： B29C33/64 , Y10S516/01
摘要： The incorporation of a poly(siloxane-glycol) surfactant having a cloud point ranging from 25.degree.-50.degree. C. into a water-based mold release composition comprising an aqueous emulsion or dispersion of at least one release effective substance and desirably at least one emulsifying agent provides for improved surface quality of the foam product.Also disclosed is a method for preparing a polyurethane foam article in a mold by applying to a mold surface a water-based mold release composition which comprises a release effective system which is in a solid (hardened) state at the mold pour temperature and a liquid state at the demold temperature, pouring a polyurethane foam composition into the mold, curing the foam composition and demolding the foam article. The use of such release effective system in the aqueous mold release composition provides for a reduction in surface defects of the polyurethane foam article.

6. 发明授权

US4217422A High resiliency polyurethane foams 失效
标题翻译：高弹性聚氨酯泡沫
公开(公告)号：US4217422A
公开(公告)日：1980-08-12
申请号：US890744
申请日：1978-03-27
申请人： George J. Wasilczyk
发明人： George J. Wasilczyk
IPC分类号： C08G18/72 , C08G18/76 , C08J9/00 , C08G18/14
CPC分类号： C08J9/0066 , C08G18/721 , C08G18/7621 , C08J2375/04
摘要： Flexible polyurethane foams are prepared from polyols containing 0.1 to 5.0 percent by weight of an inorganic filler such as fumed silica having a pH value of 6-8.5 and an effective particle size of less than 7 microns. Foams molded from such polyols exhibit in some instances an improvement in some of the strength properties and do not alter substantially, the mold fill time. In addition, there is an improvement in foam porosity (air flow) as well as a reduction in the force required to crush foam articles.
摘要翻译：柔性聚氨酯泡沫由含有0.1至5.0重量％的无机填料的多元醇制备，所述无机填料如pH值为6-8.5，有效粒度小于7微米的热解法二氧化硅。由这种多元醇模塑的泡沫在一些情况下表现出一些强度性能的改进，并且基本上不改变模具填充时间。此外，泡沫孔隙率（气流）的改善以及压碎泡沫制品所需的力的降低。

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