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1. 发明授权

US08206597B2 Protected alloy surfaces in microchannel apparatus and catalysts, alumina supported catalysts, catalyst intermediates, and methods of forming catalysts and microchannel apparatus 有权
标题翻译：微通道设备和催化剂中受保护的合金表面，氧化铝负载催化剂，催化剂中间体以及形成催化剂和微通道设备的方法
公开(公告)号：US08206597B2
公开(公告)日：2012-06-26
申请号：US13012797
申请日：2011-01-24
申请人： Barry L. Yang , Anna Lee Tonkovich , Junko M. Watson , Francis P. Daly , Sean P. Fitzgerald , Chunshe Cao , Xiaohong Li , Terry Mazanec , Bradley R. Johnson , Ravi Arora , David J. Hesse , Dongming Qiu , Rachid Taha , Jeffrey J. Ramler , Yong Wang , Richard Long , Ya-Huei Chin
发明人： Barry L. Yang , Anna Lee Tonkovich , Junko M. Watson , Francis P. Daly , Sean P. Fitzgerald , Chunshe Cao , Xiaohong Li , Terry Mazanec , Bradley R. Johnson , Ravi Arora , David J. Hesse , Dongming Qiu , Rachid Taha , Jeffrey J. Ramler , Yong Wang , Richard Long , Ya-Huei Chin
IPC分类号： B01D37/00 , B01D39/00 , B01J8/00
CPC分类号： C01B3/384 , B01J19/0093 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00869 , B01J2219/00873 , B01J2219/0236 , C01B2203/0233 , C01B2203/0811 , C23C8/10 , C23C16/12 , C23C16/56 , H01M2008/1293 , Y02P20/52 , Y10S585/92 , Y10S585/924
摘要： The invention describes microchannel apparatus and catalysts that contain a layer of a metal aluminide or are made in a process in which a metal aluminide layer is formed as an intermediate. Certain processing conditions have surprisingly been found to result in superior coatings. The invention includes chemical processes conducted through apparatus described in the specification. Other catalysts and catalyst synthesis techniques are also described.
摘要翻译：本发明描述了包含金属铝化物层的微通道装置和催化剂，或者是在其中形成金属铝化物层作为中间体的方法制造的。令人惊奇地发现某些加工条件导致优异的涂层。本发明包括通过本说明书中描述的设备进行的化学过程。还描述了其它催化剂和催化剂合成技术。

2. 发明授权

US07959880B2 Hydrogen peroxide production in microchannel reactors 有权
标题翻译：微通道反应器中的过氧化氢生产
公开(公告)号：US07959880B2
公开(公告)日：2011-06-14
申请号：US12157587
申请日：2008-06-11
申请人： Anna Lee Y. Tonkovich , Bin Yang , William Allen Rogers, Jr. , Paul William Neagle , Sean P. Fitzgerald , Kai Tod Paul Jarosch , Dongming Qiu , David J. Hesse , Micheal Lamont
发明人： Anna Lee Y. Tonkovich , Bin Yang , William Allen Rogers, Jr. , Paul William Neagle , Sean P. Fitzgerald , Kai Tod Paul Jarosch , Dongming Qiu , David J. Hesse , Micheal Lamont
IPC分类号： B01J12/00
CPC分类号： C01B15/029 , B01J19/0093 , B01J2219/00783 , B01J2219/00822 , B01J2219/00826 , B01J2219/00828 , B01J2219/00831 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/00907 , B01J2219/00918 , C01B3/384 , C01B15/01 , C01B15/027
摘要： The present invention includes methods and apparatuses for producing hydrogen peroxide using microchannel technology. An exemplary process for producing hydrogen peroxide comprises flowing feed streams into intimate fluid communication with one another within a process microchannel to form a reactant mixture stream comprising a hydrogen source and an oxygen source such as, without limitation, hydrogen gas and oxygen gas. Thereafter, a catalyst is contacted by the reactant mixture and is operative to convert a majority of the reactant mixture to hydrogen peroxide that is withdrawn via an egressing product stream. During the hydrogen peroxide chemical reaction, exothermic energy is generated and absorbed by the fluid within the microchannel as well as the microchannel itself.
摘要翻译：本发明包括使用微通道技术生产过氧化氢的方法和装置。用于生产过氧化氢的示例性方法包括使进料流在工艺微通道内相互流体连通，以形成包含氢源和氧源（例如但不限于氢气和氧气）的反应物混合物流。此后，催化剂被反应物混合物接触并且可操作地将大部分反应物混合物转化成通过出口产物流排出的过氧化氢。在过氧化氢化学反应期间，放热能由微通道内的流体以及微通道本身产生和吸收。

3. 发明授权

US07931875B2 Integrated combustion reactors and methods of conducting simultaneous endothermic and exothermic reactions 有权
标题翻译：综合燃烧反应器和进行同时吸热和放热反应的方法
公开(公告)号：US07931875B2
公开(公告)日：2011-04-26
申请号：US11825286
申请日：2007-07-03
申请人： Anna Lee Tonkovich , Gary Roberts , Sean P. Fitzgerald , Paul W. Neagle , Dongming Qiu , Matthew B. Schmidt , Steven T. Perry , David J. Hesse , Robert J. Luzenski , G. Bradley Chadwell , Ying Peng , James A. Mathias , Nathan P. Gano , Ravi Arora , Barry L. Yang , David J. Kuhlmann , Thomas D. Yuschak , John Arthur Monahan
发明人： Anna Lee Tonkovich , Gary Roberts , Sean P. Fitzgerald , Paul W. Neagle , Dongming Qiu , Matthew B. Schmidt , Steven T. Perry , David J. Hesse , Robert J. Luzenski , G. Bradley Chadwell , Ying Peng , James A. Mathias , Nathan P. Gano , Ravi Arora , Barry L. Yang , David J. Kuhlmann , Thomas D. Yuschak , John Arthur Monahan
IPC分类号： B01J35/02 , B01J15/00 , B01J16/00 , B01J19/00
CPC分类号： F23C13/00 , B01J19/0093 , B01J2219/00117 , B01J2219/00164 , B01J2219/00783 , B01J2219/0081 , B01J2219/00835 , B01J2219/00873 , B01J2219/00984 , C01B3/382 , C01B3/384 , C01B2203/0233 , C01B2203/0811 , C01B2203/0822 , C01B2203/142 , F23C99/006 , F23C2900/03001 , F23C2900/03002 , F28D9/0093 , F28F2260/02 , Y02P20/128 , Y02P20/52 , Y10T156/10
摘要： Integrated Combustion Reactors (ICRs) and methods of making ICRs are described in which combustion chambers (or channels) are in direct thermal contact to reaction chambers for an endothermic reaction. Particular reactor designs are also described. Processes of conducting reactions in integrated combustion reactors are described and results presented. Some of these processes are characterized by unexpected and superior results, and/or results that can not be achieved with any prior art devices.
摘要翻译：描述了集成燃烧反应器（ICR）和制造ICR的方法，其中燃烧室（或通道）与用于吸热反应的反应室直接热接触。还描述了特定的反应器设计。介绍了综合燃烧反应器中进行反应的过程，并提出了结果。这些过程中的一些特征在于意想不到的和优异的结果，和/或不能用任何现有技术装置实现的结果。

4. 发明授权

US07874432B2 Protected alloy surfaces in microchannel apparatus and catalysts, alumina supported catalysts, catalyst intermediates, and methods of forming catalysts and microchannel apparatus 有权
标题翻译：微通道设备和催化剂中受保护的合金表面，氧化铝负载催化剂，催化剂中间体以及形成催化剂和微通道设备的方法
公开(公告)号：US07874432B2
公开(公告)日：2011-01-25
申请号：US11088685
申请日：2005-03-23
申请人： Barry L. Yang , Francis P. Daly , Junko M. Watson , Terry Manzanec , Sean P. Fitzgerald , Bradley R. Johnson , Xiaohong Li , Chunshe Cao , Ya-Huei Chin , Anna Lee Tonkovich , Ravi Arora , David J. Hesse , Dongming Qiu , Rachid Taha , Jeffrey J. Ramler , Yong Wang , Richard Long
发明人： Barry L. Yang , Francis P. Daly , Junko M. Watson , Terry Manzanec , Sean P. Fitzgerald , Bradley R. Johnson , Xiaohong Li , Chunshe Cao , Ya-Huei Chin , Anna Lee Tonkovich , Ravi Arora , David J. Hesse , Dongming Qiu , Rachid Taha , Jeffrey J. Ramler , Yong Wang , Richard Long
IPC分类号： B01D8/02 , B01D39/00 , C07C7/20
CPC分类号： C01B3/384 , B01J19/0093 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00869 , B01J2219/00873 , B01J2219/0236 , C01B2203/0233 , C01B2203/0811 , C23C8/10 , C23C16/12 , C23C16/56 , H01M2008/1293 , Y02P20/52 , Y10S585/92 , Y10S585/924
摘要： The invention describes microchannel apparatus and catalysts that contain a layer of a metal aluminide or are made in a process in which a metal aluminide layer is formed as an intermediate. Certain processing conditions have surprisingly been found to result in superior coatings. The invention includes chemical processes conducted through apparatus described in the specification. Other catalysts and catalyst synthesis techniques are also described.
摘要翻译：本发明描述了包含金属铝化物层的微通道装置和催化剂，或者是在其中形成金属铝化物层作为中间体的方法制造的。令人惊奇地发现某些加工条件导致优异的涂层。本发明包括通过本说明书中描述的设备进行的化学过程。还描述了其它催化剂和催化剂合成技术。

5. 发明申请

US20100300550A1 Multi-Stream Microchannel Device 审中-公开
标题翻译：多流微通道设备
公开(公告)号：US20100300550A1
公开(公告)日：2010-12-02
申请号：US12839063
申请日：2010-07-19
申请人： James Allen Mathias , G. Bradley Chadwell , Dongming Qiu , Anna Lee Y.Tonkovich , Steven T. Perry , Matthew B. Schmidt , Sean P. Fitzgerald , David J. Hesse , Thomas D. Yuschak , Bin Yang
发明人： James Allen Mathias , G. Bradley Chadwell , Dongming Qiu , Anna Lee Y.Tonkovich , Steven T. Perry , Matthew B. Schmidt , Sean P. Fitzgerald , David J. Hesse , Thomas D. Yuschak , Bin Yang
IPC分类号： B81B1/00 , F15C1/06 , F28D3/02
CPC分类号： F16L41/02 , B01J19/0093 , B01J35/04 , B01J2219/00869 , B01J2219/00891 , C01B3/384 , C01B2203/0233 , C01B2203/0811 , C01B2203/0822 , F28D7/0066 , F28D9/0093 , F28F3/12 , F28F7/02 , F28F2260/02 , Y02P20/128 , Y02P20/52 , Y10T137/0318 , Y10T137/6579 , Y10T137/87153 , Y10T137/87249
摘要： Provided is a process and device for exchanging heat energy between three or more streams in a microchannel heat exchanger which can be integrated with a microchannel reactor to form an integrated microchannel processing unit. The combining of a plurality of integrated microchannel devices to provide the benefits of large-scale operation is enabled. In particular, the microchannel heat exchanger enables flexible heat transfer between multiple streams and total heat transfer rates of about 1 Watt or more per core unit volume expressed as W/cc.
摘要翻译：提供了一种用于在微通道热交换器中的三个或更多个流之间交换热能的过程和装置，其可以与微通道反应器集成以形成集成的微通道处理单元。实现了多个集成微通道装置的组合以提供大规模操作的优点。特别地，微通道热交换器使得能够在多个流之间实现柔性热传递，并且以W / cc表示的每单位体积的约1瓦或更高的总传热速率。

6. 发明授权

US07780944B2 Multi-stream microchannel device 有权
标题翻译：多流微通道设备
公开(公告)号：US07780944B2
公开(公告)日：2010-08-24
申请号：US11300914
申请日：2005-12-15
申请人： James A. Mathias , G. Bradley Chadwell , Dongming Qiu , Annalee Y. Tonkovich , Steven T. Perry , Matthew B. Schmidt , Sean P. Fitzgerald , David J. Hesse , Thomas D. Yuschak , Bin Yang
发明人： James A. Mathias , G. Bradley Chadwell , Dongming Qiu , Annalee Y. Tonkovich , Steven T. Perry , Matthew B. Schmidt , Sean P. Fitzgerald , David J. Hesse , Thomas D. Yuschak , Bin Yang
IPC分类号： C01B3/24 , C01B3/26
CPC分类号： F16L41/02 , B01J19/0093 , B01J35/04 , B01J2219/00869 , B01J2219/00891 , C01B3/384 , C01B2203/0233 , C01B2203/0811 , C01B2203/0822 , F28D7/0066 , F28D9/0093 , F28F3/12 , F28F7/02 , F28F2260/02 , Y02P20/128 , Y02P20/52 , Y10T137/0318 , Y10T137/6579 , Y10T137/87153 , Y10T137/87249
摘要： The invention is a process and device for exchanging heat energy between three or more streams in a microchannel heat exchanger which can be integrated with a microchannel reactor to form an integrated microchannel processing unit. The invention enables the combining of a plurality of integrated microchannel devices to provide the benefits of large-scale operation. In particular, the microchannel heat exchanger of the present invention enables flexible heat transfer between multiple streams and total heat transfer rates of about 1 Watt or more per core unit volume expressed as W/cc.
摘要翻译：本发明是一种用于在微通道热交换器中的三个或更多个流之间交换热能的方法和装置，其可以与微通道反应器集成以形成集成的微通道处理单元。本发明使得能够组合多个集成微通道装置以提供大规模操作的优点。特别地，本发明的微通道热交换器能够在多个流之间实现柔性热传递，并且以W / cc表示的每单位体积的约1瓦特或更高的总传热速率。

7. 发明申请

US20090196805A1 In Situ Mixing in Microchannels 有权
标题翻译：微通道原位混合
公开(公告)号：US20090196805A1
公开(公告)日：2009-08-06
申请号：US12334550
申请日：2008-12-15
申请人： Anna Lee Tonkovich , Kai Jarosch , David J. Hesse , Sean P. Fitzgerald
发明人： Anna Lee Tonkovich , Kai Jarosch , David J. Hesse , Sean P. Fitzgerald
IPC分类号： B01J8/06 , G05D11/00
CPC分类号： B01L3/502715 , B01F5/0475 , B01F5/0682 , B01F5/0691 , B01F13/0059 , B01F2215/0427 , B01F2215/0431 , B01J19/0093 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01L2400/04 , Y10T137/0329
摘要： The present invention provides methods, systems and apparatus in which one fluid passes through an orifice or orifices and mixes with another fluid as it flows through a microchannel.
摘要翻译：本发明提供了一种方法，系统和装置，其中一种流体在其流过微通道时通过孔或孔并与另一流体混合。

8. 发明申请

US20090131612A1 Microchannel polymerization reactor 有权
标题翻译：微通道聚合反应器
公开(公告)号：US20090131612A1
公开(公告)日：2009-05-21
申请号：US12288571
申请日：2008-10-21
申请人： Sean P. Fitzgerald , David J. Hesse , Anna Lee Y. Tonkovich , Laura J. Silva
发明人： Sean P. Fitzgerald , David J. Hesse , Anna Lee Y. Tonkovich , Laura J. Silva
IPC分类号： B01J19/18 , C08F2/01
CPC分类号： B01J19/0093 , B01F5/0475 , B01F5/0478 , B01F5/0619 , B01F5/0646 , B01F5/0653 , B01F5/0682 , B01F5/0688 , B01F13/0059 , B01J2219/00783 , B01J2219/00822 , B01J2219/00844 , B01J2219/0086 , B01J2219/00862 , B01J2219/00871 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/00907 , F28D7/00 , F28D9/00 , F28F2260/02 , Y10S526/918 , Y10T137/212
摘要： A microchannel polymerization reactor comprising: (a) a first microchannel adapted to carry a reactant stream; (b) a fluid conduit adapted to carry a fluid in thermal communication with the first microchannel; and (c) a static mixer in fluid communication with the first microchannel adapted to provide a mixing zone operative to change the cross-sectional fluid flow profile at a predetermined point along the first microchannel without changing the primary direction of the reactant stream through the first microchannel. The present invention also includes a method of carrying out a polymerization reaction within a microchannel reactor comprising: (i) directing at least one of monomer, initiator, water, surfactant, coagulant, and solvent into a reactant stream and into contact with reactant flowing within a first microchannel to initiate a polymerization reaction occurring within a first microchannel; and (ii) mixing the reactant of the reactant stream by positioning at least one static mixer in series with the reactant stream, where the static mixer is adapted to change a cross-sectional fluid flow profile of the reactant stream flowing through the first microchannel without changing a primary direction of the reactant stream through the first microchannel.
摘要翻译：一种微通道聚合反应器，包括：（a）适于携带反应物流的第一微通道; （b）适于承载与第一微通道热连通的流体的流体导管; 和（c）与所述第一微通道流体连通的静态混合器，其适于提供混合区域，其可操作以沿着所述第一微通道改变在预定点处的横截面流体流动分布，而不改变所述反应物流的主要方向通过所述第一微通道。本发明还包括在微通道反应器内进行聚合反应的方法，包括：（i）将单体，引发剂，水，表面活性剂，凝结剂和溶剂中的至少一种引入反应物流中并与在其内流动的反应物接触引发在第一微通道内发生聚合反应的第一微通道; 和（ii）通过将至少一个与反应物流串联的静态混合器定位来混合反应物流的反应物，其中静态混合器适于改变流过第一微通道的反应物流的横截面流体流动分布，而没有改变反应物流通过第一微通道的主要方向。

9. 发明授权

US07459508B2 Microchannel polymerization reactor 失效
标题翻译：微通道聚合反应器
公开(公告)号：US07459508B2
公开(公告)日：2008-12-02
申请号：US11073350
申请日：2005-03-02
申请人： Sean P. Fitzgerald , David J. Hesse , Anna Lee Y. Tonkovich , Laura J. Silva
发明人： Sean P. Fitzgerald , David J. Hesse , Anna Lee Y. Tonkovich , Laura J. Silva
IPC分类号： C08F2/00 , B01J19/24
CPC分类号： B01J19/0093 , B01F5/0475 , B01F5/0478 , B01F5/0619 , B01F5/0646 , B01F5/0653 , B01F5/0682 , B01F5/0688 , B01F13/0059 , B01J2219/00783 , B01J2219/00822 , B01J2219/00844 , B01J2219/0086 , B01J2219/00862 , B01J2219/00871 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/00907 , F28D7/00 , F28D9/00 , F28F2260/02 , Y10S526/918 , Y10T137/212
摘要： A microchannel polymerization reactor comprising: (a) a first microchannel adapted to carry a reactant stream; (b) a fluid conduit adapted to carry a fluid in thermal communication with the first microchannel; and (c) a static mixer in fluid communication with the first microchannel adapted to provide a mixing zone operative to change the cross-sectional fluid flow profile at a predetermined point along the first microchannel without changing the primary direction of the reactant stream through the first microchannel. The present invention also includes a method of carrying out a polymerization reaction within a microchannel reactor comprising: (i) directing at least one of monomer, initiator, water, surfactant, coagulant, and solvent into a reactant stream and into contact with reactant flowing within a first microchannel to initiate a polymerization reaction occurring within a first microchannel; and (ii) mixing the reactant of the reactant stream by positioning at least one static mixer in series with the reactant stream, where the static mixer is adapted to change a cross-sectional fluid flow profile of the reactant stream flowing through the first microchannel without changing a primary direction of the reactant stream through the first microchannel.
摘要翻译：一种微通道聚合反应器，包括：（a）适于携带反应物流的第一微通道; （b）适于承载与第一微通道热连通的流体的流体导管; 和（c）与所述第一微通道流体连通的静态混合器，其适于提供混合区域，其可操作以沿着所述第一微通道改变在预定点处的横截面流体流动分布，而不改变所述反应物流的主要方向通过所述第一微通道。本发明还包括在微通道反应器内进行聚合反应的方法，包括：（i）将单体，引发剂，水，表面活性剂，凝结剂和溶剂中的至少一种引入反应物流中并与在其内流动的反应物接触引发在第一微通道内发生聚合反应的第一微通道; 和（ii）通过将至少一个与反应物流串联的静态混合器定位来混合反应物流的反应物，其中静态混合器适于改变流过第一微通道的反应物流的横截面流体流动分布，而没有改变反应物流通过第一微通道的主要方向。

10. 发明授权

US09500414B2 Partial boiling in mini and micro-channels 有权
公开(公告)号：US09500414B2
公开(公告)日：2016-11-22
申请号：US13596033
申请日：2012-08-27
申请人： Anna Lee Tonkovich , David J. Hesse , Sean P. Fitzgerald , Bin Yang , Ravi Arora , Laura J. Silva , G. Bradley Chadwell , Kai Jarosch , Dongming Qiu
发明人： Anna Lee Tonkovich , David J. Hesse , Sean P. Fitzgerald , Bin Yang , Ravi Arora , Laura J. Silva , G. Bradley Chadwell , Kai Jarosch , Dongming Qiu
IPC分类号： B01J19/24 , F28D9/00 , B01B1/00 , F28F1/00 , B01J19/00 , C07B61/00 , F28D15/04 , F28F13/00 , F28D21/00 , F28D15/02 , F28F13/18
CPC分类号： F28F1/00 , B01B1/005 , B01J19/0013 , B01J19/0093 , B01J2219/00054 , B01J2219/00074 , B01J2219/00783 , B01J2219/00822 , B01J2219/00835 , B01J2219/0086 , B01J2219/00869 , B01J2219/00873 , B01J2219/00891 , B01J2219/00995 , B01J2219/182 , B01J2219/2411 , B01J2219/2462 , C07B61/00 , F28D9/00 , F28D15/04 , F28D2015/0225 , F28D2021/0022 , F28D2021/0064 , F28F13/00 , F28F13/187 , F28F2260/02
摘要： The invention provides methods, apparatus and systems in which there is partial boiling of a liquid in a mini-channel or microchannel. The partial boiling removes heat from an exothermic process.

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