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1. 发明授权

US06315965B1 Phosphine generator for producing phosphine-containing gas 有权
标题翻译：用于生产含磷化氢气体的磷化氢发生器
公开(公告)号：US06315965B1
公开(公告)日：2001-11-13
申请号：US09351129
申请日：1999-07-12
申请人： Franziskus Horn Feja , Christoph Reichmuth
发明人： Franziskus Horn Feja , Christoph Reichmuth
IPC分类号： B01J808
CPC分类号： A23L3/3409 , A23B9/18 , A23L3/358 , B01J4/00 , B01J7/02 , C01B25/06 , C01B25/081 , C01B25/085 , Y02P20/145
摘要： A process and apparatus is disclosed for generating a mixture of phosphine and diluent gas(es). A hydrolysable metal phosphide, preferably magnesium phosphide, is released directly into liquid water under an atmosphere of gas inert to phosphine and in a free-flowing particulate form, composed of loose metal phosphide particles. The generated mixture of phosphine and inert carrier gas, e.g. CO2, is used as such or is diluted into a gas mixing chamber with air to a concentration below the ignitability limit before being used in fumigation. Using argon as a carrier gas the phosphine mixture is suitable for semiconductor doping.
摘要翻译：公开了用于产生磷化氢和稀释气体的混合物的方法和装置。可水解的金属磷化物，优选磷化镁，在对磷化氢惰性气体和由松散金属磷化物颗粒组成的自由流动的颗粒形式的气氛中直接释放到液态水中。生成的膦和惰性载气的混合物，例如二氧化碳原样使用，或者在用于熏蒸之前用空气稀释至浓度低于可燃极限的气体混合室。使用氩作为载气，磷化氢混合物适用于半导体掺杂。

2. 发明授权

US6027667A Process and apparatus for producing phosphine-containing gas 失效
标题翻译：用于生产含磷的气体的方法和装置
公开(公告)号：US6027667A
公开(公告)日：2000-02-22
申请号：US659911
申请日：1996-06-07
申请人： Franziskus Horn Feja , Christoph Reichmuth
发明人： Franziskus Horn Feja , Christoph Reichmuth
IPC分类号： A01M17/00 , A01N25/18 , A23B9/18 , A23L3/3409 , A23L3/358 , B01J4/00 , B01J7/02 , B01J19/14 , C01B25/06 , C01B25/08 , C07F9/00
CPC分类号： A23L3/3409 , A23B9/18 , A23L3/358 , B01J4/00 , B01J7/02 , C01B25/06 , C01B25/081 , C01B25/085 , Y02P20/145
摘要： A process and apparatus is disclosed for generating a mixture of phosphine and diluent gas(es). A hydrolyzable metal phosphide, preferably magnesium phosphide, is released directly into liquid water under an atmosphere of gas inert to phosphine and in a free-flowing particulate form, composed of loose metal phosphide particles. The generated mixture of phosphine and inert carrier gas, e.g. CO.sub.2, is used as such or is diluted into a gas mixing chamber with air to a concentration below the ignitability limit before being used in fumigation. Using argon as a carrier gas the phosphine mixture is suitable for semiconductor doping.
摘要翻译：公开了用于产生磷化氢和稀释气体的混合物的方法和装置。可水解的金属磷化物，优选磷化镁，在对磷化氢惰性气体和由松散的金属磷化物颗粒组成的自由流动的颗粒形式的气氛中直接释放到液态水中。生成的膦和惰性载气的混合物，例如二氧化碳原样使用，或者在用于熏蒸之前用空气稀释至浓度低于可燃极限的气体混合室。使用氩作为载气，磷化氢混合物适用于半导体掺杂。

3. 发明授权

US3932225A Process for separately recovering uranium, transuranium elements, and fission products of uranium from atomic reactor fuel 失效
标题翻译：从原子反应堆燃料中单独回收铀，铀元素和铀裂变产物的过程
公开(公告)号：US3932225A
公开(公告)日：1976-01-13
申请号：US303377
申请日：1972-11-03
申请人： Abdel-Lativ Bilal , Klaus Metscher , Bernhard Muhlig , Christoph Reichmuth , Bernd Schwarz , Karl-Erik Zimen
发明人： Abdel-Lativ Bilal , Klaus Metscher , Bernhard Muhlig , Christoph Reichmuth , Bernd Schwarz , Karl-Erik Zimen
IPC分类号： B01D57/00 , B01D59/46 , G21C19/46 , C01G56/00
CPC分类号： G21C19/46 , Y02W30/883
摘要： Spent reactor fuel elements are dissolved in dilute nitric acid. After addition of acetic acid as a complexing agent, the nitric acid is partly decomposed and the mixture subjected to electrolysis while a carrier liquid, which may be dilute acetic acid or a dilute mixture of acetic acid and nitric acid is caused to flow in the electric field between the electrodes either against the direction of ion migration or transversely thereto. The ions of uranium, plutonium and other transuranium elements, and of fission products accumulate in discrete portions of the electrolyte and are separately withdrawn as at least three fractions after one or more stages of electrolysis.
摘要翻译：废反应堆燃料元素溶解在稀硝酸中。加入乙酸作为络合剂后，硝酸部分分解，混合物进行电解，同时将可能是稀乙酸或乙酸和硝酸的稀混合物的载液流入电电极之间的电场相对于离子迁移的方向或横向于其之间。铀，钚和其他超铀元素的离子和裂变产物的离子积聚在电解质的离散部分中，并且在一个或多个电解阶段之后分别作为至少三个馏分取出。

4. 发明授权

US5820840A Composition for producing phosphine gas 失效
标题翻译：用于生产磷化氢气体的组成
公开(公告)号：US5820840A
公开(公告)日：1998-10-13
申请号：US659916
申请日：1996-06-07
申请人： Franziskus Horn Feja , Christoph Reichmuth
发明人： Franziskus Horn Feja , Christoph Reichmuth
IPC分类号： A01M17/00 , A01N25/18 , A23B9/18 , A23L3/3409 , A23L3/358 , B01J4/00 , B01J7/02 , B01J19/14 , C01B25/06 , C01B25/08 , C07F9/00 , C01B25/00
CPC分类号： A23L3/3409 , A23B9/18 , A23L3/358 , B01J4/00 , B01J7/02 , C01B25/06 , C01B25/081 , C01B25/085 , Y02P20/145
摘要： A metal phosphide composition is disclosed for generating a mixture of phosphine and diluent gas(es), presented ready for use in a hydrolysis process or apparatus in the form of a free-flowing particulate metal phosphide material composed of loose particles of said metal phosphide essentially free of metal phosphide dust, essentially free of hydrolysis retarding agents and essentially free of hydrophobic substances in the form of coatings or hydrophobizing additives. In use the hydrolyzable metal phosphide, preferably magnesium phosphide, is released directly into liquid water under an atmosphere of gas inert to phosphine. The generated mixture of phosphine and inert carrier gas, e.g. CO.sub.2, can be used as such or is diluted into a gas mixing chamber with air to a concentration below the ignitability limit before being used in fumigation. The composition is manufactured by reacting a finely divided metal, selected from the group consisting of aluminum, calcium and magnesium with yellow phosphorus in an inert gas atmosphere and in the presence of a catalyst. Throughout the reaction batch and throughout the process, once reacting has commenced, a temperature is maintained within the range of 350.degree. C. to 550.degree. C. The metal phosphide is withdrawn as a particulate free-flowing material and is packaged ready for use in phosphine generation in such free-flowing condition, essentially free of dust, essentially free of hydrolysis retarding agents and essentially free of hydrophobizing substance in the form of coating or hydrophobizing additives, in a gastight container.
摘要翻译：公开了一种金属磷化物组合物，其用于产生磷化氢和稀释气体的混合物，其准备用于水解过程或设备，其形式为自由流动的颗粒状金属磷化物材料，所述颗粒金属磷化物基本上由所述金属磷化物的松散颗粒组成没有金属磷化物粉尘，基本上不含水解阻滞剂，基本上不含涂层或疏水添加剂形式的疏水物质。在使用中，可水解金属磷化物，优选磷化镁，在对膦无惰性气体的气氛中直接释放到液态水中。生成的膦和惰性载气的混合物，例如 CO2可以原样使用，或者在用于熏蒸之前，用空气稀释到浓度低于可燃极限的气体混合室。该组合物通过在惰性气体气氛中和在催化剂存在下使选自铝，钙和镁的细碎金属与黄磷反应来制造。在整个反应批次和整个过程中，一旦反应开始，温度保持在350℃至550℃的范围内。金属磷化物作为颗粒自由流动材料取出，并被包装准备用于这种自由流动状态下的膦生成基本上不含灰尘，基本上不含水解阻滞剂，并且在气密容器中基本上不含涂层或疏水添加剂形式的疏水化物质。

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