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1. 发明申请

US20120208246A1 PRODUCTION OF ALCOHOL ESTERS AND IN SITU PRODUCT REMOVAL DURING ALCOHOL FERMENTATION 有权
标题翻译：在酒精发酵期间生产酒精产品和脱除产品
公开(公告)号：US20120208246A1
公开(公告)日：2012-08-16
申请号：US13193147
申请日：2011-07-28
申请人： Douglas Robert Anton , Stephane Francois Bazzana , Keith H. Burlew , Jelena Cirakovic , Robert Dicosimo , Bruce A. Diner , Michael Charles Grady , Brian Michael Roesch , Francis J. Woerner
发明人： Douglas Robert Anton , Stephane Francois Bazzana , Keith H. Burlew , Jelena Cirakovic , Robert Dicosimo , Bruce A. Diner , Michael Charles Grady , Brian Michael Roesch , Francis J. Woerner
IPC分类号： C12P7/64 , C12N9/16 , A23K1/06 , C12P7/16
CPC分类号： A23K1/007 , A23K10/12 , A23K10/38 , C12P7/16 , C12P7/62 , C12P7/649 , C12P2203/00 , Y02E50/10 , Y02E50/13 , Y02P60/873
摘要： An alcohol fermentation process and composition that includes production of alcohol esters by esterification of product alcohol in a fermentation medium with a carboxylic acid (e.g., fatty acid) and a catalyst (e.g., lipase) capable of esterifying the product alcohol, such as butanol, with the carboxylic acid to form the alcohol esters. The alcohol esters can be extracted from the fermentation medium, and the product alcohol recovered from the alcohol esters. The carboxylic acid can also serve as an extractant for removal of the alcohol esters from the fermentation medium.
摘要翻译：醇发酵方法和组合物，其包括通过在发酵培养基中与产物醇与羧酸（例如，脂肪酸）和能够酯化产物醇（例如丁醇）的催化剂（例如脂肪酶）酯化产生醇酯，与羧酸形成醇酯。醇酯可以从发酵培养基中提取，并从醇酯中回收产物醇。羧酸也可以用作从发酵培养基中除去醇酯的提取剂。

2. 发明授权

US06294700B1 Separation processes 有权
标题翻译：分离过程
公开(公告)号：US06294700B1
公开(公告)日：2001-09-25
申请号：US09526636
申请日：2000-03-15
申请人： Jeffrey Scott Kanel , John Nicholas Argyropoulos , Ailene Gardner Phillips , Brian Michael Roesch , John Robert Briggs , Max Min Lee , John Michael Maher , David Robert Bryant
发明人： Jeffrey Scott Kanel , John Nicholas Argyropoulos , Ailene Gardner Phillips , Brian Michael Roesch , John Robert Briggs , Max Min Lee , John Michael Maher , David Robert Bryant
IPC分类号： C07C4550
CPC分类号： C07B63/00 , C07C45/50 , Y02P20/582 , C07C47/02
摘要： This invention relates to a process for separating one or more products from a reaction product fluid comprising a metal-organophosphorus ligand complex catalyst, optionally free organophosphorus ligand, said one or more products, one or more polar reaction solvents and one or more nonpolar reaction solvents, wherein said process comprises (1) subjecting said reaction product fluid to fractional countercurrent extraction with at least two immiscible extraction solvents, said at least two immiscible extraction solvents comprising at least one polar extraction solvent and at least one nonpolar extraction solvent, to obtain a polar phase comprising said metal-organophosphorus ligand complex catalyst, said optionally free organophosphorus ligand, said one or more polar reaction solvents and said at least one polar extraction solvent and a nonpolar phase comprising said one or more products, said one or more nonpolar reaction solvents and said at least one nonpolar extraction solvent, and (2) recovering said nonpolar phase from said polar phase; wherein (i) the organophosphorus ligand has a partition coefficient Kp1 defined herein between the polar phase and the nonpolar phase of greater than about 5, and (ii) the one or more products have a partition coefficient Kp2 defined herein between the polar phase and the nonpolar phase of less than about 2.0.
摘要翻译：本发明涉及用于从反应产物流体中分离一种或多种产物的方法，其包括金属 - 有机磷配体配合物催化剂，任选的游离有机磷配体，所述一种或多种产物，一种或多种极性反应溶剂和一种或多种非极性反应溶剂其中所述方法包括（1）使所述反应产物流体与至少两种不混溶的萃取溶剂进行分数逆流萃取，所述至少两种不混溶的萃取溶剂包含至少一种极性萃取溶剂和至少一种非极性萃取溶剂，以获得所述极性相包含所述金属 - 有机磷配体配合物催化剂，所述任选游离的有机磷配体，所述一种或多种极性反应溶剂和所述至少一种极性提取溶剂和包含所述一种或多种产物的非极性相，所述一种或多种非极性反应溶剂并表示至少一种非极性萃取溶剂，和（ 2）从所述极性相中回收所述非极性相; 其中（i）有机磷配体在极性相和非极性相之间定义的分配系数Kp1大于约5，和（ii）一种或多种产物在极性相和极性相之间具有限定的分配系数Kp2 非极性相小于约2.0。

3. 发明授权

US09040263B2 Production of alcohol esters and in situ product removal during alcohol fermentation 有权
标题翻译：酒精发酵过程中生产醇酯和原位产物去除
公开(公告)号：US09040263B2
公开(公告)日：2015-05-26
申请号：US13193147
申请日：2011-07-28
申请人： Douglas Robert Anton , Stephane Francois Bazzana , Keith H. Burlew , Jelena Cirakovic , Robert Dicosimo , Bruce A. Diner , Michael Charles Grady , Brian Michael Roesch , Francis J. Woerner
发明人： Douglas Robert Anton , Stephane Francois Bazzana , Keith H. Burlew , Jelena Cirakovic , Robert Dicosimo , Bruce A. Diner , Michael Charles Grady , Brian Michael Roesch , Francis J. Woerner
IPC分类号： C12P7/64 , A23K1/00 , A23K1/06 , C12P7/16 , C12P7/62
CPC分类号： A23K1/007 , A23K10/12 , A23K10/38 , C12P7/16 , C12P7/62 , C12P7/649 , C12P2203/00 , Y02E50/10 , Y02E50/13 , Y02P60/873
摘要： An alcohol fermentation process and composition that includes production of alcohol esters by esterification of product alcohol in a fermentation medium with a carboxylic acid (e.g., fatty acid) and a catalyst (e.g., lipase) capable of esterifying the product alcohol, such as butanol, with the carboxylic acid to form the alcohol esters. The alcohol esters can be extracted from the fermentation medium, and the product alcohol recovered from the alcohol esters. The carboxylic acid can also serve as an extractant for removal of the alcohol esters from the fermentation medium.
摘要翻译：醇发酵方法和组合物，其包括通过在发酵培养基中与产物醇与羧酸（例如，脂肪酸）和能够酯化产物醇（例如丁醇）的催化剂（例如脂肪酶）酯化产生醇酯，与羧酸形成醇酯。醇酯可以从发酵培养基中提取，并从醇酯中回收产物醇。羧酸也可以用作从发酵培养基中除去醇酯的提取剂。

4. 发明授权

US08557540B2 Methods and systems for removing undissolved solids prior to extractive fermentation in the production of butanol 有权
标题翻译：在生产丁醇中萃取发酵之前去除未溶解固体的方法和系统
公开(公告)号：US08557540B2
公开(公告)日：2013-10-15
申请号：US13163243
申请日：2011-06-17
申请人： Keith H. Burlew , Michael Charles Grady , John W. Hallam , David J. Lowe , Brian Michael Roesch , Joseph J. Zaher
发明人： Keith H. Burlew , Michael Charles Grady , John W. Hallam , David J. Lowe , Brian Michael Roesch , Joseph J. Zaher
IPC分类号： C12P7/16 , C12P7/04 , C12P7/06 , C12P1/00 , C12M1/00 , C12M3/00 , A23J1/14
CPC分类号： C12P7/16 , A23K10/38 , B01D3/002 , B01D11/0492 , B01D21/26 , B01D21/262 , C07C29/86 , C11B1/025 , C11B13/00 , C12F3/10 , C12M1/00 , C12M21/12 , C12M45/04 , C12M45/09 , C12N1/14 , C12N15/00 , C12P7/18 , C12P7/6418 , Y02E50/10 , Y02E50/16 , Y02E50/17 , Y02W30/74
摘要： A method and system for efficiently producing a fermentative product alcohol such as butanol utilizing in situ product extraction are provided. The efficiency is obtained through separating undissolved solids after liquefying a given feedstock to create a feedstock and prior to fermentation, for example, through centrifugation. Removal of the undissolved solids avoids problems associated with having the undissolved solids present during in situ production extraction, and thereby increases the efficiency of the alcohol production.
摘要翻译：提供了利用原位产物提取有效地生产发酵产物醇如丁醇的方法和系统。通过在液化给定原料以产生原料并且在发酵之前，例如通过离心分离未溶解的固体，获得效率。去除未溶解的固体避免了在原位生产提取期间存在未溶解固体的问题，从而提高了醇生产的效率。

5. 发明申请

US20120164302A1 METHODS AND SYSTEMS FOR REMOVING UNDISSOLVED SOLIDS PRIOR TO EXTRACTIVE FERMENTATION IN THE PRODUCTION OF BUTANOL 有权
标题翻译：在丁醇生产中提取发酵前除去未溶解固体的方法和系统
公开(公告)号：US20120164302A1
公开(公告)日：2012-06-28
申请号：US13163243
申请日：2011-06-17
申请人： BRIAN MICHAEL ROESCH , Keith H. Burlew , John W. Hallam , David J. Lowe , Joseph J. Zaher
发明人： BRIAN MICHAEL ROESCH , Keith H. Burlew , John W. Hallam , David J. Lowe , Joseph J. Zaher
IPC分类号： C12P7/16 , A23D9/00 , C12M1/00 , A23K1/00 , C12P7/04 , C12P7/06
CPC分类号： C12P7/16 , A23K10/38 , B01D3/002 , B01D11/0492 , B01D21/26 , B01D21/262 , C07C29/86 , C11B1/025 , C11B13/00 , C12F3/10 , C12M1/00 , C12M21/12 , C12M45/04 , C12M45/09 , C12N1/14 , C12N15/00 , C12P7/18 , C12P7/6418 , Y02E50/10 , Y02E50/16 , Y02E50/17 , Y02W30/74
摘要： A method and system for efficiently producing a fermentative product alcohol such as butanol utilizing in situ product extraction are provided. The efficiency is obtained through separating undissolved solids after liquefying a given feedstock to create a feedstock and prior to fermentation, for example, through centrifugation. Removal of the undissolved solids avoids problems associated with having the undissolved solids present during in situ production extraction, and thereby increases the efficiency of the alcohol production.
摘要翻译：提供了利用原位产物提取有效地生产发酵产物醇如丁醇的方法和系统。通过在液化给定原料以产生原料并且在发酵之前，例如通过离心分离未溶解的固体，获得效率。去除未溶解的固体避免了在原位生产提取期间存在未溶解固体的问题，从而提高了醇生产的效率。

6. 发明授权

US06310260B1 Separation processes 有权
标题翻译：分离过程
公开(公告)号：US06310260B1
公开(公告)日：2001-10-30
申请号：US09526191
申请日：2000-03-15
申请人： John Nicholas Argyropoulos , Jeffrey Scott Kanel , Michael Leo Tulchinsky , David James Miller , Donald Lee Morrison , Paul Foley , David Robert Bryant , Ailene Gardner Phillips , Brian Michael Roesch , John Robert Briggs , Max Min Lee , John Michael Maher
发明人： John Nicholas Argyropoulos , Jeffrey Scott Kanel , Michael Leo Tulchinsky , David James Miller , Donald Lee Morrison , Paul Foley , David Robert Bryant , Ailene Gardner Phillips , Brian Michael Roesch , John Robert Briggs , Max Min Lee , John Michael Maher
IPC分类号： C07C4550
CPC分类号： C07C45/50 , C07B63/00 , Y02P20/582 , C07C47/02
摘要： This invention relates to a process for separating one or more organophosphorus ligand degradation products, one or more reaction byproducts and one or more products from a continuously generated reaction product fluid comprising one or more unreacted reactants, a metal-organophosphorus ligand complex catalyst, optionally free organophosphorus ligand, said one or more organophosphorus ligand degradation products, said one or more reaction byproducts, said one or more products, one or more polar solvents and one or more nonpolar solvents by phase separation wherein (i) the selectivity of the polar phase for the organophosphorus ligand with respect to the one or more products is expressed by a partition coefficient ratio Ef1 which is a value greater than about 2.5, (ii) the selectivity of the polar phase for the organophosphorus ligand with respect to the one or more organophosphorus ligand degradation products is expressed by a partition coefficient ratio Ef2 which is a value greater than about 2.5, and (iii) the selectivity of the polar phase for the organophosphorus ligand with respect to the one or more reaction byproducts is expressed by a partition coefficient ratio Ef3 which is a value greater than about 2.5.
摘要翻译：本发明涉及从连续生成的反应产物流体中分离一种或多种有机磷配体降解产物，一种或多种反应副产物和一种或多种产物，所述反应产物流体包含一种或多种未反应的反应物，金属 - 有机磷配体络合物催化剂，有机磷配体，所述一种或多种有机磷配体降解产物，所述一种或多种反应副产物，所述一种或多种产物，一种或多种极性溶剂和一种或多种非极性溶剂通过相分离，其中（i）极性相的选择性为相对于一种或多种产物的有机磷配体由分配系数比Ef1表示，分配系数比Ef1大于约2.5，（ii）有机磷配体的极性相对于一种或多种有机磷配体的选择性降解产物由分配系数比Ef2表示，该分配系数比Ef2是大于th的值约为2.5，和（iii）极性相对于一种或多种反应副产物的有机磷配体的选择性由分配系数比Ef3表示，该分配系数比Ef3是大于约2.5的值。

7. 发明授权

US06307110B1 Separation processes 有权
标题翻译：分离过程
公开(公告)号：US06307110B1
公开(公告)日：2001-10-23
申请号：US09526337
申请日：2000-03-15
申请人： John Nicholas Argyropoulos , Jeffrey Scott Kanel , Michael Leo Tulchinsky , David James Miller , Donald Lee Morrison , Paul Foley , David Robert Bryant , Ailene Gardner Phillips , Brian Michael Roesch , John Robert Briggs , Max Min Lee , John Michael Maher
发明人： John Nicholas Argyropoulos , Jeffrey Scott Kanel , Michael Leo Tulchinsky , David James Miller , Donald Lee Morrison , Paul Foley , David Robert Bryant , Ailene Gardner Phillips , Brian Michael Roesch , John Robert Briggs , Max Min Lee , John Michael Maher
IPC分类号： C07C4550
CPC分类号： C07C45/50 , C07B63/00 , Y02P20/582 , C07C47/02
摘要： This invention relates to a process for separating one or more organophosphorus ligand degradation products, one or more reaction byproducts and one or more products from a continuously generated reaction product fluid comprising one or more unreacted reactants, a metal-organophosphorus ligand complex catalyst, optionally free organophosphorus ligand, said one or more organophosphorus ligand degradation products, said one or more reaction byproducts, said one or more products, one or more nonpolar solvents and one or more polar solvents by phase separation wherein (i) the selectivity of the nonpolar phase for the organophosphorus ligand with respect to the one or more products is expressed by a partition coefficient ratio Ef1which is a value greater than about 2.5, (ii) the selectivity of the nonpolar phase for the organophosphorus ligand with respect to the one or more organophosphorus ligand degradation products is expressed by a partition coefficient ratio Ef2 which is a value greater than about 2.5, and (iii) the selectivity of the nonpolar phase for the organophosphorus ligand with respect to the one or more reaction byproducts is expressed by a partition coefficient ratio Ef3 which is a value greater than about 2.5.
摘要翻译：本发明涉及从连续生成的反应产物流体中分离一种或多种有机磷配体降解产物，一种或多种反应副产物和一种或多种产物，所述反应产物流体包含一种或多种未反应的反应物，金属 - 有机磷配体络合物催化剂，有机磷配体，所述一种或多种有机磷配体降解产物，所述一种或多种反应副产物，所述一种或多种产物，一种或多种非极性溶剂和一种或多种极性溶剂通过相分离，其中（i）非极性相的选择性为相对于一种或多种产物的有机磷配体由分配系数比Ef1表示，分配系数比Ef1大于约2.5，（ii）非极性相对于有机磷配体相对于一种或多种有机磷配体降解的选择性产品由分配系数比Ef2表示，该分配系数比Ef2是一个很大的值（iii）非极性相对于一种或多种反应副产物对有机磷配体的选择性由分配系数比Ef3表示，该分配系数比Ef3是大于约2.5的值。

8. 发明授权

US06303829B1 Separation processes 有权
标题翻译：分离过程
公开(公告)号：US06303829B1
公开(公告)日：2001-10-16
申请号：US09526434
申请日：2000-03-15
申请人： Jeffrey Scott Kanel , John Nicholas Argyropoulos , Ailene Gardner Phillips , Brian Michael Roesch , John Robert Briggs , Max Min Lee , John Michael Maher , David Robert Bryant
发明人： Jeffrey Scott Kanel , John Nicholas Argyropoulos , Ailene Gardner Phillips , Brian Michael Roesch , John Robert Briggs , Max Min Lee , John Michael Maher , David Robert Bryant
IPC分类号： C07C4550
CPC分类号： C07C45/50 , C07B63/00 , Y02P20/582 , C07C47/02
摘要： This invention relates to a process for separating one or more products from a reaction product fluid comprising a metal-organophosphorus ligand complex catalyst, optionally free organophosphorus ligand, said one or more products, one or more nonpolar reaction solvents and one or more polar reaction solvents, wherein said process comprises (1) subjecting said reaction product fluid to fractional countercurrent extraction with at least two immiscible extraction solvents, said at least two immiscible extraction solvents comprising at least one nonpolar extraction solvent and at least one polar extraction solvent, to obtain a nonpolar phase comprising said metal-organophosphorus ligand complex catalyst, said optionally free organophosphorus ligand, said one or more nonpolar reaction solvents and said at least one nonpolar extraction solvent and a polar phase comprising said one or more products, said one or more polar reaction solvents and said at least one polar extraction solvent, and (2) recovering said polar phase from said nonpolar phase; wherein (i) the organophosphorus ligand has a partition coefficient Kp1 defined herein between the nonpolar phase and the polar phase of greater than about 5, and (ii) the one or more products have a partition coefficient Kp2 defined herein between the nonpolar phase and the polar phase of less than about 2.0.
摘要翻译：本发明涉及从反应产物流体中分离一种或多种产物的方法，其包括金属 - 有机磷配体配合物催化剂，任选的游离有机磷配体，所述一种或多种产物，一种或多种非极性反应溶剂和一种或多种极性反应溶剂其中所述方法包括（1）使所述反应产物流体用至少两种不混溶的萃取溶剂进行分数逆流萃取，所述至少两种不混溶的萃取溶剂包含至少一种非极性萃取溶剂和至少一种极性提取溶剂，以获得所述非极性相包含所述金属 - 有机磷配体配合物催化剂，所述任选游离的有机磷配体，所述一种或多种非极性反应溶剂和所述至少一种非极性萃取溶剂和包含所述一种或多种产物的极性相，所述一种或多种极性反应溶剂并表示至少一种极性提取溶剂，和（ 2）从所述非极性相中回收所述极性相; 其中（i）有机磷配体具有在非极性相和极性相之间定义的分配系数Kp1大于约5，和（ii）一种或多种产物在非极性相和非极性相之间具有本文定义的分配系数Kp2 极性相小于约2.0。

9. 发明授权

US09175315B2 Production of alcohol esters and in situ product removal during alcohol fermentation 有权
公开(公告)号：US09175315B2
公开(公告)日：2015-11-03
申请号：US13162868
申请日：2011-06-17
申请人： Douglas Robert Anton , Stephane Francois Bazzana , Keith H Burlew , Jelena Cirakovic , Robert Dicosimo , Bruce A Diner , Michael Charles Grady , Brian Michael Roesch , Francis J Woerner
发明人： Douglas Robert Anton , Stephane Francois Bazzana , Keith H Burlew , Jelena Cirakovic , Robert Dicosimo , Bruce A Diner , Michael Charles Grady , Brian Michael Roesch , Francis J Woerner
IPC分类号： C12P7/62 , C12P7/22 , C12P7/16 , C12N1/00 , C12N1/12 , C07H21/04 , B01D3/00 , B01D21/26 , C07C29/86 , C11B1/02 , C11B13/00 , C12M1/00 , C12P7/64 , C12P7/18
CPC分类号： C12P7/16 , A23K10/38 , B01D3/002 , B01D11/0492 , B01D21/26 , B01D21/262 , C07C29/86 , C11B1/025 , C11B13/00 , C12F3/10 , C12M1/00 , C12M21/12 , C12M45/04 , C12M45/09 , C12N1/14 , C12N15/00 , C12P7/18 , C12P7/6418 , Y02E50/10 , Y02E50/16 , Y02E50/17 , Y02W30/74
摘要： An alcohol fermentation process and composition that includes production of alcohol esters by esterification of product alcohol in a fermentation medium with a carboxylic acid (e.g., fatty acid) and a catalyst (e.g., lipase) capable of esterifying the product alcohol, such as butanol, with the carboxylic acid to form the alcohol esters. The alcohol esters can be extracted from the fermentation medium, and the product alcohol recovered from the alcohol esters. The carboxylic acid can also serve as an extractant for removal of the alcohol esters from the fermentation medium.

10. 发明申请

US20130164795A1 CO-PRODUCTS FROM BIOFUEL PRODUCTION PROCESSES AND METHODS OF MAKING 审中-公开
标题翻译：生物制品生产过程中的副产品及其制备方法
公开(公告)号：US20130164795A1
公开(公告)日：2013-06-27
申请号：US13524990
申请日：2012-06-15
申请人： David J. LOWE , Brian Michael Roesch
发明人： David J. LOWE , Brian Michael Roesch
IPC分类号： A23K1/06 , C12P7/64
CPC分类号： C12P7/6409 , A23K10/38 , A23K50/10 , C12P7/16 , C12P7/649 , Y02E50/10 , Y02E50/13 , Y02E50/17 , Y02P60/873
摘要： The present invention includes methods of generating co-products for animal feed and compositions useful as co-products for animal feed derived from biofuel production processes. More specifically, the invention includes co-products for animal feed from at least one process feedstream, such as fatty acids from oil hydrolysis, lipids from evaporation of thin stillage, syrup, distillers grains, distillers grains and solubles, solids from a mash before fermentation, and solids from a whole stillage after fermentation.
摘要翻译：本发明包括产生用于动物饲料的副产物的方法和用作来自生物燃料生产方法的动物饲料的副产物的组合物。更具体地，本发明包括用于来自至少一种工艺原料流的动物饲料的共同产品，例如来自油水解的脂肪酸，来自蒸馏酒精，糖浆，酒糟，酒糟和可溶物的脂质，发酵前的醪液中的固体，和发酵后的整个酒糟的固体。

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