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1. 发明授权

US08808662B2 Process for production of a borohydride compound 有权
标题翻译：硼氢化合物的制备方法
公开(公告)号：US08808662B2
公开(公告)日：2014-08-19
申请号：US13053355
申请日：2011-03-22
申请人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
发明人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
IPC分类号： C01B6/04 , C01B6/21
CPC分类号： C01B6/21
摘要： A process for production of a borohydride compound M(BH4)y. The process has three steps. The first step combines a compound of formula (R1O)yM with aluminum, hydrogen and a metallic catalyst containing at least one metal selected from the group consisting of titanium, zirconium, hafnium, niobium, vanadium, tantalum and iron to produce a compound of formula M(AlH3OR1)y, wherein R1 is phenyl or phenyl substituted by at least one alkyl or alkoxy group; M is an alkali metal, Be or Mg; and y is one or two; wherein the catalyst is present at a level of at least 200 ppm based on weight of aluminum. The second step combines the compound of formula M(AlH3OR1)y with a borate, boroxine or borazine compound to produce M(BH4)y and a byproduct mixture containing alkali metal and aluminum aryloxides. The third step separates M(BH4)y from the byproduct mixture.
摘要翻译：制备硼氢化合物M（BH4）y的方法。该过程有三个步骤。第一步是将式（R1O）yM的化合物与铝，氢和含有选自钛，锆，铪，铌，钒，钽和铁中的至少一种金属的金属催化剂组合以制备式 M（AlH 3 OR 1）y，其中R 1是苯基或被至少一个烷基或烷氧基取代的苯基; M是碱金属，Be或Mg; y是一两个; 其中所述催化剂以基于铝的重量的至少200ppm的含量存在。第二步将式M化合物（AlH 3 OR 1）y与硼酸盐，环硼氧烷或环硼氮烷化合物结合，生成M（BH4）y和含有碱金属和铝酰氧化物的副产物混合物。第三步骤将M（BH4）y与副产物混合物分离。

2. 发明申请

US20050224365A1 One-step electrosynthesis of borohydride 审中-公开
标题翻译：一步电化学合成硼氢化物
公开(公告)号：US20050224365A1
公开(公告)日：2005-10-13
申请号：US11104120
申请日：2005-04-12
申请人： Duane Mazur , Norman Weinberg , Lawrence Guilbault , Arthur Achhing Chin , Klaus Tomantschger
发明人： Duane Mazur , Norman Weinberg , Lawrence Guilbault , Arthur Achhing Chin , Klaus Tomantschger
IPC分类号： C25B11/04 , C25B1/00 , C25B1/14 , C25B3/00
CPC分类号： C25B1/00 , C25B1/14 , C25B11/04
摘要： A method for producing borohydride by causing current to flow in an electrolytic cell between an anode and a cathode, wherein a solution of a boron-containing compound is in contact with the cathode, and wherein the cathode comprises a conductive material having activity as a high hydrogen overpotential electrode.
摘要翻译：通过使电流在阳极和阴极之间的电解池中流动而制造硼氢化物的方法，其中含硼化合物的溶液与阴极接触，并且其中阴极包括具有高活性的导电材料氢超电极。

3. 发明授权

US08377405B2 Process for production of a borohydride compound 失效
公开(公告)号：US08377405B2
公开(公告)日：2013-02-19
申请号：US12322567
申请日：2009-02-03
申请人： Arthur Achhing Chin , Puja Jain , Suzanne Linehan , Francis Joseph Lipiecki , Stephen Gerard Maroldo , Samuel J. November , John Hiroshi Yamamoto
发明人： Arthur Achhing Chin , Puja Jain , Suzanne Linehan , Francis Joseph Lipiecki , Stephen Gerard Maroldo , Samuel J. November , John Hiroshi Yamamoto
IPC分类号： C01B6/11
CPC分类号： C01B6/21
摘要： A process for production of a borohydride compound. The process comprises combining a compound comprising boron and oxygen with an adduct of alane.

4. 发明申请

US20110236300A1 PROCESS FOR PRODUCTION OF A METAL HYDRIDE 有权
标题翻译：生产金属氢化物的方法
公开(公告)号：US20110236300A1
公开(公告)日：2011-09-29
申请号：US13053350
申请日：2011-03-22
申请人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
发明人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
IPC分类号： C01B6/04
CPC分类号： C01B6/04
摘要： A process for production of a metal hydride compound MHx, wherein x is one or two and M is an alkali metal, Be or Mg. The process comprises combining a compound of formula (R1O)xM with aluminum, hydrogen and at least one metal selected from among titanium, zirconium, hafnium, niobium, vanadium, tantalum and iron to produce a compound of formula MHx. R1 is phenyl or phenyl substituted by at least one alkyl or alkoxy group. A mole ratio of aluminum to (R1O)xM is from 0.1:1 to 1:1. The catalyst is present at a level of at least 200 ppm based on weight of aluminum.
摘要翻译：一种制备金属氢化物化合物MHx的方法，其中x为一个或两个，M为碱金属Be或Mg。该方法包括将式（R1O）xM化合物与铝，氢和至少一种选自钛，锆，铪，铌，钒，钽和铁的金属组合以制备式MHx的化合物。 R 1是被至少一个烷基或烷氧基取代的苯基或苯基。铝与（R1O）xM的摩尔比为0.1:1至1:1。以铝的重量计，催化剂的含量至少为200ppm。

5. 发明申请

US20090214409A1 Process for production of a borohydride compound 失效
标题翻译：硼氢化合物的制备方法
公开(公告)号：US20090214409A1
公开(公告)日：2009-08-27
申请号：US12322567
申请日：2009-02-03
申请人： Arthur Achhing Chin , Puja Jain , Suzanne Linehan , Francis Joseph Lipiecki , Stephen Gerard Maroldo , Samuel J. November , John Hiroshi Yamamoto
发明人： Arthur Achhing Chin , Puja Jain , Suzanne Linehan , Francis Joseph Lipiecki , Stephen Gerard Maroldo , Samuel J. November , John Hiroshi Yamamoto
IPC分类号： C01B6/21
CPC分类号： C01B6/21
摘要： A process for production of a borohydride compound. The process comprises combining a compound comprising boron and oxygen with an adduct of alane.
摘要翻译：硼氢化合物的制造方法。该方法包括将包含硼和氧的化合物与丙烯的加合物组合。

6. 发明授权

US07455821B2 Process for production of a borohydride compound 有权
公开(公告)号：US07455821B2
公开(公告)日：2008-11-25
申请号：US11900491
申请日：2007-09-12
申请人： Arthur Achhing Chin
发明人： Arthur Achhing Chin
IPC分类号： C01B35/00
CPC分类号： C01B6/23
摘要： A process for production of a borohydride compound. The process comprises the steps of: (a) combining a boron-containing salt, at least one of a metal and its hydride; wherein the metal is Be, Mg, Ca, Sr, Ba, Al, Ga, Si or a transition metal; and a solvent in which the borohydride compound is soluble; (b) grinding a mixture formed in step (a) to form the borohydride compound; and (c) separating a solution comprising the borohydride compound.

7. 发明授权

US07297316B2 Process for production of a borohydride compound 失效
标题翻译：硼氢化合物的制备方法
公开(公告)号：US07297316B2
公开(公告)日：2007-11-20
申请号：US11098734
申请日：2005-04-04
申请人： Arthur Achhing Chin
发明人： Arthur Achhing Chin
IPC分类号： C01B35/00
CPC分类号： C01B6/17 , C01B6/21 , C01B6/23
摘要： A process for production of a borohydride compound. The process comprises the steps of: (a) combining a boron-containing salt, at least one of a metal and its hydride; wherein the metal is Be, Mg, Ca, Sr, Ba, Al, Ga, Si or a transition metal; and a solvent in which the borohydride compound is soluble; (b) grinding a mixture formed in step (a) to form the borohydride compound; and (c) separating a solution comprising the borohydride compound.
摘要翻译：硼氢化合物的制造方法。该方法包括以下步骤：（a）将含硼盐，金属和其氢化物中的至少一种合并; 其中所述金属为Be，Mg，Ca，Sr，Ba，Al，Ga，Si或过渡金属; 和硼氢化合物可溶的溶剂; （b）研磨步骤（a）中形成的混合物以形成硼氢化合物; 和（c）分离包含硼氢化合物的溶液。

8. 发明授权

US08802051B2 Process for production of a metal hydride 有权
标题翻译：金属氢化物的制备方法
公开(公告)号：US08802051B2
公开(公告)日：2014-08-12
申请号：US13053350
申请日：2011-03-22
申请人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
发明人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
IPC分类号： C01B6/04
CPC分类号： C01B6/04
摘要： A process for production of a metal hydride compound MHx, wherein x is one or two and M is an alkali metal, Be or Mg. The process comprises combining a compound of formula (R1O)xM with aluminum, hydrogen and at least one metal selected from among titanium, zirconium, hafnium, niobium, vanadium, tantalum and iron to produce a compound of formula MHx. R1 is phenyl or phenyl substituted by at least one alkyl or alkoxy group. A mole ratio of aluminum to (R1O)xM is from 0.1:1 to 1:1. The catalyst is present at a level of at least 200 ppm based on weight of aluminum.
摘要翻译：一种制备金属氢化物化合物MHx的方法，其中x为一个或两个，M为碱金属Be或Mg。该方法包括将式（R1O）xM化合物与铝，氢和至少一种选自钛，锆，铪，铌，钒，钽和铁的金属组合以制备式MHx的化合物。 R 1是被至少一个烷基或烷氧基取代的苯基或苯基。铝与（R1O）xM的摩尔比为0.1:1至1:1。以铝的重量计，催化剂的含量至少为200ppm。

9. 发明授权

US08501137B2 Process for production of an aluminum hydride compound 失效
标题翻译：氢化铝化合物的制备方法
公开(公告)号：US08501137B2
公开(公告)日：2013-08-06
申请号：US13053356
申请日：2011-03-22
申请人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
发明人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
IPC分类号： C01B35/00 , C07F5/06
CPC分类号： C07F5/069
摘要： A compound of formula M(AlH3OR1)y, wherein R1 is phenyl substituted by at least one of: (i) an alkoxy group having from one to six carbon atoms; and (ii) an alkyl group having from three to twelve carbon atoms; wherein M is an alkali metal, Be or Mg; and y is one or two.
摘要翻译：式M（AlH 3 OR 1）y的化合物，其中R 1为被以下至少一种取代的苯基：（i）具有1至6个碳原子的烷氧基; 和（ii）具有3至12个碳原子的烷基; 其中M为碱金属，Be或Mg; 而y是一两个。

10. 发明申请

US20110236287A1 PROCESS FOR PRODUCTION OF AN ALUMINUM HYDRIDE COMPOUND 失效
标题翻译：生产氢化铝化合物的方法
公开(公告)号：US20110236287A1
公开(公告)日：2011-09-29
申请号：US13053356
申请日：2011-03-22
申请人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
发明人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
IPC分类号： C01B6/21 , C07F5/06
CPC分类号： C07F5/069
摘要： A compound of formula M(AlH3OR1)y, wherein R1 is phenyl substituted by at least one of: (i) an alkoxy group having from one to six carbon atoms; and (ii) an alkyl group having from three to twelve carbon atoms; wherein M is an alkali metal, Be or Mg; and y is one or two.
摘要翻译：式M（AlH 3 OR 1）y的化合物，其中R 1为被以下至少一种取代的苯基：（i）具有1至6个碳原子的烷氧基; 和（ii）具有3至12个碳原子的烷基; 其中M为碱金属，Be或Mg; 而y是一两个。

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