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81. 发明授权

US6136996A Catalysts for polycondensation and redistribution of organosiloxane polymers 失效
标题翻译：有机硅氧烷聚合物的缩聚和再分布的催化剂
公开(公告)号：US6136996A
公开(公告)日：2000-10-24
申请号：US573218
申请日：1995-12-13
申请人： Slawomir Rubinsztajn , Patricia P. Anderson , Dennis P. Thompson
发明人： Slawomir Rubinsztajn , Patricia P. Anderson , Dennis P. Thompson
IPC分类号： C07F7/08 , C08G77/08 , C08G77/10 , C08G77/395 , C08G79/02
CPC分类号： C08G77/395 , C08G77/08 , C08G77/10
摘要： A mixture of a short chain linear phosphazene having the formula:X.sub.3-p (HO).sub.p P(NPX2).sub.m NP(O)X.sub.2,where X is a halogen selected from the group consisting of F, Cl, Br, and I, and m is an integer ranging from 0 to 6 and p is 0 or 1; anda linear sifoxane having a viscosity ranging from 1 to 5,000 centistokes is a catalyst for the polymerization, condensation, or redistribution of siloxanes; the process of making the catalyst and the process of using the catalyst.
摘要翻译：具有下式的短链线性磷腈的混合物：X3-p（HO）pP（NPX2）mNP（O）X2，其中X是选自F，Cl，Br和I的卤素，m 为0〜6的整数，p为0或1; 并且粘度范围为1至5,000厘沲的线性硅氧烷是用于硅氧烷的聚合，缩合或再分布的催化剂; 制备催化剂的方法和使用催化剂的方法。

82. 发明授权

US6040366A Liquid injection molding silicone elastomers having primerless adhesion 失效
标题翻译：液体注塑硅酮弹性体具有无底漆粘合力
公开(公告)号：US6040366A
公开(公告)日：2000-03-21
申请号：US32461
申请日：1998-02-27
申请人： Frank S. Burkus, II , Edward M. Jeram , Slawomir Rubinsztajn
发明人： Frank S. Burkus, II , Edward M. Jeram , Slawomir Rubinsztajn
IPC分类号： C08K5/11 , C08K5/19 , C08K5/34 , C08K5/5419 , C08L83/04 , C08L83/05 , C08L83/07
CPC分类号： C08K5/5419 , C08K5/19 , C08L83/04 , C08G77/045 , C08G77/12 , C08G77/16 , C08G77/20
摘要： The compression set of elastomeric silicone compositions, addition cured injection moldable compositions, is reduced by the incorporation of nitrogen compounds wherein the nitrogen possesses at least one organic substituent and the nitrogen is tetravalent wherein the nitrogen is cationic. The adhesion of such compositions to thermoset or thermoplastic polymer substrates is improved by the addition of bis(trimethoxysilylpropyl)fumarate and a disilanol that may or may not contain alkenyl groups. The lubricity of such compositions is improved by the addition of compounds selected from the group consisting of diorganosiloxanes such as polydimethylsiloxanes, phenyl containing siloxanes such as copolymers of diphenylsiloxane with diorganosiloxanes and copolymers of methylphenylsiloxane with diorganosiloxanes, fluorosilicones such as silicones containing trifluoropropyl substituted siloxanes, polydimethylsiloxanes, aliphatic and aromatic hydrocarbons that are liquid between 0.degree. C. and 100.degree. C. without adversely affecting the adhesion of the composition.
摘要翻译：弹性体硅氧烷组合物的加压固化可注射成型组合物通过引入氮化合物而被还原，其中氮具有至少一个有机取代基，氮是四价的，其中氮是阳离子的。通过加入富马酸双（三甲氧基甲硅烷基丙基）酯和可以含有烯基的二硅烷醇，可以改善这些组合物对热固性或热塑性聚合物基材的粘合性。通过添加选自二有机硅氧烷如聚二甲基硅氧烷，含苯基硅氧烷的苯基，例如二苯基硅氧烷与二有机硅氧烷的共聚物和甲基苯基硅氧烷与二有机硅氧烷的共聚物，氟硅氧烷如含有三氟丙基取代的硅氧烷的硅氧烷，聚二甲基硅氧烷，，在0℃至100℃之间为液体的脂族和芳族烃，而不会对组合物的粘附性产生不利影响。

83. 发明授权

US05998516A Liquid injection molding silcone elastomers having low compression set 失效
标题翻译：具有低压缩永久变形的液体注塑硅橡胶弹性体
公开(公告)号：US05998516A
公开(公告)日：1999-12-07
申请号：US999475
申请日：1997-12-29
申请人： Frank S. Burkus, II , Edward M. Jeram , Slawomir Rubinsztajn
发明人： Frank S. Burkus, II , Edward M. Jeram , Slawomir Rubinsztajn
IPC分类号： C08K5/17 , C08K5/19 , C08K5/3432 , C08K5/5419 , C08L83/04 , C08L83/05 , C08L83/07 , C08J5/16 , C08J5/17
CPC分类号： C08K5/19 , C08L83/04 , B29K2083/005 , C08G77/12 , C08G77/20
摘要： The compression set of elastomeric silicone compositions, addition cured injection moldable compositions or millable compositions, is reduced by the incorporation of nitrogen compounds wherein the nitrogen possesses at least one organic substituent and the nitrogen is tetravalent wherein the nitrogen is cationic.
摘要翻译：弹性体硅氧烷组合物的压缩组合，加入固化的可注射成型组合物或可碾碎组合物通过引入氮化合物而被还原，其中氮具有至少一个有机取代基，氮是四价的，其中氮是阳离子的。

84. 发明授权

US5998515A Liquid injection molding silicone elastomers having primerless adhesion 失效
标题翻译：液体注塑硅酮弹性体具有无底漆粘合力
公开(公告)号：US5998515A
公开(公告)日：1999-12-07
申请号：US999474
申请日：1997-12-29
申请人： Frank S. Burkus, II , Edward M. Jeram , Slawomir Rubinsztajn
发明人： Frank S. Burkus, II , Edward M. Jeram , Slawomir Rubinsztajn
IPC分类号： C08K5/19 , C08K5/3432 , C08K5/5419 , C08K5/5425 , C08L83/04 , C08L83/05 , C08L83/07 , C08K5/34
CPC分类号： C08K5/5425 , C08K5/19 , C08K5/3432 , C08L83/04 , C08G77/12 , C08G77/16 , C08G77/20
摘要： The compression set of elastomeric silicone compositions, addition cured injection moldable compositions or millable compositions, is reduced by the incorporation of nitrogen compounds wherein the nitrogen possesses at least one organic substituent and the nitrogen is tetravalent wherein the nitrogen is cationic. The adhesion of such compositions to thermoset or thermoplastic polymer substrates is improved by the addition of bis(trimethoxysilylpropyl)fumarate and a disilanol that may or may not contain alkenyl groups.
摘要翻译：弹性体硅氧烷组合物的压缩组合，加入固化的可注射成型组合物或可碾碎组合物通过引入氮化合物而被还原，其中氮具有至少一个有机取代基，氮是四价的，其中氮是阳离子的。通过加入富马酸双（三甲氧基甲硅烷基丙基）酯和可以含有烯基的二硅烷醇，可以改善这些组合物对热固性或热塑性聚合物基材的粘合性。

85. 发明授权

US5905150A Process for preparing organosilanes 失效
标题翻译：制备有机硅烷的方法
公开(公告)号：US5905150A
公开(公告)日：1999-05-18
申请号：US917968
申请日：1997-08-27
申请人： Amy Kathleen Simonian , Jimmy Lynn Webb , Daniel Joseph Brunelle , Timothy Edward Banach , Slawomir Rubinsztajn
发明人： Amy Kathleen Simonian , Jimmy Lynn Webb , Daniel Joseph Brunelle , Timothy Edward Banach , Slawomir Rubinsztajn
IPC分类号： B01J31/02 , C07B61/00 , C07F7/02 , C07F7/10 , C07F7/18 , C07D251/00 , C07F7/04 , C07F7/08
CPC分类号： C07F7/025 , C07F7/1892
摘要： An improved process for preparing a nitrogen or oxygen containing organoalkoxysilane such as an isocyanurate or fumarate by reacting a haloalkylaikoxysilane such as a chloropropytrimethoxysilane and a reactant of either a cyanate or an ammonium salt of an organic acid of C1-C20 carbon atoms or a metal salt of an organic acid of C1-C20 carbon atoms or mixtures thereof to a reaction temperature of at least about 80.degree. C. to about 200.degree. C., the improvement is in carrying out the reaction in the presence of a guanidinium salt phase as a transfer catalyst such as hexaethylguanidinium chloride. The improved process also is reacted wherein the temperature increase from the exotherm reaction above the reaction temperature ranges from about 0.degree. C. to about 120.degree. C. A preferred metal cyanate is sodium cyanate.
摘要翻译：通过使卤代烷基烷氧基硅烷如氯丙基三甲氧基硅烷和C1-C20碳原子的有机酸的氰酸酯或铵盐的反应物或金属盐反应来制备含氮或氧的有机烷氧基硅烷如异氰脲酸酯或富马酸盐的改进方法的C1-C20碳原子的有机酸或其混合物，反应温度为至少约80℃至约200℃，其改进在于在胍盐相存在下进行反应，为转移催化剂如六乙基氯化胍。改进的方法也被反应，其中在反应温度以上的放热反应的温度升高范围为约0℃至约120℃。优选的金属氰酸酯是氰酸钠。

86. 发明授权

US5639840A Fluoride ion releasing dental materials 失效
标题翻译：氟离子释放牙科材料
公开(公告)号：US5639840A
公开(公告)日：1997-06-17
申请号：US378657
申请日：1995-01-26
申请人： Wilmer K. Fife , Martel Zeldin , Slawomir Rubinsztajn
发明人： Wilmer K. Fife , Martel Zeldin , Slawomir Rubinsztajn
IPC分类号： A61K6/083 , C07C233/38 , C08F220/60 , C08F20/60 , C07C237/16
CPC分类号： A61K6/083 , C07C233/38 , C08F220/60
摘要： Described are novel fluoride ion-releasing acrylic or methacrylic acid-based monomers, fluoride ion-releasing dental resin materials prepared from the monomers, and processes for preparing the monomers and dental resin materials. The monomers of the invention are prepared in good yield from readily available starting materials. Dental resin materials of the invention exhibit excellent sustained fluoride ion release.
摘要翻译：描述了由单体制备的新型氟离子释放丙烯酸或甲基丙烯酸基单体，氟化物离子释放牙科树脂材料，以及制备单体和牙科树脂材料的方法。本发明的单体以容易获得的原料以良好的产率制备。本发明的牙科树脂材料表现出优异的持续氟离子释放。

87. 发明授权

US5403909A Catalysts for polycondensation and redistribution of organosiloxane polymers 失效
标题翻译：有机硅氧烷聚合物的缩聚和再分布的催化剂
公开(公告)号：US5403909A
公开(公告)日：1995-04-04
申请号：US91900
申请日：1993-07-15
申请人： Slawomir Rubinsztajn
发明人： Slawomir Rubinsztajn
IPC分类号： C07F9/26 , B01J27/14 , B01J27/24 , C01B21/098 , C07F9/06 , C08G77/06 , C08G77/08 , C08G77/10 , C07K7/10 , B01J31/18
CPC分类号： C08G77/08 , B01J27/14 , B01J27/24 , C01B21/098 , C01B21/0986 , C07F9/067
摘要： Short-chain linear phosphazenes as well as products of their reactions with water, alcohols and organosiloxanes, and the like, are active catalysts for polycondensation and redistribution of organosiloxane polymers.
摘要翻译：短链线性磷腈及其与水，醇和有机硅氧烷等的反应产物是有机硅氧烷聚合物的缩聚和再分布的活性催化剂。

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