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61. 发明申请

US20080004366A1 ORGANIC TELLURIUM COMPOUND, PROCESS FOR PRODUCING THE SAME, LIVING RADICAL POLYMERIZATION INITIATOR, PROCESS FOR PRODUCING POLYMER WITH THE SAME, AND POLYMER 有权
标题翻译：有机金属化合物，其制造方法，生物聚合反应产物，与其制备聚合物的方法和聚合物
公开(公告)号：US20080004366A1
公开(公告)日：2008-01-03
申请号：US11878901
申请日：2007-07-27
申请人： Shigeru Yamago , Junichi Yoshida
发明人： Shigeru Yamago , Junichi Yoshida
IPC分类号： C07C395/00 , C08F2/46
CPC分类号： C07C395/00 , C08F4/00 , C08F4/72 , C08F112/08 , C08F112/12 , C08F257/00 , C08F293/005 , C08F297/00 , C08F2438/00 , C08F220/18
摘要： An organotellurium compound of the formula (1) is useful as a living radical polymerization initiator and makes possible precision control of molecular weights and molecular weight distributions under mild conditions wherein R1 is C1-C8 alkyl, R2 and R3 are each a hydrogen atom or C1-C8 alkyl, and R4 is aryl, substituted aryl, aromatic heterocyclic group, hydroxycarbonyl or cyano.
摘要翻译：式（1）的有机碲化合物可用作活性自由基聚合引发剂，并且在温和条件下可以精确控制分子量和分子量分布，其中R 1是C 1〜 C 1 -C 8烷基，R 2和R 3各自为氢原子或C 1 -C 3烷基， R 4是烷基，R 4是芳基，取代的芳基，芳族杂环基，羟基羰基或氰基。

62. 发明授权

US07297819B2 Open-chain alkoxyamines and their corresponding nitroxides for controlled low temperature radical polymerization 失效
标题翻译：开链烷氧基胺及其相应的氮氧化物用于控制低温自由基聚合
公开(公告)号：US07297819B2
公开(公告)日：2007-11-20
申请号：US10506700
申请日：2003-02-25
申请人： Tobias Hintermann , Peter Nesvadba , Andreas Kramer , Jochen Fink
发明人： Tobias Hintermann , Peter Nesvadba , Andreas Kramer , Jochen Fink
IPC分类号： C07C239/20 , C07D265/32 , C07D265/34 , C08F4/00
CPC分类号： C08F4/00
摘要： The present invention relates to open chain alkoxyamine compounds, a polymerizable composition comprising a) at least one ethylenically unsaturated monomer and b) at least one open chain alkoxyamine compound. Further aspects of the present invention are a process for polymerizing ethylenically unsaturated monomers, and the use of open chain alkoxyamine compounds for controlled polymerization. The intermediate N-oxyl derivatives, a composition of the N-oxyl derivatives with ethylenically unsaturated monomers and a free radical initiator X, as well as a process and their use for polymerization are also subjects of the present invention.
摘要翻译：本发明涉及开链烷氧基胺化合物，可聚合组合物，其包含a）至少一种烯键式不饱和单体和b）至少一种开链烷氧基胺化合物。本发明的另外的方面是用于聚合烯键式不饱和单体的方法，以及使用开链烷氧基胺化合物用于受控聚合。中间体N-氧基衍生物，具有烯键式不饱和单体的N-氧基衍生物和自由基引发剂X的组合物以及其聚合的方法和用途也是本发明的主题。

63. 发明授权

US07294686B2 Polymerization of aromatic monomers using derivatives of hematin 失效
公开(公告)号：US07294686B2
公开(公告)日：2007-11-13
申请号：US11337964
申请日：2006-01-23
申请人： Susan Tripathy, legal representative , Lynne A. Samuelson , Ferdinando F. Bruno , Sucharita Roy , Ramaswamy Nagarajan , Jayant Kumar , Bon-Cheol Ku , Soo-Hyoung Lee
发明人： Sukant Tripathy, deceased
IPC分类号： C08G73/06 , C08F2/04 , C08F4/26
CPC分类号： C07D487/22 , B01J31/1815 , B01J2231/14 , B01J2531/025 , B01J2531/842 , B82Y30/00 , C08F4/00 , C08G73/0266 , C08L25/18 , Y10T428/12861 , Y10T428/12951 , Y10T428/12958
摘要： Hematin, a hydroxyferriprotoporphyrin, is derivatized with one or more non-proteinaceous amphipathic groups. The derivatized hematin can serve as a mimic of horseradish peroxidase in polymerizing aromatic monomers, such as aromatic compounds. These derivatized hematins can also be used as catalysts in polymerizing aromatic monomers, and can exhibit significantly greater catalytic activity than underivatized hematin in acidic solutions. In one embodiment, polymerization is in the presence of a template, along which aromatic monomers align. An assembled hematin includes alternating layers of hematin and a polyelectrolyte, which are deposited on an electrically charged substrate. Assembled hematin can also be used to polymerize aromatic monomers.

64. 发明授权

US07235663B2 N-alkoxy-4,4-dioxy-polyalkyl-piperidines as radical polymerization inhibitors 失效
标题翻译： N-烷氧基-4,4-二氧基 - 多烷基 - 哌啶作为自由基聚合抑制剂
公开(公告)号：US07235663B2
公开(公告)日：2007-06-26
申请号：US10450227
申请日：2001-11-12
申请人： Francesco Fuso , Wiebke Wunderlich , Andreas Kramer , Jochen Fink
发明人： Francesco Fuso , Wiebke Wunderlich , Andreas Kramer , Jochen Fink
IPC分类号： C07D319/10 , C07D323/04 , C08F4/00 , C08F2/16 , C08K5/3492
CPC分类号： C07D405/12 , C07D211/94 , C07D491/10 , C08F4/00
摘要： The present invention relates to selected glycidyl or carbonyl functional N-alkoxy-4,4-dioxy-polyalkyl-piperidine compounds forming an open chain or cyclic ketal structure, a polymerizable composition comprising a) at least one ethylenically unsaturated monomer and b) a glycidyl or carbonyl functional N-alkoxy-4,4-dioxy-polyalkyl-piperidine nitroxide initiator compound. Further aspects of the present invention are a process for polymerizing ethylenically unsaturated monomers and the use of glycidyl or carbonyl functional N-alkoxy-4,4-dioxy-polyalkyl-piperidine nitroxide initiators for radical polymerization.
摘要翻译：本发明涉及形成开链或环状缩酮结构的选择的缩水甘油基或羰基官能的N-烷氧基-4,4-二氧基 - 多烷基 - 哌啶化合物，可聚合组合物，其包含a）至少一种烯属不饱和单体和b）缩水甘油基或羰基官能的N-烷氧基-4,4-二氧基 - 多烷基 - 哌啶氮氧根引发剂化合物。本发明的另外的方面是用于使烯键式不饱和单体聚合的方法和使用缩水甘油基或羰基官能的N-烷氧基-4,4-二氧基 - 多烷基 - 哌啶氮氧根引发剂进行自由基聚合。

65. 发明授权

US07230071B1 Methods for polymerization of electronic and photonic polymers 失效
公开(公告)号：US07230071B1
公开(公告)日：2007-06-12
申请号：US10775580
申请日：2004-02-09
申请人： Ferdinando Bruno , Lynne A. Samuelson , Ramaswamy Nagarajan , Jayant Kumar
发明人： Ferdinando Bruno , Lynne A. Samuelson , Ramaswamy Nagarajan , Jayant Kumar
IPC分类号： C08G73/06
CPC分类号： C07D487/22 , C08F4/00
摘要： A method for polymerizing electronic and photonic polymers, wherein an aromatic monomer is combined with a hematin catalyst derivatized with at least one non-proteinaceous amphipathic group, and a peroxide initiator, and employing a template, wherein the aromatic monomer aligns along the template and polymerizes to form a complex comprising the polymerized monomer and the template.

66. 发明授权

US07186791B2 Methods for polymerization of electronic and photonic polymers 失效
公开(公告)号：US07186791B2
公开(公告)日：2007-03-06
申请号：US11120031
申请日：2005-05-02
申请人： Ferdinando Bruno , Lynne A. Samuelson , Ramaswamy Nagarajan , Jayant Kumar
发明人： Ferdinando Bruno , Lynne A. Samuelson , Ramaswamy Nagarajan , Jayant Kumar
IPC分类号： C08G73/66
CPC分类号： C07D487/22 , C08F4/00
摘要： A method for polymerizing electronic and photonic polymers, wherein an aromatic monomer is combined with a hematin catalyst derivatized with at least one non-proteinaceous amphipathic group, and a peroxide initiator, and employing a template, wherein the aromatic monomer aligns along the template and polymerizes to form a complex comprising the polymerized monomer and the template.

67. 发明申请

US20070043141A1 Free-radical initiator systems containing enzymes, compositions, and methods 审中-公开
标题翻译：含有酶，组合物和方法的自由基引发剂体系
公开(公告)号：US20070043141A1
公开(公告)日：2007-02-22
申请号：US11586947
申请日：2006-10-26
申请人： Dong Wu , Joel Oxman
发明人： Dong Wu , Joel Oxman
IPC分类号： A61K6/083
CPC分类号： C08F4/00 , A61K6/005 , C08F4/40 , A61K6/083 , C08L33/08 , C08L33/10 , C08L33/26 , A61K6/0017
摘要： A free-radical initiator system that includes a combination of an oxidase enzyme, a peroxidase coenzyme, an oxidase substrate, and a reductant (i.e., reducing agent). This system can be used with a resin system that includes a polymerizable component.
摘要翻译：包含氧化酶，过氧化物酶辅酶，氧化酶底物和还原剂（还原剂）的组合的自由基引发剂体系。该系统可以与包含可聚合组分的树脂体系一起使用。

68. 发明申请

US20070010632A1 Antioxidant-functionalized polymers 审中-公开
标题翻译：抗氧化官能化聚合物
公开(公告)号：US20070010632A1
公开(公告)日：2007-01-11
申请号：US10536810
申请日：2003-11-26
申请人： David Kaplan , Amarjit Singh
发明人： David Kaplan , Amarjit Singh
IPC分类号： C08L63/00
CPC分类号： A61L29/16 , A61K47/58 , A61K47/59 , A61K47/593 , A61K47/6957 , A61L17/005 , A61L27/34 , A61L27/54 , A61L31/16 , A61L2300/40 , A61L2300/428 , A61L2300/442 , A61L2300/604 , C07D307/62 , C08F4/00 , C08F12/22 , C08F112/14 , C08F112/32 , C08F220/14 , C08G63/08 , C08G64/30 , C08G65/44 , C08G2650/64 , C08K5/005 , C08L71/126 , C12P7/62 , C12P17/04
摘要： Methods and compositions are disclosed for the preparation of free radical scavenging polymers and polymer films functionalized with antioxidants. Enzymatic and chemical tailoring of monomers with antioxidants followed by enzymatic polymerization is described. These antioxidant functionalized polymers can increase shelf life and quality of food products, as well as, increase effectiveness of pharmaceutical agents when used as packaging or as coatings on packaging for oxygen sensitive materials. The novel enzymatic covalent coupling of antioxidants to a polymer enhances the free radical scavenging ability of packaging while also inhibiting the escape of the antioxidants, and thus limiting exposure and/or absorption by an individual. In addition to its use in food or pharmaceutical packaging, methods are disclosed for using the antioxidant coupled polymers in a variety of applications including as coatings on the inside of medical devices, such as stents and catheters, which would substantially reduce free radical damage and/or oxygen depletion during medical procedures. Furthermore, through the coupling of antioxidants to biodegradable polymers, controlled delivery and sustained release of an antioxidant to a subject is possible.
摘要翻译：公开了用于制备自由基清除聚合物和用抗氧化剂官能化的聚合物膜的方法和组合物。描述了具有抗氧化剂的单体的酶和化学定制，然后进行酶促聚合。这些抗氧化剂官能化聚合物可以提高食品的保质期和质量，并且当用作包装或作为氧敏感材料的包装上的涂料时，可提高药剂的有效性。抗氧化剂与聚合物的新型酶共价偶联增强了包装的自由基清除能力，同时还抑制抗氧化剂的逸出，从而限制个体的暴露和/或吸收。除了在食品或药物包装中的使用之外，公开了在各种应用中使用抗氧化剂偶联聚合物的方法，包括作为医疗装置内部的涂层，例如支架和导管，其将显着降低自由基损伤和/ 或氧气耗尽。此外，通过将抗氧化剂与可生物降解的聚合物的偶联，可以控制抗氧化剂向受试者的递送和持续释放。

69. 发明授权

US07157537B2 α-Halogenated acid esters with polyvalent alcohols as atom transfer radical polymerization initiators 有权
标题翻译： α-卤代酸酯与多元醇作为原子转移自由基聚合引发剂
公开(公告)号：US07157537B2
公开(公告)日：2007-01-02
申请号：US10787676
申请日：2004-02-26
申请人： Andreas Mühlebach , François Rime
发明人： Andreas Mühlebach , François Rime
IPC分类号： C08F118/02
CPC分类号： C08F293/005 , C07C69/63 , C08F4/00 , C08F8/30 , C08F2438/01 , C08F293/00
摘要： The invention relates to α-halocarboxylic acid esters of polyhydric, at least trihydric, alcohols, which can be used as initiators for ATRP. Using those initiators it is possible to prepare block copolymers having branched structures.
摘要翻译：本发明涉及可用作ATRP引发剂的多元醇，至少三元醇的α-卤代羧酸酯。使用这些引发剂可以制备具有支链结构的嵌段共聚物。

70. 发明申请

US20060287451A1 Composition and process for the controlled synthesis of block copolymers 失效
公开(公告)号：US20060287451A1
公开(公告)日：2006-12-21
申请号：US10568376
申请日：2004-08-18
申请人： Hendrik Wermter , Dirk Simon , Rudolf Pfaendner
发明人： Hendrik Wermter , Dirk Simon , Rudolf Pfaendner
IPC分类号： C08F4/00
CPC分类号： C08L51/003 , C08F4/00 , C08F291/00 , C08F293/005 , C08K5/32 , C08L53/00 , C08L2666/02
摘要： The present invention relates to a polymerizable composition comprising a) at least one ethylenically unsaturated monomer and b) at least one hydroxylamine of high molecular weight, preferably a long chain alkyl substituted hydroxylamine. Further aspects of the present invention are a process for polymerizing ethylenically unsaturated monomers, and the use of high molecular weight hydroxylamines for controlled polymerization.

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