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61. 发明申请

US20140127145A1 Heat Treated Precipitated Silica 审中-公开
标题翻译：热处理沉淀二氧化硅
公开(公告)号：US20140127145A1
公开(公告)日：2014-05-08
申请号：US14070774
申请日：2013-11-04
申请人： The Procter & Gamble Company
发明人： George Endel Deckner , Lawrence Edward Dolan
IPC分类号： A61K8/25 , A61K8/55 , A61Q11/00 , C01B33/12
CPC分类号： A61K8/25 , A61K8/0241 , A61K8/044 , A61K8/21 , A61K2800/28 , A61K2800/412 , A61K2800/592 , A61Q11/00 , C01B33/18
摘要： Process for heat treating precipitated silica to improve stability. Oral care compositions comprising such heat treated precipitated silica abrasives and a stannous ion source.
摘要翻译：热处理沉淀二氧化硅以提高稳定性的方法。包含这种经热处理的沉淀二氧化硅研磨剂和亚锡离子源的口腔护理组合物。

62. 发明申请

US20140030180A1 MANUFACTURE OF CRYSTALLITE PARTICLES 有权
标题翻译：晶体颗粒的制造
公开(公告)号：US20140030180A1
公开(公告)日：2014-01-30
申请号：US13825454
申请日：2011-09-21
申请人： Magnus Odén , Emma Björk
发明人： Magnus Odén , Emma Björk
IPC分类号： C01B37/02 , A61K47/02
CPC分类号： C01B37/02 , A61K47/02 , B32B3/263 , B44C1/227 , B82Y30/00 , B82Y40/00 , C01B33/18 , C01B33/187 , C01B33/193 , C01P2002/01 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C01P2004/64 , C01P2006/16 , Y10T428/24479
摘要： A method for the manufacture of crystallite particles, said method comprising the steps of: a) reacting a reaction solution comprising a silicate, a micelle forming agent, an alkane, a salt under stirring at pH 2 or lower, wherein the reaction solution comprises HCI in a concentration of at least 1.5 M, wherein the stirring is performed not more than 10 minutes, and b) treating the obtained material to remove the micelle forming agent with one method selected from i) heat treating the material above 300° C., ii) treating the material with at least one selected from H2O2, and H2SO4, iii) treating the material with microwaves to digest the micelle forming agent. An advantage is that the time for the synthesis is shortened considerably compared to the prior art.
摘要翻译：一种制造微晶颗粒的方法，所述方法包括以下步骤：a）在pH2或更低的搅拌下使包含硅酸盐，胶束形成剂，烷烃，盐的反应溶液反应，其中反应溶液包含HCl 浓度至少为1.5M，其中搅拌不超过10分钟，b）用一种方法处理所得材料以除去胶束形成剂，方法为i）在300℃以上进行热处理， ii）用选自H 2 O 2和H 2 SO 4中的至少一种处理该材料，iii）用微波处理该材料以消化胶束形成剂。优点在于与现有技术相比，缩短了合成时间。

63. 发明申请

US20140023907A1 DIATOMACEOUS ENERGY STORAGE DEVICES 有权
标题翻译：独立的能源存储设备
公开(公告)号：US20140023907A1
公开(公告)日：2014-01-23
申请号：US13944211
申请日：2013-07-17
申请人： NthDegree Technologies Worldwide Inc.
发明人： Vera N. Lockett , John G. Gustafson , Mark D. Lowenthal , William J. Ray
IPC分类号： H01G11/52 , H01M2/16
CPC分类号： C01B33/18 , B01D21/262 , B04B7/12 , H01G11/24 , H01G11/26 , H01G11/36 , H01G11/38 , H01G11/46 , H01G11/52 , H01M2/1646 , H01M4/62 , Y02E60/13
摘要： A printed energy storage device includes a first electrode, a second electrode, and a separator between the first and the second electrode. At least one of the first electrode, the second electrode, and the separator includes frustules, for example of diatoms. The frustules may have a uniform or substantially uniform property or attribute such as shape, dimension, and/or porosity. A property or attribute of the frustules can also be modified by applying or forming a surface modifying structure and/or material to a surface of the frustules. A membrane for an energy storage device includes frustules. An ink for a printed film includes frustules.
摘要翻译：印刷储能装置包括第一电极，第二电极和第一和第二电极之间的隔板。第一电极，第二电极和分离器中的至少一个包括例如硅藻的截头圆锥体。截头锥体可以具有均匀或基本均匀的性质或属性，例如形状，尺寸和/或孔隙率。还可以通过将表面改性结构和/或材料施加或形成到截头体的表面来改变截头体的属性或属性。用于能量存储装置的膜包括截头圆锥体。用于印刷膜的油墨包括截头圆锥体。

64. 发明申请

US20140011954A1 METHOD FOR PRODUCING POROUS SILICA PARTICLE, RESIN COMPOSITION FOR ANTIREFLECTION COATING, AND ARTICLE AND ANTIREFLECTION FILM HAVING ANTIREFLECTION COATING 审中-公开
标题翻译：用于生产多孔二氧化硅颗粒的方法，用于抗反射涂层的树脂组合物，以及具有抗反射涂层的制品和抗反射膜
公开(公告)号：US20140011954A1
公开(公告)日：2014-01-09
申请号：US13980358
申请日：2012-01-19
申请人： Hiroki Tokoro , Youzou Yamashina , Kiyofumi Takano , Tomoyo Shimogaki , Minoru Tabuchi , Tomoe Deguchi
发明人： Hiroki Tokoro , Youzou Yamashina , Kiyofumi Takano , Tomoyo Shimogaki , Minoru Tabuchi , Tomoe Deguchi
IPC分类号： C09D5/00
CPC分类号： C09D5/006 , C01B33/18 , C08K3/36 , C08K7/26 , C09D7/61 , C09D7/70
摘要： An object of the present invention is to provide a method for producing porous silica particles having a small particle diameter in high yield relative to a volume of a reaction solution. In order to achieve the object, the present invention provides a method for producing porous silica particles having pores on the surfaces thereof, the method including a step of adding a mixed solution (solution A) containing tetraalkoxysilane, alkylamine, and alcohol to a mixed solution (solution B) containing ammonia, alcohol, and water and performing a hydrolysis and condensation reaction of the tetraalkoxysilane to produce silica particles, and a step of removing the alkylamine from the silica particles.
摘要翻译：本发明的目的是提供相对于反应溶液的体积，以高产率生产具有小粒径的多孔二氧化硅颗粒的方法。为了达到上述目的，本发明提供一种在其表面具有孔的多孔二氧化硅粒子的制造方法，其特征在于，在混合溶液中添加含有四烷氧基硅烷，烷基胺和醇的混合溶液（溶液A）（溶液B），并进行四烷氧基硅烷的水解缩合反应生成二氧化硅粒子，以及从二氧化硅粒子除去烷基胺的工序。

65. 发明授权

US08623312B2 Process for producing dispersion of hollow fine SiO2 particles, coating composition and substrate with antireflection coating film 有权
标题翻译：中空微细SiO 2颗粒分散体，涂料组合物和基材与防反射涂膜的制备方法
公开(公告)号：US08623312B2
公开(公告)日：2014-01-07
申请号：US11939880
申请日：2007-11-14
申请人： Kawai Yohei , Yoneda Takashige
发明人： Kawai Yohei , Yoneda Takashige
IPC分类号： C01B33/12
CPC分类号： B82Y30/00 , C01B33/14 , C01B33/18 , C01P2004/34 , C01P2004/62 , C01P2004/64 , C09C1/0081 , C09C1/043 , C09C1/30 , G02B1/111 , G02B1/113 , Y10T428/24421 , Y10T428/2982 , Y10T428/2991
摘要： To provide a process for producing a dispersion of hollow fine SiO2 particles which contains no residual core fine particles, generates no uncontrollable agglomerates, and is easy to filtrate.A process for producing a dispersion of hollow fine SiO2 particles having hollow fine SiO2 particles dispersed in a dispersion medium, which comprises at least the following steps (a), (b) and (c): (a) a step of reacting a precursor of SiO2 at a pH higher than 8 in the presence of fine ZnO particles constituting the core in the dispersion medium to form SiO2, thereby to obtain a dispersion of fine particles comprising the fine ZnO particles covered with the formed SiO2; (b) a step of mixing an acidic cation exchange resin with the dispersion of fine particles obtained in the above step (a) to bring them into contact with each other, to dissolve the fine ZnO particles as the core at a pH within a range of from 2 to 8; and (c) a step of separating the acidic cation exchange resin by solid-liquid separation after the fine ZnO particles are completely dissolved, to obtain the dispersion of hollow fine SiO2 particles.
摘要翻译：为了提供不含有残留的核心微粒的中空微细SiO 2粒子的分散液的制造方法，不产生不可控的附聚物，容易滤液。一种制备分散在分散介质中的中空微细SiO 2颗粒的中空微细SiO 2分散体的方法，其至少包括以下步骤（a），（b）和（c）：（a）使前体的SiO 2在pH高于8的情况下，在构成分散介质中的核的细ZnO颗粒存在下形成SiO 2，从而获得包含被形成的SiO 2覆盖的ZnO微粒的细颗粒的分散体; （b）将酸性阳离子交换树脂与上述步骤（a）中得到的细颗粒分散体混合以使其彼此接触的步骤，将作为核的细ZnO颗粒溶解在一定范围内的pH 从2到8; 和（c）在完全溶解ZnO微粒子之后通过固液分离来分离酸性阳离子交换树脂的步骤，以获得中空微细SiO 2颗粒的分散体。

66. 发明授权

US08552189B2 Hybrid porous material and methods of preparing the same 有权
标题翻译：混合多孔材料及其制备方法
公开(公告)号：US08552189B2
公开(公告)日：2013-10-08
申请号：US12853460
申请日：2010-08-10
申请人： Kyo-sung Park , Seon-ah Jin , Hyun-chul Lee
发明人： Kyo-sung Park , Seon-ah Jin , Hyun-chul Lee
IPC分类号： C07F15/00 , C07F7/18 , C07F3/00 , C07F5/06
CPC分类号： C07F3/003 , C01B13/363 , C01B33/12 , C01B33/18 , C01B35/1009 , C01B35/1027 , C01P2002/72 , C01P2004/03
摘要： A hybrid porous material including at least a first and a second porous material portion which are chemically bonded to each other and are each a different type of material.
摘要翻译：一种混合多孔材料，其包括至少第一和第二多孔材料部分，其彼此化学键合并且各自是不同类型的材料。

67. 发明授权

US08529787B2 Colloidal silica containing silica secondary particles having bent structure and/or branched structure, and method for producing same 有权
标题翻译：含有具有弯曲结构和/或支化结构的二氧化硅二次粒子的胶体二氧化硅及其制造方法
公开(公告)号：US08529787B2
公开(公告)日：2013-09-10
申请号：US12998096
申请日：2009-09-01
申请人： Kazuaki Higuchi , Hideki Otsuki
发明人： Kazuaki Higuchi , Hideki Otsuki
IPC分类号： C09K13/00
CPC分类号： C09K3/1409 , C01B33/14 , C01B33/18 , C01B2202/02 , C01B2202/36
摘要： This invention provides a dense, high-purity colloidal silica containing silica secondary particles having a branched and/or bent structure, and a production method thereof. Specifically, this invention provides a method for producing a colloidal silica, comprising the steps of 1) preparing a mother liquid containing an alkali catalyst and water, and having a pH of 9 to 12; and 2) adding a hydrolysis liquid obtained by hydrolysis of an alkyl silicate to the mother liquid, wherein the step of adding the hydrolysis liquid to the mother liquid sequentially comprises A) step 1 of adding the hydrolysis liquid until the pH of the resulting liquid mixture becomes less than 7; B) step 2 of adding an aqueous alkali solution until the pH of the liquid mixture becomes 7 or more; and C) step 3 of adding the hydrolysis liquid while maintaining the pH of the liquid mixture at 7 or more, and a colloidal silica containing silica secondary particles having a branched and/or bent structure, obtained by this method.
摘要翻译：本发明提供一种含有分支和/或弯曲结构的二氧化硅二次颗粒的致密的高纯度胶体二氧化硅及其制备方法。具体而言，本发明提供一种胶体二氧化硅的制造方法，其特征在于，包括以下步骤：1）制备含有碱催化剂和水的母液，pH为9〜12; 和2）将通过水解硅酸烷基酯获得的水解液加入到母液中，其中依次将水解液加到母液中的步骤包括：A）加入水解液直到所得液体混合物的pH 变得小于7; B）添加碱性水溶液直至液体混合物的pH变为7以上为止的步骤2; 和C）在将液体混合物的pH保持在7以上的同时添加水解液的步骤3和通过该方法获得的含有分支和/或弯曲结构的二氧化硅二次粒子的胶体二氧化硅。

68. 发明授权

US08449856B2 Mesoporous silica particles 有权
标题翻译：介孔二氧化硅颗粒
公开(公告)号：US08449856B2
公开(公告)日：2013-05-28
申请号：US13241707
申请日：2011-09-23
申请人： Toshihiro Yano , Takuya Sawada
发明人： Toshihiro Yano , Takuya Sawada
IPC分类号： C01B33/12
CPC分类号： C01B37/02 , B01J20/103 , B01J20/28004 , B01J20/28021 , B01J20/28061 , B01J20/28064 , B01J20/28066 , B01J20/28083 , B01J20/3293 , B01J21/08 , B01J35/023 , B01J35/08 , B01J35/1023 , C01B33/18 , Y10S977/773 , Y10S977/775 , Y10S977/776 , Y10T428/2982
摘要： The present invention relates to (1) hollow silica particles including an outer shell portion having a mesoporous structure with an average pore size of from 1 to 10 nm, wherein the silica particles have an average particle diameter of from 0.05 to 10 μm, and 80% or more of the whole silica particles have a particle diameter falling within the range of ±30% of the average particle diameter; (2) composite silica particles including silica particles which include an outer shell portion having a mesoporous structure with an average pore size of from 1 to 10 nm, and have a BET specific surface area of 100 m2/g or more, and a hydrophobic organic compound or a polymeric organic compound incorporated inside of the silica particles; and a process for producing the hollow silica particles.
摘要翻译：本发明涉及（1）包含具有平均孔径为1〜10nm的介孔结构的外壳部的中空二氧化硅粒子，其中，二氧化硅粒子的平均粒径为0.05〜10μm，80 全部二氧化硅粒子的％以上的粒径在平均粒径的±30％的范围内; （2）包括二氧化硅颗粒的复合二氧化硅颗粒，其包括具有平均孔径为1至10nm的介孔结构的外壳部分，并且具有100m 2 / g以上的BET比表面积，以及疏水性有机物化合物或掺入二氧化硅颗粒内部的聚合有机化合物; 以及中空二氧化硅粒子的制造方法。

69. 发明申请

US20130068995A1 SILICA HAVING METAL IONS ABSORBED THEREON AND FABRICATING METHOD THEREOF 有权
标题翻译：具有吸收金属离子的二氧化硅及其制备方法
公开(公告)号：US20130068995A1
公开(公告)日：2013-03-21
申请号：US13615539
申请日：2012-09-13
申请人： Yun-Lung Ho , Song-Yuan Chang , Ming-Hui Lu , Chung-Wei Chiang
发明人： Yun-Lung Ho , Song-Yuan Chang , Ming-Hui Lu , Chung-Wei Chiang
IPC分类号： C09K13/00 , C01B33/00
CPC分类号： C01B33/12 , B82Y30/00 , C01B33/126 , C01B33/149 , C01B33/18 , C01P2002/72 , C01P2004/03 , C01P2004/62 , C01P2004/64 , C09K3/1436
摘要： A silica having metal ions absorbed thereon and a fabricating method thereof are provided. The silica having metal ions absorbed thereon is a silica having metal ions absorbed thereon and being modified with persulfate salt. The method includes following steps. A solution is provided, and the solution includes silica and persulfate salt therein. The solution is heated to react the silica with the persulfate salt, so as to obtain silica modified with persulfate salt. Metal ion source is added in the solution, the metal ion source dissociates metal ions, and the silica modified with persulfate salt absorbs the metal ions to obtain the silica having metal ions absorbed thereon.
摘要翻译：提供了吸收了金属离子的二氧化硅及其制造方法。其上吸附有金属离子的二氧化硅是金属离子被吸附在其上并用过硫酸盐改性的二氧化硅。该方法包括以下步骤。提供溶液，溶液中含有二氧化硅和过硫酸盐。将溶液加热以使二氧化硅与过硫酸盐反应，以获得用过硫酸盐改性的二氧化硅。在溶液中加入金属离子源，金属离子源解离金属离子，用过硫酸盐改性的二氧化硅吸收金属离子，得到吸附有金属离子的二氧化硅。

70. 发明申请

US20130052115A1 METHOD OF MANUFACTURING SPHERICAL MESOPOROUS SILICA CONTAINING DISPERSED SILVER NANOPATICLES, AND SPHERICAL MESOPOROUS SILICA MANUFACTURED BY SAID METHOD 有权
标题翻译：包含分散银纳米粒子的球形多孔二氧化硅的制备方法和通过方法制造的球形多孔二氧化硅
公开(公告)号：US20130052115A1
公开(公告)日：2013-02-28
申请号：US13640953
申请日：2010-10-13
申请人： Chung Kwon Park , Sang Cheol Han
发明人： Chung Kwon Park , Sang Cheol Han
IPC分类号： C01B33/20 , B82Y40/00 , B82Y30/00
CPC分类号： B01J20/28007 , B01J20/0233 , B01J20/103 , B01J20/28083 , B01J20/28097 , B01J20/3057 , B01J20/3085 , B82Y30/00 , C01B33/12 , C01B33/18 , C01P2002/72 , C01P2004/03 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C01P2006/12
摘要： The present invention relates to a method of preparing a spherical mesoporous silica structure containing silver nanoparticles dispersed therein by adding a silver nitrate solution to an aqueous surfactant solution and performing a sol-gel process and to spherical mesoporous silica prepared thereby. The spherical mesoporous silica is cost-effective compared to a conventional method that uses silver nanoparticles as a raw material, because the silver nitrate solution that is inexpensive compared to silver nanoparticles is used. Also, the spherical mesoporous silica can be with high productivity in large amounts, and thus is easily commercialized. Moreover, because silver nanoparticles are incorporated into the pores of the mesoporous silica, the silver nanoparticles are used stably and do not change color and odor. In addition, the spherical mesoporous silica exhibits various additional effects, including far-infrared ray emission and deodorization, attributable to silica.
摘要翻译：本发明涉及一种通过向表面活性剂水溶液中加入硝酸银溶液并进行溶胶 - 凝胶法制备其中分散有银纳米颗粒的球形介孔二氧化硅结构体和由其制备的球状介孔二氧化硅的方法。与使用银纳米颗粒作为原料的常规方法相比，使用球形介孔二氧化硅是成本有效的，因为使用与银纳米颗粒相比便宜的硝酸银溶液。此外，球状介孔二氧化硅可以大量高生产率，因此容易商业化。此外，由于银纳米颗粒结合到介孔二氧化硅的孔中，银纳米颗粒被稳定地使用并且不改变颜色和气味。此外，球状中孔二氧化硅表现出各种附加效果，包括由二氧化硅引起的远红外线发射和除臭。

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