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61. 发明授权

US06329555B1 Preparation of substituted butenes 失效
标题翻译：取代丁烯的制备
公开(公告)号：US06329555B1
公开(公告)日：2001-12-11
申请号：US09432202
申请日：1999-11-02
申请人： Maik Aron , Ralf Böhling , Peter Zehner
发明人： Maik Aron , Ralf Böhling , Peter Zehner
IPC分类号： C07C4106
CPC分类号： C07C41/06 , C07C45/513 , C07C47/02 , C07C43/046
摘要： Described is a process for preparing substituted butenes of the formula I and/or II, where the radical R is unsubstituted or mono- or di-C1-C10-alkoxy-substituted or mono- or dihydroxy-substituted C2-C20-alkyl or alkenyl or is C6-C10-aryl, C7-C11-aralkyl or methyl by reacting 1,3-butadiene with an alcohol of the formula ROH in which R is as defined in the presence of an acidic particulate catalyst insoluble in the reaction medium, which involves contacting the butadiene, the alcohol and the catalyst in a fluidized bed reactor which is flow-approached from below and is operated at above the loosening point.
摘要翻译：描述了制备式I和/或II的取代丁烯的方法，其中基团R是未取代的或单或二-C 1 -C 10 - 烷氧基取代的或单或二羟基取代的C 2 -C 20 - 烷基或烯基或者是C 13 -C 10 - 芳基，C 7 -C 11 - 芳烷基或甲基，通过使1,3-丁二烯与式ROH的醇反应，其中R在不溶于反应介质的酸性颗粒催化剂存在下如上所定义，其中R 包括在流化床反应器中使丁二烯，醇和催化剂接触，流化床反应器从下方流动接近并在松动点之上操作。

62. 发明授权

US06258281B1 Breaking down aromatic compounds in industrial wastewaters 有权
标题翻译：打破工业废水中的芳香族化合物
公开(公告)号：US06258281B1
公开(公告)日：2001-07-10
申请号：US09336722
申请日：1999-06-21
申请人： Edmund Niedbalski , Laurance Thurman , Irene Troetsch-Schaller , Ludwig Schuster , Dieter Voges , Peter Zehner , Klaus Bittins , Rudolf Schnur
发明人： Edmund Niedbalski , Laurance Thurman , Irene Troetsch-Schaller , Ludwig Schuster , Dieter Voges , Peter Zehner , Klaus Bittins , Rudolf Schnur
IPC分类号： C02F178
CPC分类号： C02F1/78 , Y10S210/909
摘要： A process for breaking down aromatics in industrial wastewaters that contain small amounts of aromatics by reaction with an ozone-containing oxygen stream at a temperature of from 40 to 70° C. and at a pH of from 4 to 7, involves treating industrial wastewaters that contain small amounts of aromatics in two stages with an oxygen stream that contains from 5 to 8% by volume of ozone with thorough mixing by causing the wastewater to flow upward through two reaction zones, the overflow of the wastewater at the top of the first reaction zone entering the second reaction zone at the base, the purified wastewater being obtained at the top of the second reaction zone, the ozone-containing oxygen stream first entering at the base of the second reaction zone, and the waste gas obtained at the top of the second reactor being introduced at the base of the first reaction zone, and, furthermore, a gas containing less than 0.2% by volume of ozone being obtained at the top of the first reaction zone.
摘要翻译：在-40〜70℃，pH4〜7的温度下，通过与含臭氧的氧气流反应而含有少量芳族化合物的工业废水中的芳族化合物的分解方法涉及处理工业废水，在两个阶段中含有少量芳烃，其中含有5-8％（体积）臭氧的氧气，通过使废水通过两个反应区向上流动而充分混合，第一反应顶部的废水溢出进入第二反应区的第二反应区的第二反应区的第二反应区的净化废水，在第二反应区的顶部得到的纯化废水，首先进入第二反应区的碱的含臭氧的氧流，第二反应器被引入第一反应区的底部，此外，在第一反应区的顶部获得含有小于0.2体积％的臭氧的气体。

63. 发明授权

US5401873A Preparation of methyl formate 失效
标题翻译：甲酸甲酯的制备
公开(公告)号：US5401873A
公开(公告)日：1995-03-28
申请号：US208823
申请日：1994-03-11
申请人： Peter Zehner , Klaus Bittins , Wilhelm Haarde , Ulrich Eiden , Dietrich Wolff , Manfred Herr , Leopold Hupfer
发明人： Peter Zehner , Klaus Bittins , Wilhelm Haarde , Ulrich Eiden , Dietrich Wolff , Manfred Herr , Leopold Hupfer
IPC分类号： B01J31/02 , C07B61/00 , C07C67/36 , C07C69/06
CPC分类号： C07C67/36
摘要： Preparation of methyl formate by the reaction of carbon monoxide and methanol under conditions of elevated pressure and temperature in the presence of an alkali metal methylate, in whichA) the starting materials are mixed in a mixing zone, are allowed to react partially, and the reaction solution is saturated with CO andB) the reaction is allowed to reach completion in one or more secondary reaction zones without the addition of further starting materials.
摘要翻译：在甲醇酸碱金属（其中A）原料在混合区中混合的条件下，通过一氧化碳和甲醇在升高的压力和温度条件下反应制备甲酸甲酯，使其部分反应，反应溶液用CO饱和，B）使反应在一个或多个次级反应区中达到完成，而不添加进一步的起始原料。

64. 发明授权

US4778929A Continuous hydroformylation of olefinically unsaturated compounds 失效
标题翻译：烯属不饱和化合物的连续加氢甲酰化
公开(公告)号：US4778929A
公开(公告)日：1988-10-18
申请号：US70963
申请日：1987-07-08
申请人： Peter Zehner , Herwig Hoffmann , Wolfgang Richter , Dieter Stuetzer , Max Strohmeyer , Helmut Walz , Erich Weippert
发明人： Peter Zehner , Herwig Hoffmann , Wolfgang Richter , Dieter Stuetzer , Max Strohmeyer , Helmut Walz , Erich Weippert
IPC分类号： C07B61/00 , B01J31/00 , C07C45/00 , C07C45/50 , C07C47/02 , C07C67/00
CPC分类号： C07C45/50
摘要： Olefinically unsaturated compounds are hydroformylated continuously, the olefin being passed into the lower region of the reactor, under from 1 to 40 bar and at from 50.degree. to 140.degree. C. with the aid of a rhodium complex as a catalyst in a hydroformylation reactor having a liquid reaction zone which occupies about 60-85% of the reactor volume, the gaseous products and reactants being removed from the hydroformylation reactor, the products being isolated and the major part of the remaining gas being recycled to the reactor by the cycle gas method, by a process in which from 20 to 80% by volume of the cycle gas is fed into the hydroformylation reactor above the liquid reaction zone and/or below the liquid surface in the top fourth of the liquid reaction zone.
摘要翻译：烯化不饱和化合物连续加氢甲酰化，在加氢甲酰化反应器中借助于铑络合物作为催化剂，将烯烃在1至40巴和50至140℃下进入反应器的下部区域，占反应器体积约60-85％的液体反应区，气态产物和反应物从加氢甲酰化反应器中除去，产物被分离，剩余气体的主要部分通过循环气体法再循环到反应器，其中循环气体的20至80体积％被输入到液体反应区上方的加氢甲酰化反应器和/或液体反应区顶部第四个液体表面下方的流程。

65. 发明授权

US4192856A Manufacture of hydroxylammonium salts 失效
标题翻译：羟基铵盐的制造
公开(公告)号：US4192856A
公开(公告)日：1980-03-11
申请号：US932636
申请日：1978-08-10
申请人： Guenther Rapp , Erwin Thomas , Dieter Wolf , Kuerten, Heribert , Peter Zehner
发明人： Guenther Rapp , Erwin Thomas , Dieter Wolf , Kuerten, Heribert , Peter Zehner
IPC分类号： B01J10/00 , B01J19/24 , B01J19/26 , B01J23/00 , C01B21/14
CPC分类号： C01B21/1418 , B01J19/2465 , B01J19/26 , B01J2219/00103 , B01J2219/0011 , B01J2219/00777
摘要： Hydroxylammonium salts are manufactured by a process comprising the catalytic reduction of nitric oxide with hydrogen in a dilute aqueous solution of a mineral acid in the presence of a suspended platinum catalyst at an elevated temperature, wherein the reaction mixture is recycled and the gas mixture, containing nitric oxide and hydrogen, present in the gas space above the reaction zone, is introduced, by means of one or more downwardly directed jets of liquid, consisting of the recycled reaction mixture and issuing from a nozzle orifice, into one or more circulation zones which are present in the reaction zone, are open at both sides, extend in the direction of the entering jet of liquid and are completely covered by the reaction mixture, the reaction mixture leaving the bottom of the circulation zone and containing unconverted gases is deflected, passed upwards in the annular zone externally surrounding the circulation zone, and at the same time reaction mixture of low gas content is recycled from a separation zone located under the reaction zone.
摘要翻译：羟基铵盐通过包括在悬浮的铂催化剂的存在下在升高的温度下在无机酸的稀的水溶液中用氢催化还原一氧化氮的方法制备，其中反应混合物被再循环，并且含有存在于反应区上方的气体空间中的一氧化氮和氢气通过一个或多个向下定向的液体喷射引入，由再循环的反应混合物组成并从喷嘴孔排出到一个或多个循环区存在于反应区中，在两侧开放，沿着进入的液体射流的方向延伸并被反应混合物完全覆盖，离开循环区底部并含有未转化气体的反应混合物偏转，通过向上在循环区域外部的环形区域中，同时反应混合低气体量i 从位于反应区下方的分离区回收。

66. 发明授权

US4019719A Fluid mixing device 失效
标题翻译：流体混合装置
公开(公告)号：US4019719A
公开(公告)日：1977-04-26
申请号：US672612
申请日：1976-04-01
申请人： Hans H. Schuster , Peter Zehner
发明人： Hans H. Schuster , Peter Zehner
IPC分类号： B01F5/00 , B01F5/06
CPC分类号： B01F5/0619 , B01F5/0617
摘要： An apparatus for thoroughly mixing components of fluid material and, more particularly, for combining and homogenizing streams of gaseous, liquid and/or granular material by passage through a tube-like conduit which contains a plurality of consecutive mixing elements comprising a set of stationary, angularly disposed flow-deflecting baffles of particular form and configuration which cause a repeated dividing, displacement and recombining of the fluid stream and thereby provide improved radial mixing and approximation of ideal plug flow.
摘要翻译：一种用于充分混合流体材料的组分的装置，更具体地说，用于通过穿过包含多个连续混合元件的管状导管来混合和均匀气态，液体和/或颗粒材料流，该装置包括一组静止的，具有特定形式和构造的角度设置的流动偏转挡板，其导致流体流的重复分割，移位和复合，从而提供理想的塞流量的改进的径向混合和近似。

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