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61. 发明授权

US06582569B1 Process for sputtering copper in a self ionized plasma 有权
标题翻译：在自离子等离子体中溅射铜的工艺
公开(公告)号：US06582569B1
公开(公告)日：2003-06-24
申请号：US09685978
申请日：2000-10-10
申请人： Tony P. Chiang , Yu D. Cong , Peijun Ding , Jianming Fu , Howard H. Tang , Anish Tolia
发明人： Tony P. Chiang , Yu D. Cong , Peijun Ding , Jianming Fu , Howard H. Tang , Anish Tolia
IPC分类号： C23C1434
CPC分类号： H01L21/76843 , C23C14/046 , C23C14/345 , C23C14/3457 , C23C14/35 , C23C14/358 , C23C14/564 , H01J37/321 , H01J37/3402 , H01J37/3408 , H01J37/3441 , H01J2237/3327 , H01L21/2855 , H01L21/76862 , H01L21/76865 , H01L21/76868 , H01L21/76871 , H01L21/76873 , H01L21/76876 , H01L21/76877 , H01L2221/1089
摘要： A DC magnetron sputter reactor for sputtering copper, its method of use, and shields and other parts promoting self-ionized plasma (SIP) sputtering, preferably at pressures below 5 milliTorr, preferably below 1 milliTorr. Also, a method of coating copper into a narrow and deep via or trench using SIP for a first copper layer. SIP is promoted by a small magnetron having poles of unequal magnetic strength and a high power applied to the target during sputtering. The SIP copper layer can act as a seed and nucleation layer for hole filling with conventional sputtering (PVD) or with electrochemical plating (ECP). For very high aspect-ratio holes, a copper seed layer is deposited by chemical vapor deposition (CVD) over the SIP copper nucleation layer, and PVD or ECP completes the hole filling. The copper seed layer may be deposited by a combination of SIP and high-density plasma sputtering. For very narrow holes, the CVD copper layer may fill the hole.
摘要翻译：用于溅射铜的直流磁控溅射反应器，其使用方法，以及促进自离子等离子体（SIP）溅射的屏蔽和其它部件，优选在低于5毫托的压力，优选低于1毫托的压力下。另外，使用SIP将第一铜层涂覆在窄的和深的通孔或沟槽中的方法。 SIP由在溅射期间施加到靶的不均匀磁强度和高功率的磁极的小磁控管促进。 SIP铜层可以作为用常规溅射（PVD）或电化学电镀（ECP）进行孔填充的晶种和成核层。对于非常高的纵横比孔，通过化学气相沉积（CVD）在SIP铜成核层上沉积铜籽晶层，并且PVD或ECP完成孔填充。可以通过SIP和高密度等离子体溅射的组合来沉积铜籽晶层。对于非常窄的孔，CVD铜层可以填充孔。

62. 发明授权

US5998534A Water-soluble or water-dispersible addition copolymer 失效
标题翻译：水溶性或水分散性加成共聚物
公开(公告)号：US5998534A
公开(公告)日：1999-12-07
申请号：US100517
申请日：1998-06-19
申请人： Robert H. Tang , Huawen Li , Alan E. Wang
发明人： Robert H. Tang , Huawen Li , Alan E. Wang
IPC分类号： C08F220/10 , C08F220/28 , C08F26/06
CPC分类号： C08F220/28 , C08F220/10
摘要： Water-soluble or water-dispersible addition copolymer of ethylenically unsaturated monomers, wherein the ethylenically unsaturated monomers comprise N-vinyl-2-pyrrolidinone and ethylenically unsaturated polyether, is useful as a component of inkjet printable coatings. The copolymer serves to reduce later migration of inks printed on the coatings.
摘要翻译：烯键式不饱和单体的水溶性或水分散性加成共聚物，其中烯属不饱和单体包括N-乙烯基-2-吡咯烷酮和烯属不饱和聚醚，可用作喷墨印刷涂料的组分。该共聚物用于减少印刷在涂料上的油墨的稍后迁移。

63. 发明授权

US5980724A Method of electrochemically producing epoxides 失效
标题翻译：电化学生产环氧化物的方法
公开(公告)号：US5980724A
公开(公告)日：1999-11-09
申请号：US112657
申请日：1998-07-09
申请人： David G. Roberts , Peter C. Foller , Robert H. Tang , Yingchao Zhang
发明人： David G. Roberts , Peter C. Foller , Robert H. Tang , Yingchao Zhang
IPC分类号： C25B3/04 , C25B3/00 , C25B7/00
CPC分类号： C25B3/04
摘要： Described is a method of electrochemically converting .alpha.-halohydrins, e.g., 1-chloro-2-hydroxypropane and 1,3-dichloro-2-hydroxypropane, to epoxides, e.g., propylene oxide and epichlorohydrin. An electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and a bipolar ion exchange membrane, (2) an anode compartment containing an anode assembly comprising either (a) a hydrogen consuming gas diffusion anode and a current collecting electrode or (b) a hydrogen consuming gas diffusion anode which is fixedly held between a hydraulic barrier and a current collecting electrode, and (3) at least one pair of intermediate compartments separating the catholyte and anode compartments and separated from each other by an anion exchange membrane. The following are introduced into the cell: a first aqueous conductive electrolyte solution into the catholyte compartment; hydrogen gas into the anode compartment; an aqueous solution of .alpha.-halohydrin into the first compartment of the pair of intermediate compartments; and a second aqueous conductive electrolyte solution into the second compartment of the pair of intermediate compartments. Direct current is passed through the electrolytic cell, and an aqueous solution comprising epoxide is removed from the first compartment.
摘要翻译：描述了将α-卤代醇如1-氯-2-羟基丙烷和1,3-二氯-2-羟基丙烷电化学转化为环氧化物，例如环氧丙烷和表氯醇的方法。提供一种电解池，其具有（1）阴极电解液室，其包含阴极组件，阴极组件包括阴极和双极离子交换膜，（2）阳极室，其包含阳极组件，阳极组件包括（a）消耗氢的气体扩散阳极和电流收集电极或（b）固定保持在液压屏障和集电电极之间的消耗氢的气体扩散阳极，以及（3）至少一对隔离阴极电解液室和阳极室的中间隔室，阴离子交换膜。将以下物质引入电池中：将第一水性导电电解质溶液引入到阴极电解液室中; 氢气进入阳极室; 将α-卤代醇的水溶液注入到该对中间隔室的第一隔室中; 以及第二水性导电电解质溶液进入所述一对中间隔室中的第二隔室。直流电流通过电解槽，从第一隔室除去包含环氧化物的水溶液。

64. 发明授权

US5904829A Method of converting amine hydrohalide into free amine 失效
标题翻译：将胺氢卤化物转化为游离胺的方法
公开(公告)号：US5904829A
公开(公告)日：1999-05-18
申请号：US914601
申请日：1997-08-18
申请人： Peter C. Foller , David G. Roberts , Robert H. Tang
发明人： Peter C. Foller , David G. Roberts , Robert H. Tang
IPC分类号： B01D61/44 , C07C209/68 , C25B3/00 , C25B1/00 , C25B7/00 , C25B9/00
CPC分类号： B01D61/445 , C07C209/68 , C25B3/00
摘要： Describes a method of electreochemically converting amine hydrohalide, e.g., amine hydrochloride, into free amine, e.g., free ethyleneamine. An electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and a bipolar ion exchange membrane, (2) an anode compartment containing an anode assembly comprising either (a) a hydrogen consuming gas diffusion anode and a current collecting electrode or (b) a hydrogen consuming gas diffusion anode which is fixedly held between a hydraulic barrier and a current collecting electrode, and (3) at least one pair of intermediate compartments separating the catholyte and anode compartments and separated from each other by an anion exchange membrane. The following are introduced into the cell: a first aqueous conductive electrolyte solution into the catholyte compartment; hydrogen gas into the anode compartment; an aqueous solution of amine hydrohalide into the first compartment of the pair of intermediate compartments; and a second aqueous conductive electrolyte solution into the second compartment of the pair of intermediate compartments. Direct current is passed through the electrolytic cell, and an aqueous solution comprising free amine is removed from the first compartment.
摘要翻译：描述了将胺氢卤化物（例如胺盐酸盐）电化学转化成游离胺，例如游离亚乙基胺的方法。提供一种电解池，其具有（1）阴极电解液室，其包含阴极组件，阴极组件包括阴极和双极离子交换膜，（2）阳极室，其包含阳极组件，阳极组件包括（a）消耗氢的气体扩散阳极和电流收集电极或（b）固定保持在液压屏障和集电电极之间的消耗氢的气体扩散阳极，以及（3）至少一对隔离阴极电解液室和阳极室的中间隔室，阴离子交换膜。将以下物质引入电池中：将第一水性导电电解质溶液引入到阴极电解液室中; 氢气进入阳极室; 胺氢卤酸盐的水溶液进入该对中间隔室的第一隔室; 以及第二水性导电电解质溶液进入所述一对中间隔室中的第二隔室。直流电流通过电解槽，从第一隔室除去包含游离胺的水溶液。

65. 发明授权

US5531998A Polycarbonate-based block copolymers and devices 失效
公开(公告)号：US5531998A
公开(公告)日：1996-07-02
申请号：US162814
申请日：1993-12-03
申请人： Frank Mares , William J. Boyle, Jr. , Reginald T.-H. Tang , Kundanbhai M. Patel , Abraham M. Kotliar , Tin-Ho Chiu
发明人： Frank Mares , William J. Boyle, Jr. , Reginald T.-H. Tang , Kundanbhai M. Patel , Abraham M. Kotliar , Tin-Ho Chiu
IPC分类号： A61L15/64 , A61L17/10 , A61L27/18 , A61L31/06 , A61K9/70 , A61L15/00 , A61L17/00 , A61L31/00
CPC分类号： A61L27/18 , A61L15/64 , A61L17/10 , A61L31/06 , Y10T428/1352 , Y10T428/1362 , Y10T428/249958 , Y10T428/2973 , Y10T428/2975 , Y10T428/2976 , Y10T428/2978 , Y10T442/183 , Y10T442/3106 , Y10T442/425
摘要： This invention relates to a novel polycarbonate-based block polymer, and to fibers and bioresorbable implantable medical devices fabricated from said fibers.

66. 发明授权

US5496476A Non-formaldehyde durable press finishing for cellulosic textiles with phosphonoalkylpolycarboxylic acid 失效
标题翻译：纤维素纺织品与膦酰基烷基多羧酸的非甲醛耐久压机加工
公开(公告)号：US5496476A
公开(公告)日：1996-03-05
申请号：US247943
申请日：1994-05-24
申请人： Robert H. Tang , William A. Williams, Jr.
发明人： Robert H. Tang , William A. Williams, Jr.
IPC分类号： D06M13/192 , D06M13/203 , D06M13/288 , D06M14/04 , D06M15/263 , D06M13/282
CPC分类号： D06M13/203 , D06M13/192 , D06M13/288 , D06M14/04 , D06M15/263 , D06M2101/06
摘要： A composition and method for providing a non-formaldehyde durable press finish to cellulosic fabrics by employing phosphonoalkylpolycarboxylic acids are disclosed. The phosphonoalkylpolycarboxylic acid is optimally used in combination with another polycarboxylic acid, such as polyacrylic acid, and/or, for cost effectiveness, a low-cost polycarboxylic acid such as citric acid. The catalyst for the curing reaction is optimally a phosphorus-containing acid or alkali metal salt thereof, such as a mixture of sodium monophosphate and sodium hypophosphite.
摘要翻译：公开了一种通过使用膦酰基烷基多羧酸向纤维素织物提供非甲醛耐久的压光加工的组合物和方法。膦酰基烷基多羧酸与另一种多元羧酸（如聚丙烯酸）组合使用，和/或为了成本效益，优选使用低成本多元羧酸如柠檬酸。用于固化反应的催化剂最好是含磷酸或其碱金属盐，例如单磷酸钠和次磷酸钠的混合物。

67. 发明授权

US5231211A Method for preparing di(organo) esters of pyrocarbonic acid 失效
标题翻译：制备热碳酸二（有机）酯的方法
公开(公告)号：US5231211A
公开(公告)日：1993-07-27
申请号：US947211
申请日：1992-09-18
申请人： Robert H. Tang
发明人： Robert H. Tang
IPC分类号： B01J31/02 , B01J31/06 , C07B61/00 , C07C68/02 , C07C69/96
CPC分类号： C07C68/02
摘要： Di(organo) esters of pyrocarbonic acid, e.g., dialkyl pyrocarbonates, such as diethyl pyrocarbonate, are prepared by reaction of the corresponding organohaloformate with aqueous alkali metal hydroxide, e.g., sodium hydroxide, in the substantial absence of an organic solvent and in the presence of a catalytic amount of a bis[poly(oxy(C.sub.2 -C.sub.4)alkylene)] C.sub.6 -C.sub.20 aliphatic amine, e.g., coco bis(polyoxyethylene) amine.
摘要翻译：通过相应的有机卤代甲酸酯与碱金属氢氧化物如氢氧化钠在基本上不存在有机溶剂的条件下反应制备焦碳碳酸二（有机）酯，例如焦碳酸二乙酯，催化量的双[聚（氧（C 2 -C 4）亚烷基）] C 6 -C 20脂族胺，例如椰油双（聚氧乙烯）胺。

68. 发明授权

US5219937A Process for preparing graft and block copolymers of polyphenylene oxides and polyesters and copolymers prepared by said process 失效
标题翻译：制备聚苯醚和聚酯的接枝和嵌段共聚物的方法以及通过所述方法制备的共聚物
公开(公告)号：US5219937A
公开(公告)日：1993-06-15
申请号：US898280
申请日：1992-06-15
申请人： Reginald T-H. Tang , Michael C. Bochnik , Frank Mares , Steve Arnold
发明人： Reginald T-H. Tang , Michael C. Bochnik , Frank Mares , Steve Arnold
IPC分类号： C08G81/00
CPC分类号： C08G81/00 , Y10S525/905
摘要： A process of forming block and/or graft copolymers of a polyester and a polyphenylene oxide which comprises heating a mixture of the polyester and the polyphenylene oxide in the presence of a phosphite compound.
摘要翻译：一种形成聚酯和聚苯醚的嵌段和/或接枝共聚物的方法，包括在亚磷酸酯化合物的存在下加热聚酯和聚苯醚的混合物。

69. 发明授权

US5214589A Throat height control during lapping of magnetic heads 失效
标题翻译：磁头穿透时的高度控制
公开(公告)号：US5214589A
公开(公告)日：1993-05-25
申请号：US675096
申请日：1991-03-22
申请人： George H. Tang
发明人： George H. Tang
IPC分类号： G11B5/00 , G11B5/187 , G11B5/31 , G11B5/455 , G11B5/465
CPC分类号： G11B5/1871 , G11B5/3116 , G11B5/3166 , G11B2005/0013 , G11B5/455 , G11B5/465
摘要： During a lapping operation to obtain an optimum throat height for a thin film magnetic head, an M-H looper circuit is coupled directly to the head coil for measuring the magnetization and saturation current of the head in response to a given drive current. An amplitude modulated analog output signal is digitized and the resultant digital number is compared to stored data signals which are representative of optimum throat heights for the design of the head being lapped. The lapping operation is controlled in response to the difference signals obtained by the comparison.

70. 发明授权

US4742133A Poly(allyl carbonate)-functional prepolymers prepared by treatment with molecular oxygen 失效
标题翻译：通过用分子氧处理制备的聚（碳酸烯丙酯）官能预聚物
公开(公告)号：US4742133A
公开(公告)日：1988-05-03
申请号：US779400
申请日：1985-09-24
申请人： Felicia Y. Tang , Robert H. Tang
发明人： Felicia Y. Tang , Robert H. Tang
IPC分类号： C08F4/00 , C08F18/24
CPC分类号： C08F18/24
摘要： A liquid monomer composition comprising of at least one poly(allyl carbonate)-functional monomer is contacted with molecular oxygen to produce a liquid intermediate composition which is then heated to produce a polymerizable, liquid substantially gel-free composition which contains poly(allyl carbonate)-funtional prepolymer which has an allylic utilization of at least about 12 percent.
摘要翻译：包含至少一种聚（碳酸烯丙酯）官能单体的液体单体组合物与分子氧接触以产生液体中间体组合物，然后将其加热以产生可聚合的液体基本上不含凝胶的组合物，其含有聚（碳酸烯丙酯）其具有至少约12％的烯丙基利用率的自由基预聚物。

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