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51. 发明授权

US07332634B2 Method for the continuous purification by distillation of 1,2-propylene glycol that accumulates during the synthesis of propylene oxide without coupling products 有权
标题翻译：通过蒸馏连续纯化1,2-丙二醇的方法，在合成环氧丙烷过程中积聚而不产生偶联产物
公开(公告)号：US07332634B2
公开(公告)日：2008-02-19
申请号：US10521783
申请日：2003-07-22
申请人： Peter Bassler , Hans-Georg Goebbel , Joaquim Henrique Teles , Peter Rudolf
发明人： Peter Bassler , Hans-Georg Goebbel , Joaquim Henrique Teles , Peter Rudolf
IPC分类号： C07C27/28 , C07C29/74 , C07C31/20
CPC分类号： B01D3/141 , B01D3/143 , C07D301/32
摘要： The invention relates to a continuously operated process for the purification by distillation of the 1,2-propylene glycol formed as by-product in the synthesis of propylene oxide, wherein the mixture formed in the synthesis which contains the 1,2-propylene glycol is separated in a dividing wall column into low-, intermediate- and high-boiling fractions and the 1,2-propylene glycol is taken off as intermediate boiler at the side offtake of the column.
摘要翻译：本发明涉及通过蒸馏在合成环氧丙烷中作为副产物形成的1,2-丙二醇进行纯化的连续操作方法，其中在含有1,2-丙二醇的合成中形成的混合物是在分隔壁塔中分离成低，中和高沸点馏分，1,2-丙二醇作为塔的出料侧的中间锅炉取出。

52. 发明授权

US07217818B2 Purification of caprolactam 有权
标题翻译：己内酰胺的纯化
公开(公告)号：US07217818B2
公开(公告)日：2007-05-15
申请号：US10534802
申请日：2003-11-11
申请人： Rolf-Hartmuth Fischer , Hermann Luyken , Andreas Ansmann , Peter Bassler , Christoph Benisch , Stefan Maixner , Johann-Peter Melder
发明人： Rolf-Hartmuth Fischer , Hermann Luyken , Andreas Ansmann , Peter Bassler , Christoph Benisch , Stefan Maixner , Johann-Peter Melder
IPC分类号： C07D201/16
CPC分类号： C07D201/16 , C07D201/08
摘要： A process for removing high boilers from crude caprolactam which comprises high boilers, caprolactam and in some cases low boilers, and which has been obtained by a) reacting 6-aminocapronitrile with water to give a reaction mixture b) removing ammonia and unconverted water from the reaction mixture to obtain crude caprolactam, which comprises c) feeding the crude caprolactam to a distillation apparatus to obtain a first substream via the top as a product and a second substream via the bottom, by setting the pressure in the distillation in such a way that the bottom temperature does not go below 170° C., and adjusting the second substream in such a way that the caprolactam content of the second substream is not less than 10% by weight, based on the entire second substream.
摘要翻译：一种从粗己内酰胺中除去高锅炉的方法，其包括高锅炉，己内酰胺，在某些情况下是低锅炉，并且通过以下方法获得：a）使6-氨基己腈与水反应得到反应混合物; b）除去氨和未转化的水反应混合物以获得粗己内酰胺，其包括c）将粗己内酰胺加入到蒸馏装置中，通过顶部获得第一子流作为产物，通过底部通过设置第二子流，通过将蒸馏中的压力设定为使得底部温度不低于170℃，并且调节第二子流，使得第二子流的己内酰胺含量基于整个第二子流不小于10重量％。

53. 发明申请

US20060276662A1 Method for producing an alkene oxide 失效
标题翻译：烯烃生产方法
公开(公告)号：US20060276662A1
公开(公告)日：2006-12-07
申请号：US10553516
申请日：2004-04-16
申请人： Hans-Georg Gobbel , Peter Bassler , Joaquim Teles , Peter Rudolf
发明人： Hans-Georg Gobbel , Peter Bassler , Joaquim Teles , Peter Rudolf
IPC分类号： C07D301/12
CPC分类号： C07D301/12
摘要： Process for preparing an alkene oxide, which comprises at least the steps (i), (ii) and (v): (i) providing a stream S1 comprising compressed, liquid alkene; (ii) depressurizing at least part of the stream S1 with absorption of heat and with at least partial vaporization of the liquid alkene; (v) reacting the alkene obtained in (ii) with a hydroperoxide in the presence of at least one solvent and at least one catalyst to give a mixture comprising alkene oxide and the solvent or solvents.
摘要翻译：制备氧化烯的方法，其至少包括步骤（i），（ii）和（v）：（i）提供包含压缩的液体烯烃的料流S1; （ii）吸收热量并至少部分汽化液态烯烃使至少部分流S1减压; （v）使（ii）中获得的烯烃与至少一种溶剂和至少一种催化剂存在下的氢过氧化物反应，得到包含烯烃氧化物和溶剂或溶剂的混合物。

54. 发明申请

US20060167287A1 Continuos recirculation of the olefin which has not been reacted in the oxidation of olefins by hydroperoxides, by means of solvent scrubbing 失效
标题翻译：通过氢过氧化物在烯烃的氧化中没有反应的烯烃的连续再循环，通过溶剂洗涤
公开(公告)号：US20060167287A1
公开(公告)日：2006-07-27
申请号：US10531868
申请日：2003-10-23
申请人： Peter Bassler , Hans-Georg Gobbel , Joaquim Teles , Peter Rudolf
发明人： Peter Bassler , Hans-Georg Gobbel , Joaquim Teles , Peter Rudolf
IPC分类号： C07D301/19
CPC分类号： C07D301/12 , B01D53/1487 , B01D53/1493 , B01D2257/702 , C07D301/32
摘要： Process for the continuous recirculation of the olefin which has not been reacted in the oxidation of olefins by means of hydroperoxide to give oxiranes and is present in the offgas stream formed during the oxidation, which comprises the steps (i) to (iii) (i) separating the olefin from the offgas stream by absorption in a hydrocarbon, (ii) desorbing the olefin from the hydrocarbon, (iii) recirculating the olefin obtained in step (ii) to the oxidation process.
摘要翻译：通过氢过氧化物在烯烃氧化中未反应的烯烃的连续再循环以产生环氧乙烷并存在于氧化期间形成的废气流中的方法，其包括步骤（i）至（iii）（i ）通过在烃中的吸收从废气流中分离烯烃，（ii）从烃解链烯烃，（iii）将步骤（ii）中获得的烯烃再循环到氧化过程中。

55. 发明申请

US20050258026A1 Method for the continuous purification by distillation of the solvent methanol, used in the synthesis of propylene oxide 有权
标题翻译：通过蒸馏法连续净化溶剂甲醇的方法，用于合成环氧丙烷
公开(公告)号：US20050258026A1
公开(公告)日：2005-11-24
申请号：US10521784
申请日：2003-07-22
申请人： Peter Bassler , Hans-Georg Gobbel , Joaquin Teles , Peter Rudolf
发明人： Peter Bassler , Hans-Georg Gobbel , Joaquin Teles , Peter Rudolf
IPC分类号： B01D3/14 , B01D3/42 , C07D301/12 , B01D3/38
CPC分类号： B01D3/141 , B01D3/143 , B01D3/4222 , C07D301/12 , Y10S203/20 , Y10S203/24
摘要： Process for the continuously operated purification by distillation of the methanol used as solvent in the synthesis of propylene oxide by reaction of a hydroperoxide with propylene, with the methoxypropanols being separated off simultaneously, wherein the solvent mixture obtained in the synthesis is separated in a dividing wall column into a low-boiling fraction comprising methanol, an intermediate-boiling fraction comprising the methoxypropanols as azeotrope with water and a high-boiling fraction comprising water and propylene glycol.
摘要翻译：通过蒸馏通过氢过氧化物与丙烯的反应合成环氧丙烷的甲醇作为溶剂进行连续操作纯化的方法，同时将甲氧基丙醇分离出来，其中合成中得到的溶剂混合物在分隔壁色谱柱成为包含甲醇的低沸点馏分，包含与水共沸的甲氧基丙醇的中间沸点馏分和包含水和丙二醇的高沸点馏分。

56. 发明授权

US06896772B2 Method for separating ammonia from solutions containing caprolactam and ammonia 失效
标题翻译：从含有己内酰胺和氨的溶液中分离氨的方法
公开(公告)号：US06896772B2
公开(公告)日：2005-05-24
申请号：US10297051
申请日：2001-06-02
申请人： Hermann Luyken , Frank Ohlbach , Stefan Maixner , Rolf-Hartmuth Fischer , Johann-Peter Melder , Peter Bassler , Andreas Ansmann
发明人： Hermann Luyken , Frank Ohlbach , Stefan Maixner , Rolf-Hartmuth Fischer , Johann-Peter Melder , Peter Bassler , Andreas Ansmann
IPC分类号： C07D223/10 , B01D3/00 , C01C1/10 , C07D201/08 , C07D201/16 , B01D5/00 , C01C1/00
CPC分类号： C01C1/10 , C07D201/08 , C07D201/16
摘要： A process for distillative removal of ammonia from solutions (I) which include a lactam and ammonia comprises effecting said removal in a distillation apparatus (a) at an absolute pressure of less than 10 bar.
摘要翻译：从包括内酰胺和氨的溶液（I）中蒸馏除去氨的方法包括在绝对压力小于10巴的蒸馏装置（a）中进行所述除去。

57. 发明授权

US06852199B2 Method for separating pentenenitrile isomers 失效
标题翻译：分离戊烯腈异构体的方法
公开(公告)号：US06852199B2
公开(公告)日：2005-02-08
申请号：US10381338
申请日：2001-09-25
申请人： Tim Jungkamp , Dagmar Pascale Kunsmann-Keitel , Robert Baumann , Peter Bassler , Wolfgang Siegel
发明人： Tim Jungkamp , Dagmar Pascale Kunsmann-Keitel , Robert Baumann , Peter Bassler , Wolfgang Siegel
IPC分类号： C07C253/34 , C07C255/07 , B01D3/36 , B01D3/38
CPC分类号： C07C253/34 , C07C255/07
摘要： A process is provided for the distillative separation of pentene nitrile isomers which have a relative volatility alpha ranging from 1.0 to 1.3 in the pressure range from 1 to 500 kPa, wherein the distillation is carried out in the presence of a liquid diluent which forms with the pentene nitrile isomers, under the same pressure conditions, azeotropes whose relative volatility alpha is higher than that of the pentene nitrile isomers to be separated.
摘要翻译：提供了一种用于蒸馏分离戊烯腈异构体的方法，其在1至500kPa的压力范围内的相对挥发度α为1.0至1.3，其中蒸馏在与戊烯腈异构体，在相同的压力条件下，其相对挥发度α高于待分离的戊烯腈异构体的共沸物。

58. 发明授权

US06849162B2 Method for the production of propylene oxide 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US06849162B2
公开(公告)日：2005-02-01
申请号：US10312884
申请日：2001-07-05
申请人： Joaquim Henrique Teles , Alwin Rehfinger , Peter Bassler , Anne Wenzel , Norbert Rieber , Peter Rudolf
发明人： Joaquim Henrique Teles , Alwin Rehfinger , Peter Bassler , Anne Wenzel , Norbert Rieber , Peter Rudolf
IPC分类号： C07D301/12 , C07D301/32 , B01D3/34 , C07C27/28
CPC分类号： C07D301/32 , C07D301/12 , Y10S203/22 , Y10S203/24
摘要： A process for the preparation of propylene oxide in the presence of methanol, in which propylene oxide is separated from a mixture propylene oxide and methanol, and the resultant methanol containing mixture is worked up, including seperating methanol from a mixture comprising methanol and methyl formate during the work-up.
摘要翻译：在甲醇存在下制备环氧丙烷的方法，其中环氧丙烷与环氧丙烷和甲醇的混合物分离，并且所得到的含甲醇的混合物被处理，包括从包含甲醇和甲酸甲酯的混合物中分离甲醇，上班。

59. 发明授权

US06727371B2 Method for converting an organic compound with a hydroperoxide 有权
标题翻译：用氢过氧化物转化有机化合物的方法
公开(公告)号：US06727371B2
公开(公告)日：2004-04-27
申请号：US10240278
申请日：2002-09-30
申请人： Ulrich Müller , Joaquim Henrique Teles , Norbert Rieber , Andreas Walch , Peter Bassler , Alwin Rehfinger , Anne Wenzel , Wolfgang Harder
发明人： Ulrich Müller , Joaquim Henrique Teles , Norbert Rieber , Andreas Walch , Peter Bassler , Alwin Rehfinger , Anne Wenzel , Wolfgang Harder
IPC分类号： C07D30112
CPC分类号： B01J8/02 , B01J8/0285 , B01J29/90 , B01J2208/021 , B01J2219/00033 , B01J2219/00051 , C07D301/00
摘要： In a continuous process for reacting an organic compound with hydroperoxide in the presence of a catalyst, the reaction is carried out in a reactor assembly comprising at least two reactors connected in parallel.
摘要翻译：在催化剂存在下使有机化合物与氢过氧化物反应的连续方法中，反应在包含至少两个平行连接的反应器的反应器组件中进行。

60. 发明授权

US06683179B2 Preparation of caprolactam 有权
标题翻译：己内酰胺的制备
公开(公告)号：US06683179B2
公开(公告)日：2004-01-27
申请号：US10258941
申请日：2002-10-29
申请人： Peter Bassler , Dieter Baumann , Rolf-Hartmuth Fischer , Eberhard Fuchs , Johann-Peter Melder , Frank Ohlbach
发明人： Peter Bassler , Dieter Baumann , Rolf-Hartmuth Fischer , Eberhard Fuchs , Johann-Peter Melder , Frank Ohlbach
IPC分类号： C07D20108
CPC分类号： C07D201/08
摘要： A process for the preparation of caprolactam is provided, wherein a) a mixture (I) containing 6-aminocapronitrile and water is reacted in the gas phase, in the presence of a catalyst, to give a mixture (II) containing caprolactam, ammonia, water, high-boiling components and low-boiling components, b) ammonia is then removed from the mixture (II) to give a mixture (III) containing caprolactam, water, high-boiling components and low-boiling components, c) water is then removed from the mixture (III) to give a mixture (IV) containing caprolactam, high-boiling components and low-boiling components, and d) a solid (V) containing caprolactam is then obtained from the mixture (IV) by crystallization, the proportion by weight of caprolactam in the solid (V) being greater than in the mixture (IV).
摘要翻译：提供了制备己内酰胺的方法，其中a）含有6-氨基己腈和水的混合物（I）在催化剂存在下在气相中反应，得到含己内酰胺，氨，水的混合物（II），高沸点组分和低沸点组分，b）然后从混合物（II）中除去氨，得到含有己内酰胺，水，高沸点组分和低沸点组分的混合物（III），c）然后将水从混合物（III）中除去，得到含有己内酰胺，高沸点组分和低沸点组分的混合物（IV），然后通过结晶从混合物（IV）获得含有己内酰胺的固体（V），比例的固体（V）中的己内酰胺的量大于混合物（IV）中的。

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