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41. 发明申请

US20130277605A1 Cyclohexylbenzene Compositions 审中-公开
标题翻译：环己基苯组合物
公开(公告)号：US20130277605A1
公开(公告)日：2013-10-24
申请号：US13816338
申请日：2011-08-16
申请人： Keith H. Kuechler , Francisco M. Benitez
发明人： Keith H. Kuechler , Francisco M. Benitez
IPC分类号： C07C49/303 , C07C39/04
CPC分类号： C07C49/303 , C07C37/08 , C07C39/04 , C07C45/53 , C07C2601/14 , C07C49/403
摘要： In a process for producing phenol and cyclohexanone, a feed comprising cyclohexylbenzene is oxidized to produce an oxidation reaction product comprising cyclohexyl-1-phenyl-1-hydroperoxide. At least a portion of the oxidation reaction product is then cleaved to produce a cleavage reaction product comprising phenol, cyclohexanone, and at least one contaminant. At least a portion of the cleavage reaction product is contacted with an acidic material to convert at least a portion of the at least one contaminant to a converted contaminant and thereby produce a modified reaction product. The oxidation reaction product may have at least 50 wt % of cyclohexylbenzene, no greater than 80 wt % of cyclo-hexyl-1-phenyl-1-hydroperoxide, and 0.1 wt % to 10 wt % of another hydroperoxide.
摘要翻译：在生产苯酚和环己酮的方法中，将包含环己基苯的进料氧化生成包含环己基-1-苯基-1-氢过氧化物的氧化反应产物。然后将至少一部分氧化反应产物切割以产生包含苯酚，环己酮和至少一种污染物的裂解反应产物。裂解反应产物的至少一部分与酸性物质接触以将至少一部分至少一种污染物转化为转化的污染物，从而产生改性的反应产物。氧化反应产物可以具有至少50重量％的环己基苯，不大于80重量％的环己基-1-苯基-1-氢过氧化物和0.1重量％至10重量％的其它氢过氧化物。

42. 发明授权

US08546633B2 Method for producing alkylated aromatic compound, method for producing cumene, and method for producing phenol 有权
标题翻译：烷基化芳香族化合物的制造方法，异丙基苯的制造方法以及苯酚的制造方法
公开(公告)号：US08546633B2
公开(公告)日：2013-10-01
申请号：US13125163
申请日：2009-10-22
申请人： Kenji Fujiwara , Tsuneyuki Ohkubo , Terunori Fujita , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Kozo Yasuda
发明人： Kenji Fujiwara , Tsuneyuki Ohkubo , Terunori Fujita , Shinobu Aoki , Masayasu Ishibashi , Masao Imai , Kozo Yasuda
IPC分类号： C07C2/86 , C07C37/08
CPC分类号： C07C37/08 , B01J23/80 , B01J29/7007 , B01J29/7038 , C07C2/867 , C07C15/085 , C07C407/00 , C07C409/10 , Y02P20/52 , Y02P20/588 , C07C39/04
摘要： A method for producing an alkylated aromatic compound includes a step (i) of producing a reaction product (a1) containing the alkylated aromatic compound and water by the reaction of an aromatic compound, a ketone, and hydrogen using a metal component containing at least one metallic element of copper, nickel, cobalt, and rhenium and a solid acid substance; a step (ii) of forming a dehydrated product (a2) from at least a portion of the reaction product (a1) by removing at least a portion of the water in the reaction product (a1); and a step (iii) of producing a reaction product (a3) containing the alkylated aromatic compound by bringing at least a portion of the dehydrated product (a2) into contact with a solid acid substance.
摘要翻译：烷基化芳香族化合物的制造方法包括使用含有至少一种以上的金属成分，通过芳香族化合物，酮和氢的反应来制造含有烷基化芳香族化合物和水的反应产物（a1）的工序（i）铜，镍，钴和铼的金属元素和固体酸物质; 通过除去反应产物（a1）中的至少一部分水，从至少一部分反应产物（a1）形成脱水产物（a2）的步骤（ii）; 和通过使脱水产物（a2）的至少一部分与固体酸物质接触来制造含有烷基化芳香族化合物的反应产物（a3）的步骤（iii）。

43. 发明申请

US20130150630A1 METHOD FOR PREPARING PHENOLIC COMPOUNDS 有权
标题翻译：制备酚醛化合物的方法
公开(公告)号：US20130150630A1
公开(公告)日：2013-06-13
申请号：US13683473
申请日：2012-11-21
申请人： INDUSTRIAL TECHNOLOGY RESEARCH INSTIT
发明人： Chiung-Fang LIU , Chih-Ching CHEN , Chih-Hao CHEN , Pei-Jung YU , Ying-Hsi CHANG , Hou-Peng WAN , Hom-Ti LEE
IPC分类号： C07C37/50
CPC分类号： C07C37/50 , C07C37/00 , Y02P20/52 , C07C39/04 , C07C39/07
摘要： In an embodiment of the disclosure, a method for preparing a phenolic compound is provided. The method includes providing a lignin depolymerization product, and hydrogenating the lignin depolymerization product under iron oxide and hydrogen gas to prepare a phenolic compound. The prepared phenolic compound is a crude phenolic composition including phenol, methylphenol, dimethylphenol or a combination thereof.
摘要翻译：在本公开的一个实施方案中，提供了一种制备酚类化合物的方法。该方法包括提供木质素解聚产物，并在氧化铁和氢气下氢化木质素解聚产物以制备酚类化合物。所制备的酚类化合物是包括苯酚，甲基苯酚，二甲基苯酚或它们的组合的粗制酚类组合物。

44. 发明授权

US08445730B2 Process for producing phenol 失效
标题翻译：苯酚生产工艺
公开(公告)号：US08445730B2
公开(公告)日：2013-05-21
申请号：US13061601
申请日：2009-07-14
申请人： Jihad M. Dakka , Kun Wang , Edmund J. Mozeleski , Stephen Zushma
发明人： Jihad M. Dakka , Kun Wang , Edmund J. Mozeleski , Stephen Zushma
IPC分类号： C07C409/00
CPC分类号： B01J23/002 , B01J21/066 , B01J23/28 , B01J23/30 , B01J23/888 , B01J31/0247 , B01J31/38 , B01J37/031 , B01J37/10 , B01J2523/00 , C07C37/08 , C07C45/53 , C07C407/00 , C07C409/08 , C07C409/14 , C07C2601/08 , C07C2601/14 , C07C2601/18 , Y02P20/52 , C07C39/04 , C07C49/10 , C07C49/403 , B01J2523/17 , B01J2523/48 , B01J2523/69 , B01J2523/842 , B01J2523/68
摘要： In a process for producing phenol or a substituted phenol, an alkylaromatic hydroperoxide having a general formula (I): in which R1 and R2 each independently represents an alkyl group having from 1 to 4 carbon atoms, provided that R1 and R2 may be joined to form a cyclic group having from 4 to 10 carbon atoms, said cyclic group being optionally substituted, and R3 represents hydrogen, one or more alkyl groups having from 1 to 4 carbon atoms or a cyclohexyl group, is contacted with a catalyst comprising an oxide of at least one metal from Groups 3 to 5 and Groups 7 to 14 of the Periodic Table of the Elements and an oxide of at least one metal from Group 6 of the Periodic Table of the Elements.
摘要翻译：在制备苯酚或取代苯酚的方法中，具有通式（I）的烷基芳基氢过氧化物：其中R 1和R 2各自独立地表示具有1至4个碳原子的烷基，条件是R 1和R 2可以连接到形成具有4至10个碳原子的环状基团，所述环状基团任选被取代，并且R 3表示氢，具有1至4个碳原子的一个或多个烷基或环己基与包含以下化合物的催化剂接触：元素周期表第3至5族和第7至14族中的至少一种金属和至少一种元素周期表第6族金属的氧化物。

45. 发明申请

US20130090499A1 Cyclohexanone Dehydrogenation Catalyst and Process 有权
标题翻译：环己酮脱氢催化剂和工艺
公开(公告)号：US20130090499A1
公开(公告)日：2013-04-11
申请号：US13520467
申请日：2010-12-17
申请人： Teng Xu , Terry E. Helton , Jihad M. Bakka , Tan-Jen Chen , Sabato Miseo , Lorenzo C. Decaul , Edward A. Lemon, JR.
发明人： Teng Xu , Terry E. Helton , Jihad M. Bakka , Tan-Jen Chen , Sabato Miseo , Lorenzo C. Decaul , Edward A. Lemon, JR.
IPC分类号： B01J23/58 , C07C37/07 , C07C37/08
CPC分类号： B01J23/58 , B01J21/08 , B01J37/0205 , B01J37/12 , C07C2/74 , C07C37/06 , C07C37/07 , C07C37/08 , C07C45/53 , C07C407/00 , C07C2529/70 , C07C2601/14 , Y02P20/52 , C07C13/28 , C07C39/04 , C07C49/403 , C07C409/14
摘要： A catalyst composition comprising: (i) a support; (ii) a first component comprising at least one metal component selected from Group 1 and Group 2 of the Periodic Table of Elements; and (iii) a second component comprising at least one metal component selected from Groups 6 to 10 of the Periodic Table of Elements, wherein the catalyst composition exhibits an oxygen chemisorption of greater than 50%.
摘要翻译：一种催化剂组合物，其包含：（i）载体; （ii）包含选自元素周期表第1族和第2族的至少一种金属成分的第一成分; 和（iii）包含选自元素周期表第6至10族的至少一种金属组分的第二组分，其中催化剂组合物显示出大于50％的氧化学吸附。

46. 发明申请

US20120302799A1 Dehydrogenation Catalyst And Process 有权
标题翻译：脱氢催化剂和工艺
公开(公告)号：US20120302799A1
公开(公告)日：2012-11-29
申请号：US13515142
申请日：2010-12-17
申请人： Jihad M. Dakka , Lorenzo C. Decaul , Terry E. Helton , Teng Xu , Jenna L. Wallace
发明人： Jihad M. Dakka , Lorenzo C. Decaul , Terry E. Helton , Teng Xu , Jenna L. Wallace
IPC分类号： C07C37/07 , C07C37/08 , B01J23/04 , B01J37/08 , B01J23/58
CPC分类号： B01J23/58 , B01J21/08 , B01J37/0205 , B01J37/12 , C07C2/74 , C07C37/06 , C07C37/08 , C07C45/53 , C07C407/00 , C07C2529/70 , C07C2601/14 , Y02P20/52 , C07C13/28 , C07C39/04 , C07C49/403 , C07C409/14
摘要： A catalyst composition comprises (i) a support; (ii) a dehydrogenation component comprising at least one metal or compound thereof selected from Groups 6 to 10 of the Periodic Table of Elements; and (iii) potassium or a potassium compound present in an amount of about 0.15 to about 0.6 wt % of potassium based upon the total weight of the catalyst composition, wherein the catalyst composition has an oxygen chemisorption of greater than 50%.
摘要翻译：催化剂组合物包含（i）载体; （ii）包含选自元素周期表第6至10族的至少一种金属或其化合物的脱氢组分; 和（iii）基于催化剂组合物的总重量，钾或钾化合物的存在量为约0.15至约0.6重量％的钾，其中催化剂组合物的氧化学吸附率大于50％。

47. 发明申请

US20120283486A1 PROCESS FOR THE PREPARATION OF PHENOL FROM CUMENE 有权
标题翻译：从酚类制备苯酚的方法
公开(公告)号：US20120283486A1
公开(公告)日：2012-11-08
申请号：US13508619
申请日：2010-10-29
申请人： Mauro Burattini , Roberto Bagatin
发明人： Mauro Burattini , Roberto Bagatin
IPC分类号： C07C37/08
CPC分类号： C07C407/00 , C07C37/08 , C07C45/53 , C07C39/04 , C07C49/08 , C07C409/10
摘要： Process for the production in continuous or semi-continuous of phenol/acetone from cumene, via cumene hy-droperoxide (CHP), which comprises: a. producing CHP in an air-lift reactor in which at least the upper and/or lower part of the downcomer has a flaring; b. cleaving the cumene hydroperoxide by means of acid treatment in a loop reactor comprising two heat exchangers connected in series and wherein the feedings of CHP and fresh acetone are in pairs and each pair is positioned up-stream of each exchanger.
摘要翻译：由枯烯连续或半连续生产苯酚/丙酮的方法，通过氢过氧化枯烯（CHP），其包括：a。在其中至少下降管的上部和/或下部具有扩口的空气提升反应器中产生CHP; b。在包含串联连接的两个热交换器的环管反应器中通过酸处理裂解氢过氧化枯烯，其中CHP和新鲜丙酮的进料成对，并且每对在每个交换器的上游设置。

48. 发明授权

US08273932B2 Process for producing alkylated aromatic compounds and process for producing phenol 有权
标题翻译：烷基化芳香族化合物的制造方法和苯酚的制造方法
公开(公告)号：US08273932B2
公开(公告)日：2012-09-25
申请号：US12997433
申请日：2009-06-03
申请人： Shinji Senoo , Kazuhiko Kato , Kenji Doi , Katsunari Higashi
发明人： Shinji Senoo , Kazuhiko Kato , Kenji Doi , Katsunari Higashi
IPC分类号： C07C1/20 , C07C33/18 , C07C33/34 , C07C39/00
CPC分类号： C07C2/867 , B01J23/80 , B01J29/06 , B01J29/072 , B01J29/076 , B01J29/7007 , B01J29/7615 , B01J29/7815 , B01J35/0006 , C07C37/08 , C07C2523/80 , Y02P20/52 , C07C15/085 , C07C39/04
摘要： The process for producing alkylated aromatic compounds includes feeding raw materials including an aromatic compound, a ketone and hydrogen in a gas-liquid downward concurrent flow mode to a fixed-bed reactor packed with a catalyst thereby to produce an alkylated aromatic compound, wherein the catalyst includes a solid acid component and a metal component, the catalyst is loaded in the fixed-bed reactor such that the catalyst forms a catalyst layer, and the reaction gas flow rate defined by Equation (1) below is not less than 0.05 at an entrance of a layer containing the solid acid: ρg·ug·[ρair·ρwater/(ρg·ρl)]1/2 (kgm−2s−1).
摘要翻译：制造烷基化芳香族化合物的方法包括以气液向下并流方式将包含芳族化合物，酮和氢的原料进料到填充有催化剂的固定床反应器中，从而制备烷基化芳族化合物，其中催化剂包括固体酸组分和金属组分，将催化剂装载到固定床反应器中，使得催化剂形成催化剂层，并且下面的等式（1）定义的反应气体流速在入口处不小于0.05 含有固体酸的层：1/2（kgm-2s-1），其含有固体酸的层：＆lt; ggr•g·ug·[＆rgr空气·水/（＆rgrg。

49. 发明授权

US08257557B2 Dehydration method 失效
标题翻译：脱水方法
公开(公告)号：US08257557B2
公开(公告)日：2012-09-04
申请号：US12064982
申请日：2006-08-29
申请人： Tateo Seo , Tetsuya Suzuta , Toshiaki Ui
发明人： Tateo Seo , Tetsuya Suzuta , Toshiaki Ui
IPC分类号： B01D3/34 , C07C37/02 , C07C37/74 , C07C39/04
CPC分类号： C07C37/02 , C07C37/78 , C07C37/80 , C07C39/04
摘要： A dehydration method for removing water from a hydrolysis reaction mixture containing unreacted water generated when monochlorobenzene is hydrolyzed to produce phenol, the method for dehydrating the hydrolysis reaction mixture includes supplying a hydrolysis reaction mixture to a distillation tower, supplying a liquid containing monochlorobenzene to the tower top portion of the distillation tower, and removing the substantially whole amount of the water in the hydrolysis reaction mixture together with monochlorobenzene from the tower top portion by distillation.
摘要翻译：从含有一氯苯水解生成苯酚的未反应水的水解反应混合物中除去水分的脱水方法，水解反应混合物的脱水方法包括向蒸馏塔供给水解反应混合物，向塔内供给含有一氯苯的液体并且通过蒸馏从塔顶馏分中除去水解反应混合物中基本上全部量的水和一氯苯。

50. 发明申请

US20120157704A1 Method for the Hydroxylation of Halogenated Aryl Compounds 有权
标题翻译：卤化芳基化合物的羟基化方法
公开(公告)号：US20120157704A1
公开(公告)日：2012-06-21
申请号：US13376999
申请日：2010-06-08
申请人： Marc Taillefer , Anis Tlilli , Florian Monnier , Ning Xia
发明人： Marc Taillefer , Anis Tlilli , Florian Monnier , Ning Xia
IPC分类号： C07C37/02 , C07C41/26 , C07C253/30 , C07C205/22 , C07C45/64
CPC分类号： C07C37/02 , C07B41/02 , C07C41/26 , C07C45/64 , C07C201/12 , C07C253/30 , C07C39/07 , C07C39/14 , C07C39/04 , C07C39/15 , C07C39/27 , C07C39/28 , C07C43/23 , C07C49/825 , C07C255/53 , C07C205/22
摘要： The present invention relates to a method for the hydroxylation of halogen aryl compounds carried out at a temperature lower than 200° C. in the presence of a catalytic system including a copper-based catalyst and a ligand L according to reaction scheme Formula (A), in which: R is selected from the groups having an acceptor inductive effect and the groups having a donor mesomer effect; M is selected from alkaline or alkaline-earth cations; X is a halogen atom; r is between 0 and 5; and the ligand L is selected from compounds having formula I.
摘要翻译：本发明涉及在根据反应式（A）的方案的包括铜基催化剂和配体L的催化体系存在下，在低于200℃的温度下进行卤代芳基化合物羟基化的方法，其中：R选自具有受体诱导作用的基团和具有施主介体效应的基团; M选自碱金属或碱土金属阳离子; X是卤原子; r在0和5之间; 配体L选自具有式I的化合物。

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