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41. 发明授权

US06809215B2 Method for hydrogenation of aromatic urethanes in the presence of a supported ruthenium catalyst 失效
标题翻译：在负载型钌催化剂存在下氢化芳族聚氨酯的方法
公开(公告)号：US06809215B2
公开(公告)日：2004-10-26
申请号：US10331644
申请日：2002-12-31
申请人： Norbert Finke , Ranier Lomoelder , Christian Lettmann , Guido Stochniol
发明人： Norbert Finke , Ranier Lomoelder , Christian Lettmann , Guido Stochniol
IPC分类号： C07C26100
CPC分类号： C07C269/06 , B01J23/462 , B01J35/002 , B01J35/0053 , B01J35/008 , B01J35/10 , B01J35/1014 , B01J35/108 , B01J35/109 , B01J35/1095 , B01J37/0201 , C07C271/20
摘要： The invention relates to a method for hydrogenation of aromatic urethanes, which contain one or more aromatic rings and one or more urethane groups bonded directly and/or indirectly to one aromatic ring or to different aromatic rings, using hydrogen in the presence of a supported catalyst, which contains ruthenium as active metal. The catalyst support of the catalyst to be used according to the invention has a BET surface ranging from larger than 30 m2/g to smaller than 70 m2/g and more than 50% of the pore volume of the catalyst support is represented by macropores with a pore diameter of larger than 50 nm and less than 50% is represented by mesopores with a pore diameter of 2 to 50 nm. The method is suitable in particular for hydrogenation of dibutyl 4,4′-methylenedicarbanilate to dibutyl 4,4′-methylenedicyclohexylcarbamate with a trans-trans isomer content of
摘要翻译：本发明涉及芳族聚氨酯的氢化方法，该方法含有一个或多个芳环和一个或多个氨基甲酸酯基团，其直接和/或间接地与一个芳香环或不同的芳环键合，使用氢气在负载催化剂存在下，其含有钌作为活性金属。根据本发明使用的催化剂的催化剂载体的BET表面积大于30m 2 / g至小于70m 2 / g，超过催化剂孔体积的50％载体由孔径大于50nm的大孔表示，小于50％的孔径由孔径为2〜50nm的中孔表示。该方法特别适用于将反式异构体含量<30％，优选<20％，特别优选5-15％的4,4'-亚甲基二苯甲酸二丁酯氢化成二丁基4,4'-亚甲基二环己基氨基甲酸酯。

42. 发明申请

US20160304426A1 TWO-STAGE HYDROFORMYLATION PROCESS WITH CIRCULATING GAS AND SILP TECHNOLOGY 有权
标题翻译：具有循环气和硅胶技术的两级氢化方法
公开(公告)号：US20160304426A1
公开(公告)日：2016-10-20
申请号：US15103842
申请日：2014-12-10
申请人： Marc Becker , Katrin Marie Dyballa , Robert Franke , Dirk Fridag , Hanna Hahn , Marina Lazar , Markus Priske , Guido Stochniol
发明人： Marc Becker , Katrin Marie Dyballa , Robert Franke , Dirk Fridag , Hanna Hahn , Marina Lazar , Markus Priske , Guido Stochniol
IPC分类号： C07C45/50 , C07C45/79 , B01D61/36 , B01J31/18 , B01J31/02 , B01D5/00 , C07C45/82 , B01J31/24
CPC分类号： C07C45/50 , B01D5/006 , B01D5/0072 , B01D61/362 , B01D61/38 , B01D2311/02 , B01D2311/04 , B01D2311/06 , B01D2311/263 , B01D2311/2669 , B01D2311/2673 , B01J31/0292 , B01J31/1845 , B01J31/185 , B01J31/24 , B01J2231/321 , B01J2531/822 , C07C45/786 , C07C45/79 , C07C45/82 , C07C47/02
摘要： The invention relates to processes for preparing aldehydes by hydroformylation of alkenes, in which an alkene-containing feed mixture is subjected to a primary hydroformylation with synthesis gas in the presence of a homogeneous catalyst system, the primary hydroformylation being effected in a primary reaction zone from which a cycle gas containing at least some of the products and unconverted reactants of the primary hydroformylation are drawn off continuously and partly condensed, with recycling of uncondensed components of the cycle gas into the primary reaction zone, and with distillative separation of condensed components of the cycle gas in an aldehyde removal stage to give an aldehyde-rich mixture and a low-aldehyde mixture. The problem that it addresses is that of developing the process such that it achieves high conversions and affords aldehyde in good product quality even in the case of a deteriorating raw material position. More particularly, a solution is to be found for making legacy oxo process plants capable of utilizing lower-value raw material sources. This problem is solved by separating the low-aldehyde mixture into a retentate and a permeate by means of a membrane separation unit in such a way that alkenes present in the low-aldehyde mixture become enriched in the permeate, while alkanes present in the low-aldehyde mixture become enriched in the retentate. The alkene-rich permeate is then transferred into a secondary reaction zone and subjected to a secondary hydroformylation therein with synthesis gas in the presence of an SILP catalyst system. The reaction product obtained from the secondary hydroformylation is recycled into the aldehyde removal stage.
摘要翻译：本发明涉及通过烯烃的加氢甲酰化制备醛的方法，其中含烯烃的进料混合物在均相催化剂体系的存在下用合成气进行初级加氢甲酰化，初级加氢甲酰化在主反应区其中包含至少一些产物的循环气体和初级加氢甲酰基化的未转化的反应物被连续地和部分地冷凝，循环气体的未冷凝的组分循环进入初级反应区，并且通过蒸馏分离在醛去除阶段中循环气体，得到富含醛的混合物和低醛混合物。它所解决的问题是开发该方法，即使在原料位置恶化的情况下，其达到高转化率并提供良好的产品质量的醛。更具体地说，可以找到一种解决方案，用于制造能够利用较低价值的原材料来源的传统氧化工艺装置。通过将低醛混合物通过膜分离单元将低醛混合物分离成滞留物和渗透物来解决，使得存在于低醛混合物中的烯烃变得富集在渗透物中，醛混合物在保留物中变得富集。然后将富含烯烃的渗透物转移到第二反应区中，并在有SILP催化剂体系的情况下用合成气对其进行二次加氢甲酰化。从二次加氢甲酰化得到的反应产物再循环到醛去除阶段。

43. 发明授权

US08889009B2 Process for purifying low molecular weight hydridosilanes 有权
标题翻译：纯化低分子量硅藻土的方法
公开(公告)号：US08889009B2
公开(公告)日：2014-11-18
申请号：US13123827
申请日：2009-10-09
申请人： Nicole Brausch , Goetz Baumgarten , Guido Stochniol , Yuecel Oenal , Martin Trocha
发明人： Nicole Brausch , Goetz Baumgarten , Guido Stochniol , Yuecel Oenal , Martin Trocha
IPC分类号： C01B33/04 , C07F7/02 , B01D61/00
CPC分类号： C01B33/04 , B01D61/00 , C01B33/046 , Y02P20/582
摘要： The present invention relates to a process for purifying low molecular weight hydridosilane solutions, in which a solution to be purified comprising a) at least one low molecular weight hydridosilane, b) at least one solvent and c) at least one impurity selected from the group of the compounds having at least 20 silicon atoms and/or the group of the homogeneous catalyst systems is subjected to a crossflow membrane process with at least one membrane separation step using a permeation membrane.
摘要翻译：本发明涉及一种用于纯化低分子量氢硅烷溶液的方法，其中待纯化的溶液包含a）至少一种低分子量氢硅烷，b）至少一种溶剂和c）至少一种选自以下的杂质：的具有至少20个硅原子的化合物和/或该均相催化剂体系的组合，使用渗透膜进行至少一个膜分离步骤的横流膜方法。

44. 发明申请

US20140086816A1 USE OF BURNERS WITH A JET TUBE IN REACTORS FOR CONVERSION OF CHLOROSILANES 审中-公开
标题翻译：燃烧器与喷射管在反应器中的转换使用氯化石蜡
公开(公告)号：US20140086816A1
公开(公告)日：2014-03-27
申请号：US14007495
申请日：2012-02-27
申请人： Bernd Wehner , Christof Zipper , Guido Stochniol , Ingo Pauli , Norbert Schladerbeck
发明人： Bernd Wehner , Christof Zipper , Guido Stochniol , Ingo Pauli , Norbert Schladerbeck
IPC分类号： C01B33/107
CPC分类号： C01B33/1071 , B01J4/001 , B01J12/007 , B01J19/24 , B01J2219/00155 , B01J2219/00157 , C01B33/10757 , F23C3/002 , F27B17/0016 , F27D99/0035
摘要： The invention provides for the use of a particular burner design to heat reactors for conversion of chlorosilanes, wherein the burner has a jet tube and the jet tube surrounds the flame and the flame tube in a gastight manner, as a result of which the combustion air, the gaseous and/or liquid fuels, and also the flue gases cannot get into the reaction furnace space. The advantage is the complete separation of the flue gas from the actual interior of the reaction furnace, which prevents critical interactions between flue gas moisture and chlorosilanes in the case of fracture of the arrangement accommodating the chlorosilanes. This in turn makes it possible to use gaseous or liquid fuels to heat such a reaction furnace. Excessive local input of heat as a result of direct flame contact is prevented; the heat input is homogenized.
摘要翻译：本发明提供了使用特定的燃烧器设计来加热反应器以转化氯硅烷，其中燃烧器具有喷射管，喷射管以气密方式围绕火焰和火焰管，结果燃烧空气，气体和/或液体燃料，以及烟道气不能进入反应炉空间。优点是烟道气与反应炉的实际内部完全分离，这防止了在容纳氯硅烷的装置断裂的情况下烟道气体与氯硅烷之间的关键相互作用。这又可以使用气体或液体燃料来加热这种反应炉。防止由于直接火焰接触导致的局部过热热输入; 热输入均匀化。

45. 发明授权

US08524945B2 Method for producing acrolein comprising the regeneration of a raw glycerin phase 有权
标题翻译：制备丙烯醛的方法，其包括再生生成的甘油相
公开(公告)号：US08524945B2
公开(公告)日：2013-09-03
申请号：US13128538
申请日：2009-11-03
申请人： Guido Stochniol , Goetz Baumgarten , Franz-Felix Kuppinger
发明人： Guido Stochniol , Goetz Baumgarten , Franz-Felix Kuppinger
IPC分类号： C07C51/00 , C07C31/22
CPC分类号： C07C45/79 , C07C45/52 , C07C45/786 , C07C45/82 , C07C47/22
摘要： The invention relates to a method for producing acrolein by dehydrating an aqueous glycerin phase in an acrolein reaction region, obtaining an aqueous acrolein reaction phase; at least partially separating the aqueous acrolein reaction phase into an acrolein-rich acrolein phase and an acrolein-poor residual phase comprising glycerin, water and various other residuals; and recirculating at least part of the residual phase into the acrolein reaction region. Additionally, removing at least one of the residuals, other than glycerin or water, from either of the glycerin phase or a mixture phase obtained by mixing the glycerol phase with the low-acrolein residue phase and feeding the resulting purified glycerin or mixture phase into the acrolein reaction region. The invention furthermore relates to a method for producing acrylic acid, water-absorbing polymer formations, compounds and hygiene articles, and to devices for carrying out those methods.
摘要翻译：本发明涉及通过在丙烯醛反应区域中脱水甘油三酯相来制备丙烯醛的方法，获得丙烯醛水溶液反应相; 至少部分地将丙烯醛水溶液反应相分离成富含丙烯醛的丙烯醛相和不含丙烯醛的残余相，其包含甘油，水和各种其它残余物; 并将至少部分剩余相再循环到丙烯醛反应区中。此外，从甘油相或通过将甘油相与低丙烯醛残基相混合而获得的甘油相或混合相中除去甘油或水以外的至少一种残余物，并将得到的纯化甘油或混合物相加入到丙烯醛反应区。本发明还涉及制备丙烯酸，吸水聚合物结构，化合物和卫生制品的方法以及用于实施这些方法的装置。

46. 发明申请

US20130053522A1 SUPERABSORBENT POLYMERS AND METHODS OF MAKING THE SAME 有权
标题翻译：超吸收聚合物及其制备方法
公开(公告)号：US20130053522A1
公开(公告)日：2013-02-28
申请号：US13630302
申请日：2012-09-28
申请人： Franz-Felix Kuppinger , Axel Hengstermann , Guido Stochniol , Günther Bub , Jürgen Mosler , Andreas Sabbagh
发明人： Franz-Felix Kuppinger , Axel Hengstermann , Guido Stochniol , Günther Bub , Jürgen Mosler , Andreas Sabbagh
IPC分类号： C08F220/28
CPC分类号： C08F120/06 , C07C51/377 , C07C51/43 , Y02P20/127 , C07C57/04
摘要： In one aspect, a process for the preparation of a superabsorbent polymer is described herein. In some embodiments, the process comprises (I) preparing acrylic acid, wherein the process comprises (a1) provision of a fluid F1 having a composition comprising from about 5 to about 20 wt. % of hydroxypropionic acid, salts thereof, or mixtures thereof; from about 0.1 to about 5 wt. % of inorganic salts; from about 0.1 to about 30 wt. % of organic compounds which differ from hydroxypropionic acid; from 0 to about 50 wt. % of solids; and from about 20 to about 90 wt. % of water; (a2) dehydration of said hydroxypropionic acid to give a fluid F2 containing acrylic acid; and (a3) purification of said fluid F2 to give a purified acrylic acid phase comprising acrylic acid having a purity of at least 70 wt. %; and (II) polymerizing the acrylic acid of (I) to form a superabsorbent polymer.
摘要翻译：一方面，本文描述了制备超吸收性聚合物的方法。在一些实施方案中，该方法包括（I）制备丙烯酸，其中该方法包括（a1）提供具有包含约5至约20wt。％的羟基丙酸，其盐或其混合物; 约0.1至约5wt。％的无机盐; 约0.1至约30wt。％羟基丙酸不同的有机化合物的％; 0至约50wt。％的固体; 和约20至约90wt。％的水; （a2）所述羟基丙酸的脱水，得到含有丙烯酸的流体F2; 和（a3）纯化所述流体F2以得到包含纯度至少为70重量％的丙烯酸的纯化丙烯酸相。％; 和（II）使（I）的丙烯酸聚合以形成超吸收性聚合物。

47. 发明申请

US20110262336A1 PRODUCTION OF SOLAR-GRADE SILICON FROM SILICON DIOXIDE 审中-公开
标题翻译：从二氧化硅生产太阳能级硅
公开(公告)号：US20110262336A1
公开(公告)日：2011-10-27
申请号：US13121761
申请日：2009-09-28
申请人： Hartwig Rauleder , Ekkehard Mueh , Mustafa Siray , Peter Nagler , Bodo Frings , Ingrid Lunt-Rieg , Alfons Karl , Christian Panz , Thomas Groth , Guido Stochniol , Matthias Rochnia , Juergen Erwin Lang , Oliver Wolf , Rudolf Schmitz , Bernd Nowitzki , Dietmar Wewers
发明人： Hartwig Rauleder , Ekkehard Mueh , Mustafa Siray , Peter Nagler , Bodo Frings , Ingrid Lunt-Rieg , Alfons Karl , Christian Panz , Thomas Groth , Guido Stochniol , Matthias Rochnia , Juergen Erwin Lang , Oliver Wolf , Rudolf Schmitz , Bernd Nowitzki , Dietmar Wewers
IPC分类号： C01B31/36 , B01J19/32 , B01J19/00 , C01B33/025 , C01B33/02
CPC分类号： C01B33/025 , C01B32/05 , C01B32/956
摘要： The invention relates to a complete method for producing pure silicon that is suitable for use as solar-grade silicon, comprising the reduction of a silicon oxide, purified by acidic precipitation from an aqueous solution of a silicon oxide dissolved in an aqueous phase, using one or more pure carbon sources, the purified silicon oxide being obtained, in particular, by the precipitation of a silicon oxide dissolved in an aqueous phase in an acidifier. The invention also relates to a formulation containing an activator and to a device for producing silicon, a reactor and electrodes.
摘要翻译：本发明涉及一种适用于太阳能级硅的纯硅生产的完整方法，其中包括通过酸性沉淀从溶解在水相中的氧化硅水溶液中纯化的氧化硅，使用一种或更多的纯碳源，纯化的氧化硅，特别是通过在酸化器中沉淀溶解在水相中的氧化硅。本发明还涉及含有活化剂和用于生产硅，反应器和电极的装置的制剂。

48. 发明申请

US20110182796A1 METHOD FOR THE PYROLYSIS OF CARBOHYDRATES 审中-公开
标题翻译：碳水化合物的分解方法
公开(公告)号：US20110182796A1
公开(公告)日：2011-07-28
申请号：US13121758
申请日：2009-09-28
申请人： Juergen Erwin Lang , Alfons Karl , Hartwig Rauleder , Ekkehard Mueh , Guido Stochniol
发明人： Juergen Erwin Lang , Alfons Karl , Hartwig Rauleder , Ekkehard Mueh , Guido Stochniol
IPC分类号： C01B33/025 , C01B33/02
CPC分类号： C01B33/025 , C01B32/20
摘要： The present invention relates to methods for the technical pyrolysis of a carbohydrate or carbohydrate mixture at an elevated temperature while adding silicon oxide, to a pyrolysis product obtainable in this way, and to the use thereof as a reducing agent for the production of solar silicon from silicic acid and carbon at a high temperature.
摘要翻译：本发明涉及在高温下对碳水化合物或碳水化合物混合物进行技术热解同时加入氧化硅的方法，涉及以这种方式获得的热解产物及其作为用于生产太阳能硅的还原剂的用途硅酸和碳在高温下。

49. 发明授权

US07939597B2 Acrylic acid and water-absorbing polymer structures based on renewable raw materials and process for their production by dehydration 有权
标题翻译：基于可再生原料的丙烯酸和吸水聚合物结构及其脱水生产工艺
公开(公告)号：US07939597B2
公开(公告)日：2011-05-10
申请号：US12438256
申请日：2007-08-22
申请人： Günther Bub , Jürgen Mosler , Franz-Felix Kuppinger , Andreas Sabbagh , Guido Stochniol , Jörg Sauer , Markus Winterberg , Udo Knippenberg , Günter Latoschinski , Franck Furno , Thorsten Schwärtzke , Jörg Leistner
发明人： Günther Bub , Jürgen Mosler , Franz-Felix Kuppinger , Andreas Sabbagh , Guido Stochniol , Jörg Sauer , Markus Winterberg , Udo Knippenberg , Günter Latoschinski , Franck Furno , Thorsten Schwärtzke , Jörg Leistner
IPC分类号： C08L33/02 , C07C51/16 , C08F20/06 , B01J8/04
CPC分类号： B01J19/2415 , B01J8/025 , B01J8/22 , B01J10/002 , B01J19/006 , B01J19/32 , B01J2208/00176 , B01J2208/0053 , B01J2219/0004 , B01J2219/00081 , B01J2219/00094 , B01J2219/00159 , B01J2219/00768 , B01J2219/185 , B01J2219/1943 , B01J2219/32279 , B01J2219/32286 , C07C45/52 , C07C51/252 , C08F2/00 , C08F2/20 , C08F220/06 , C07C47/22 , C07C57/04
摘要： The present invention relates to a process for production of acrylic acid, comprising the steps of a) dehydration of glycerine to an acrolein-comprising dehydration product; b) gas phase oxidation of the dehydration product to obtain an acrylic acid-comprising monomer gas; c) bringing into contact of the monomer gas with a quench agent to obtain an acrylic acid-comprising quench phase; and d) work-up of the quench phase to obtain an acrylic acid-comprising monomer phase; whereby, during the dehydration a liquid phase a1 and a gas phase a2 is present, whereby in the liquid phase a1 a plurality of gas bubbles is generated, as well as a process for production of polymers by polymerization of acrylic acid, preferably for production of water-absorbing polymers, the water-absorbing polymers obtainable by this process, a composite, a process for production of a composite, the composite obtainable by this process, and further chemical products.
摘要翻译：本发明涉及一种生产丙烯酸的方法，包括以下步骤：a）将甘油脱水为含丙烯醛的脱水产物; b）脱水产物的气相氧化，得到含丙烯酸的单体气体; c）使单体气体与骤冷剂接触以获得含丙烯酸的淬火相; 和d）淬火阶段的后处理以获得含丙烯酸的单体相; 由此，在脱水时，存在液相a1和气相a2，由此在液相a1中产生多个气泡，以及通过丙烯酸的聚合制备聚合物的方法，优选用于生产吸水聚合物，通过该方法获得的吸水聚合物，复合材料，复合材料的制造方法，可通过该方法获得的复合材料，以及其他化学产品。

50. 发明申请

US20090239995A1 ACRYLIC ACID AND WATER-ABSORBING POLYMER STRUCTURES BASED ON RENEWABLE RAW MATERIALS AND PROCESS FOR THEIR PRODUCTION BY DEHYDRATION 有权
标题翻译：基于可再生原料的丙烯酸和吸水聚合物结构及其脱水生产工艺
公开(公告)号：US20090239995A1
公开(公告)日：2009-09-24
申请号：US12438256
申请日：2007-08-22
申请人： Günther Bub , Jürgen Mosler , Franz-Felix Kuppinger , Andreas Sabbagh , Guido Stochniol , Jörg Sauer , Markus Winterberg , Udo Knippenberg , Günter Latoschinski , Franck Furno
发明人： Günther Bub , Jürgen Mosler , Franz-Felix Kuppinger , Andreas Sabbagh , Guido Stochniol , Jörg Sauer , Markus Winterberg , Udo Knippenberg , Günter Latoschinski , Franck Furno
IPC分类号： C08L33/02 , C07C51/16 , C08F20/06 , B01J8/04
CPC分类号： B01J19/2415 , B01J8/025 , B01J8/22 , B01J10/002 , B01J19/006 , B01J19/32 , B01J2208/00176 , B01J2208/0053 , B01J2219/0004 , B01J2219/00081 , B01J2219/00094 , B01J2219/00159 , B01J2219/00768 , B01J2219/185 , B01J2219/1943 , B01J2219/32279 , B01J2219/32286 , C07C45/52 , C07C51/252 , C08F2/00 , C08F2/20 , C08F220/06 , C07C47/22 , C07C57/04
摘要： The present invention relates to a process for production of acrylic acid, comprising the steps of a) dehydration of glycerine to an acrolein-comprising dehydration product; b) gas phase oxidation of the dehydration product to obtain an acrylic acid-comprising monomer gas; c) bringing into contact of the monomer gas with a quench agent to obtain an acrylic acid-comprising quench phase; and d) work-up of the quench phase to obtain an acrylic acid-comprising monomer phase; whereby, during the dehydration a liquid phase a1 and a gas phase a2 is present, whereby in the liquid phase a1 a plurality of gas bubbles is generated, as well as a process for production of polymers by polymerisation of acrylic acid, preferably for production of water-absorbing polymers, the water-absorbing polymers obtainable by this process, a composite, a process for production of a composite, the composite obtainable by this process, and further chemical products.
摘要翻译：本发明涉及一种生产丙烯酸的方法，包括以下步骤：a）将甘油脱水为含丙烯醛的脱水产物; b）脱水产物的气相氧化，得到含丙烯酸的单体气体; c）使单体气体与骤冷剂接触以获得含丙烯酸的淬火相; 和d）淬火阶段的后处理以获得含丙烯酸的单体相; 由此，在脱水期间，存在液相a1和气相a2，由此在液相a1中产生多个气泡，以及通过丙烯酸的聚合制备聚合物的方法，优选用于生产吸水聚合物，通过该方法获得的吸水聚合物，复合材料，复合材料的制造方法，可通过该方法获得的复合材料，以及其他化学产品。

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