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41. 发明授权

US4263209A Aromatic dianhydrides 失效
标题翻译：芳香族二酐
公开(公告)号：US4263209A
公开(公告)日：1981-04-21
申请号：US114004
申请日：1980-01-21
申请人： Edmund P. Woo
发明人： Edmund P. Woo
IPC分类号： C07C57/34 , C07C59/64 , C07D309/32 , C07D307/60
CPC分类号： C07D309/32 , C07C57/34 , C07C59/64
摘要： Novel aromatic dianhydride compounds are described of the formula ##STR1## wherein Ar, R' and R" are named substituents, and both x's are either zeros or ones.
摘要翻译：描述了新颖的芳族二酐化合物，其分子式为“IMAGE”，其中Ar，R'和R“被命名为取代基，并且两者都是零或一个。

42. 发明授权

US06514632B1 Fluorene-containing polymers and compounds useful in the preparation thereof 有权
标题翻译：含有芴的聚合物和可用于其制备的化合物
公开(公告)号：US06514632B1
公开(公告)日：2003-02-04
申请号：US09661264
申请日：2000-09-13
申请人： Edmund P. Woo , William R. Shiang , Michael Inbasekaran , Gordon R. Roof , Mark T. Bernius , Weishi Wu
发明人： Edmund P. Woo , William R. Shiang , Michael Inbasekaran , Gordon R. Roof , Mark T. Bernius , Weishi Wu
IPC分类号： B32B900
CPC分类号： H01L51/0043 , C07C17/2637 , C07C17/266 , C07C25/22 , C07C25/24 , C07C211/48 , C07C2602/44 , C07C2603/18 , C08G61/00 , C08G61/02 , C08G61/10 , C09B69/105 , C09B69/109 , C09K11/06 , C09K2211/1408 , C09K2211/1416 , H01L51/0036 , H01L51/0037 , H01L51/0038 , H01L51/0039 , H01L51/0042 , H01L51/0052 , H01L51/0059 , H01L51/0062 , H01L51/007 , H01L51/0081 , H01L51/42 , H01L51/5012 , H01L2251/308 , Y10S428/917
摘要： A compound of the formula: and compounds of the formulas: wherein R1 is independently in each occurrence C1-20 hydrocarbyl or C1-20 hydrocarbyl containing one or more S, N, O, P or Si atoms, C4-16 hydrocarbyl carbonyloxy, C4-16 aryl(trialkylsiloxy) or both R1 may form with the 9-carbon on the fluorene ring a C5-20 ring structure or a C4-20 ring structure containing one or more heteroatoms of S, N or O; R2 is independently in each occurrence C1-20 hydrocarbyl, C120 hydrocarbyloxy, C1-20 thioether, C1-20 hydrocarbylcarbonyloxy or cyano; R3 is independently in each occurrence C1-20 hydrocarbyl or C1-20 hydrocarbyl substituted with di(C1-20 alkyl)amino, C1-20 hydrocarbyloxy or C1-20 hydrocarbyl or tri(C1-10 alkyl)siloxy; a is independently in each occurrence 0 or 1; X is independently in each occurrence a halogen moiety; and Z is independently in each occurrence —B(OH)2, —B(OR4)2 or wherein R4 is independently in each occurrence a C1-10 alkyl group and, R5 is independantly in each occurrence a C2-10 alkylene group.
摘要翻译：下式的化合物和下式的化合物：其中R 1在每次出现时独立地为C 1-20烃基或含有一个或多个S，N，O，P或Si原子的C 1-20烃基，C 4-16烃基羰氧基，C 4 -16芳基（三烷基甲硅烷氧基）或两者R 1可以与芴环上的9-碳形成C5-20环结构或含有一个或多个S，N或O杂原子的C 4-20环结构; R 2各自独立地表示 C 1-20烃基，C 1-20烃基羰基氧基或氰基; R 3在每次出现时独立地为C 1-20烃基或被二（C 1-20烷基）氨基取代的C 1-20烃基，C 1-20 烃氧基或C 1-20烃基或三（C 1-10烷基）甲硅烷氧基; a各自独立地为0或1; X各自独立地为卤素部分; 和Z各自独立地为-B（OH）2，-B（OR 4）2或其中R 4在每次出现时独立地为C 1-10烷基，并且R 5在每次出现时独立地为C 2-10亚烷基。

43. 发明授权

US06309763B1 Fluorene-containing polymers and electroluminescent devices therefrom 失效
标题翻译：含芴聚合物及其电致发光器件
公开(公告)号：US06309763B1
公开(公告)日：2001-10-30
申请号：US09063615
申请日：1998-04-21
申请人： Edmund P. Woo , Mark T. Bernius , Michael Inbasekaran , Weishi Wu
发明人： Edmund P. Woo , Mark T. Bernius , Michael Inbasekaran , Weishi Wu
IPC分类号： C08G6100
CPC分类号： H05B33/14 , C07C25/22 , C08G61/00 , C08G61/02 , C08G61/12 , C08G73/02 , C08G73/026 , C09K11/06 , H01L51/0039 , H01L51/0043 , H01L51/0059 , H01L51/5012 , Y10S428/917 , Y10T428/31678
摘要： A copolymer comprising 10-90 percent by weight of groups of Formula (I): and from 10-90 percent by weight of groups selected from Formulas (II), (III), and (IV): and mixtures thereof; wherein R1 is independently in each occurrence H, C1-C20 hydrocarbyl or C1-C20 hydrocarbyl containing one or more S, N, O, P or Si atoms, C4-C16 hydrocarbyl carbonyloxy, C4-C16 aryl(trialkylsiloxy) or both R1 may form with the 9-carbon on the fluorene ring a C5-C20 cycloaliphatic structure or a C4-C20 cycloaliphatic structure containing one or more heteroatoms of S, N, or O; R2 is independently in each occurrence C1-C20 hydrocarbyl, C1-C20 hydrocarbyloxy, C1-C20 thioether, C1-C20 hydrocarbylcarbonyloxy or cyano; R3 is independently in each occurrence carboxyl, C1-C20 alkyl, C1-C20 alkoxy or a group of the formula —CO2R4 wherein R4 is a C1-C20 alkyl; and a and b are independently in each occurrence an integer from 0 to 3.
摘要翻译：包含10-90重量％的式（I）的基团和10-90重量％的选自式（II），（III）和（IV）的基团的共聚物及其混合物; 其中R 1在每次出现时独立地为H，C 1 -C 20烃基或含有一个或多个S，N，O，P或Si原子的C 1 -C 20烃基，C 4 -C 16烃基羰氧基，C 4 -C 16芳基（三烷基甲硅烷氧基）或两个R 1 与芴环上的9-碳形成C5-C20脂环族结构或含有一个或多个S，N或O的杂原子的C 4 -C 20脂环族结构; R2各自独立地为C1-C20烃基，C1-C20烃氧基，C1-C20硫醚，C1-C20烃基羰基氧基或氰基; R3各自独立地为羧基，C 1 -C 20烷基，C 1 -C 20烷氧基或式-CO 2 R 4基团，其中R 4为C 1 -C 20烷基; 并且a和b各自独立地为0至3的整数。

44. 发明授权

US5929194A Crosslinkable or chain extendable polyarylpolyamines and films thereof 失效
标题翻译：可交联或可链可延伸的聚芳基多胺及其膜
公开(公告)号：US5929194A
公开(公告)日：1999-07-27
申请号：US967348
申请日：1997-10-27
申请人： Edmund P. Woo , Michael Inbasekaran , William R. Shiang , Gordon R. Roof
发明人： Edmund P. Woo , Michael Inbasekaran , William R. Shiang , Gordon R. Roof
IPC分类号： C08G73/02 , C09K11/06 , H01L51/30 , H01L51/50 , C08G12/00 , C08G69/26 , C08G73/00
CPC分类号： H01L51/5012 , C08G73/02 , C08G73/026 , C09K11/06 , H01L51/0035 , H01L51/0059 , H01L51/0052
摘要： The invention relates to poly(tertiary di- or polyarylamines) which have more than one aryl moiety which is further substituted with a moiety capable of chain extension or crosslinking. In another aspect, the invention relates to poly(tertiary di- or polyarylamines) which have more than one aryl moiety which is further substituted with a moiety capable of chain extension or crosslinking which are partially or completely crosslinked or chain extended. The invention further relates to films prepared from such chain extended or crosslinked poly(tertiary di- or polyarylamines). The invention further relates to electrophotographic devices and electroluminescent devices, such as polymeric light-emitting diodes, containing such films.
摘要翻译：本发明涉及具有多于一个芳基部分的聚（叔二或多芳基胺），其进一步被能够扩链或交联的部分取代。在另一方面，本发明涉及具有多于一个芳基部分的聚（叔二或多芳基胺），其进一步被部分或完全交联或链延长的能够扩链或交联的部分取代。本发明还涉及由这种扩链或交联的聚（叔二或多芳基胺）制备的膜。本发明还涉及包含这种膜的电子照相设备和电致发光器件，例如聚合物发光二极管。

45. 发明授权

US5777070A Process for preparing conjugated polymers 失效
标题翻译：共轭聚合物的制备方法
公开(公告)号：US5777070A
公开(公告)日：1998-07-07
申请号：US956797
申请日：1997-10-23
申请人： Michael Inbasekaran , Weishi Wu , Edmund P. Woo
发明人： Michael Inbasekaran , Weishi Wu , Edmund P. Woo
IPC分类号： C08G61/00 , C08G61/02 , H01L51/00 , H01L51/30 , H01L51/50 , C08G79/08
CPC分类号： H01L51/0039 , C08G61/02 , H01L51/0036 , H01L51/0043 , H01L51/0035 , H01L51/0059 , H01L51/5012
摘要： A process for preparing conjugated polymers which comprises contacting (i) monomers having two reactive groups selected from boronic acid, C.sub.1 -C.sub.6 boronic acid ester, C.sub.1 -C.sub.6 borane, and combinations thereof, with aromatic dihalide-functional monomers or (ii) monomers having one reactive boronic acid, boronic acid ester, or borane group and one reactive halide-functional group, with each other; (wherein the monomers are selected so that the polymerization reaction product of such has conjugated unsaturated internal groups) in a reaction mixture which contains: (a) an organic solvent in which the polymer forms at least a 1 percent solution; (b) an aqueous solution of an inorganic base having a pKa in the range of from 9 to 13, said solution having a concentration of at least 0.1N; (c) a catalytic amount of a palladium complex; and (d) at least 0.01 mole percent of a phase transfer catalyst, based on the number of moles of boronic acid, boric acid ester, and borane groups in the reaction mixture; under reaction conditions sufficient to form the corresponding conjugated polymer.
摘要翻译：制备共轭聚合物的方法，其包括使（i）具有选自硼酸，C 1 -C 6硼酸酯，C 1 -C 6甲硼烷及其组合的两个反应性基团的单体与芳族二卤化物官能单体或（ii）具有一种反应性硼酸，硼酸酯或硼烷基和一种反应性卤化物官能团; （其中选择单体，使得其聚合反应产物具有共轭不饱和内部基团）在反应混合物中，其包含：（a）其中聚合物形成至少1％溶液的有机溶剂; （b）具有pKa在9-13范围内的无机碱的水溶液，所述溶液的浓度至少为0.1N; （c）催化量的钯络合物; 和（d）基于反应混合物中硼酸，硼酸酯和硼烷基团的摩尔数的至少0.01摩尔％的相转移催化剂; 在足以形成相应共轭聚合物的反应条件下。

46. 发明授权

US5708130A 2,7-aryl-9-substituted fluorenes and 9-substituted fluorene oligomers and polymers 失效
公开(公告)号：US5708130A
公开(公告)日：1998-01-13
申请号：US508942
申请日：1995-07-28
申请人： Edmund P. Woo , William R. Shiang , Michael Inbasekaran , Gordon R. Roof
发明人： Edmund P. Woo , William R. Shiang , Michael Inbasekaran , Gordon R. Roof
IPC分类号： C07C17/26 , C07C17/266 , C07C25/22 , C07C25/24 , C07C43/225 , C07C69/00 , C07C211/48 , C08G61/00 , C08G61/02 , C08G61/10 , C09K11/06 , H01L21/28 , H01L21/336 , H01L21/66 , H01L29/423 , H01L51/00 , H01L51/30 , H01L51/42 , H01L51/50
CPC分类号： H01L51/0052 , C07C17/2637 , C07C17/266 , C07C211/48 , C07C25/22 , C07C25/24 , C08G61/00 , C08G61/02 , C08G61/10 , C09K11/06 , H01L21/28035 , H01L21/28167 , H01L22/20 , H01L29/42364 , H01L29/42376 , H01L29/66575 , H01L51/0039 , H01L51/0043 , H01L51/0058 , C07C2103/18 , H01L51/0094 , H01L51/42 , H01L51/5012 , Y10S428/917 , Y10T428/3154
摘要： The invention relates to 2,7-substituted-9-substituted fluorenes and 9-substituted fluorene oligomers and polymers. The fluorenes, oligomers and polymers are substituted at the 9-position with two hydrocarbyl moieties which may optionally contain one or more of sulfur, nitrogen, oxygen, phosphorous or silicon heteroatoms; a C.sub.5-20 ring structure formed with the 9-carbon on the fluorene ring or a C.sub.4-20 ring structure formed with the 9-carbon containing one or more heteroatoms of sulfur, nitrogen or oxygen; or a hydrocarbylidene moiety. In one embodiment, the fluorenes are substituted at the 2- and 7-positions with aryl moieties which may further be substituted with moieties which are capable of crosslinking or chain extension or a trialkylsiloxy moiety. The fluorene polymers and oligomers may be substituted at the 2- and 7'-positions. The monomer units of the fluorene oligomers and polymers are bound to one another at the 2- and 7'-positions. The 2,7'-aryl-9-substituted fluorene oligomers and polymers may be further reacted with one another to form higher molecular weight polymers by causing the optional moieties on the terminal 2,7'-aryl moieties, which are capable of crosslinking or chain extension, to undergo chain extension or crosslinking. Also disclosed are processes for preparing the disclosed compounds.

47. 发明授权

US5322916A Method for the preparation of amide oligomers and polybenzazole polymers therefrom 失效
标题翻译：用于制备酰胺低聚物和聚吲哚聚合物的方法
公开(公告)号：US5322916A
公开(公告)日：1994-06-21
申请号：US33680
申请日：1993-03-16
申请人： James J. O'Brien , Edmund P. Woo
发明人： James J. O'Brien , Edmund P. Woo
IPC分类号： C08G69/26 , C08G73/22 , C08G63/00
CPC分类号： C08G73/22 , C08G69/26
摘要： A polyamide precursor of a polybenzazole polymer is prepared by reacting an aromatic bis(alkenyl)ester with a ring forming, aromatic diamine. The precursor can be prepared in an organic solvent for the monomers to form a soluble polyamide precursor which can be subsequently cyclocondensed to form a PBX polymer. A polybenzoxazole precursor is prepared by the reaction of a bis(alkenyl)ester and a bis(ortho-hydroxyamine). A polybenzazole polymer is easily prepared by heating the polyamide, PBX precursor.
摘要翻译：通过使芳族双（烯基）酯与形成环的芳族二胺反应来制备聚吲哚聚合物的聚酰胺前体。该前体可以在有机溶剂中制备用于单体以形成可溶性聚酰胺前体，其可随后环化以形成PBX聚合物。聚苯并恶唑前体通过双（烯基）酯和双（邻羟基胺）的反应制备。通过加热聚酰胺，PBX前体，容易制备聚吲哚聚合物。

48. 发明授权

US5264538A Cyclic poly(aryl ether) oligomers 失效
标题翻译：环状聚（芳基醚）低聚物
公开(公告)号：US5264538A
公开(公告)日：1993-11-23
申请号：US544718
申请日：1990-06-27
申请人： Michael J. Mullins , Edmund P. Woo , Kimberly E. Balon , Daniel J. Murray , Cheng-Cheng C. Chen
发明人： Michael J. Mullins , Edmund P. Woo , Kimberly E. Balon , Daniel J. Murray , Cheng-Cheng C. Chen
IPC分类号： C07C45/46 , C07C49/84 , C07D323/00 , C07D327/00 , C08G65/40 , C08L71/00 , C08G2/00 , C08G75/00
CPC分类号： C08G65/4081 , C07C45/46 , C07C49/84 , C07D323/00 , C07D327/00 , C08L71/00
摘要： Cyclic poly(aryl ether) oligomers and mixtures thereof, and methods for the preparation thereof in a highly dilute reaction medium under reaction conditions favorable for ring closure at low degrees of polymerization. These oligomers are represented by the general formula ##STR1## where each Y is divalent oxygen or divalent sulfur, each Ar is an aromatic diradical which comprises one or more C.sub.6 to C.sub.20 arylene groups and has at least one electron withdrawing group attached to an aromatic ring, and n is an integer from 1 to about 20 with the proviso that for integer values of n equal to 1 or 2 all linkages between independent aromatic rings comprise at least one atom.
摘要翻译：环状聚（芳基醚）低聚物及其混合物，以及在高度稀释的反应介质中在低聚合度下有利于闭环的反应条件下制备的方法。这些低聚物由通式“IMAGE”表示，其中每个Y是二价氧或二价硫，每个Ar是包含一个或多个C 6至C 20亚芳基且具有至少一个连接到芳环上的吸电子基团的芳族双基并且n为1至约20的整数，条件是对于等于1或2的整数值，独立芳环之间的所有键均包含至少一个原子。

49. 发明授权

US4880884A Poly(aryl ether)-poly(aryl carbonate) block copolymers and their preparation 失效
标题翻译：聚（芳基醚） - 聚（芳基碳酸酯）嵌段共聚物及其制备方法
公开(公告)号：US4880884A
公开(公告)日：1989-11-14
申请号：US186997
申请日：1988-04-27
申请人： Michael J. Mullins , Steven P. Crain , Edmund P. Woo , Daniel J. Murray
发明人： Michael J. Mullins , Steven P. Crain , Edmund P. Woo , Daniel J. Murray
IPC分类号： C08G64/18 , C08G64/42
CPC分类号： C08G64/183 , C08G64/42
摘要： A method for preparing novel poly(aryl ether)-(poly aryl carbonate) block copolymers by the decarboxylation of copolycarbonates prepared by the condensation of two different aromatic dihydroxy compounds and a carbonate precursor such as phosgene. At least one of the aromatic diols must have at least one electron-withdrawing group located in a position ortho or para to at least one of its hydroxy groups and at least one of the diols must not have any electron-withdrawing groups in a position ortho or para to either of its hydroxy groups. The method is particularly effective in making crystalline block copolymers.
摘要翻译：通过使两种不同的芳族二羟基化合物和碳酸酯前体如光气缩合制备的共聚碳酸酯的脱羧来制备新的聚（芳基醚） - （聚芳基碳酸酯）嵌段共聚物的方法。至少一种芳族二醇必须具有位于至少一个羟基的邻位或对位的至少一个吸电子基团，并且至少一个二醇在邻位不能具有任何吸电子基团或对位于其任一羟基。该方法在制备结晶嵌段共聚物中特别有效。

50. 发明授权

US4751323A Novel polyaromatic cyanates 失效
标题翻译：新型多芳香族氰酸酯
公开(公告)号：US4751323A
公开(公告)日：1988-06-14
申请号：US552234
申请日：1983-11-16
申请人： Edmund P. Woo , Daniel J. Murray
发明人： Edmund P. Woo , Daniel J. Murray
IPC分类号： C07C67/00 , C07C261/02 , C07C313/00 , C07D261/02 , C07D495/00 , C07D495/08 , C08G18/76 , C08G73/00 , C08G73/06 , C07C69/00 , C07D335/04 , C08G63/38
CPC分类号： C08G73/0655 , C07C261/02 , C07C2103/68
摘要： This invention relates to a polyaromatic cyanate which corresponds to the formula ##STR1## wherein Ar is an aromatic radical;B is a C.sub.7-20 polycyclic aliphatic radical;D is independently in each occurrence any non-active hydrogen-containing substituent;q, r and s are independently in each occurrence the integers b 0, 1, 2, l or b 3l ; with the proviso that the sum of q, 4 and s is greater than or equal to 2;t is independently in each occurrence an integer of between about 0 and 4 inclusive; andx is a number between about 0 and 5 inclusive.Another aspect of this invention is a novel polytriazine which comprises the reaction product of the polyaromatic cyanate esters of this invention. The novel polytriazines may further comprise the reaction product of the novel polyaromatic cyanates of this invention in admixture with other cyanates known in the art as useful for the preparation of polytriazines.
摘要翻译：本发明涉及对应于式“IMAGE”的多芳族氰酸酯，其中Ar是芳族基团; B是C7-20多环脂族基团; D在每次出现时都是独立的任何非活性含氢取代基; q，r和s在每次出现时独立地为整数b 0,1,2,1或b 3l; 条件是q，4和s之和大于或等于2; t在每次出现时独立地为约0和4之间的整数; x是包括0和5之间的数字。本发明的另一方面是一种新的聚三嗪，其包括本发明的多芳族氰酸酯的反应产物。新颖的三叉嗪可以进一步包括本发明的新型多芳族氰酸酯与本领域已知的用于制备聚三嗪的其它氰酸酯的混合物的反应产物。

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