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41. 发明授权

US4267120A Polyester polycarbonates 失效
标题翻译：聚酯聚碳酸酯
公开(公告)号：US4267120A
公开(公告)日：1981-05-12
申请号：US103757
申请日：1979-12-14
申请人： Michael Cuscurida , George P. Speranza
发明人： Michael Cuscurida , George P. Speranza
IPC分类号： C08G63/00 , C08G18/44 , C08G63/64 , C08G64/18 , C08G64/34 , C07C69/96 , C08G63/62
CPC分类号： C08G64/183 , C08G18/44 , C08G63/64 , C08G64/34 , C08G2105/02 , Y10S521/902
摘要： Covers polyester polycarbonates of the structure: ##STR1## wherein X and Y, independently, are H, methyl, or ethyl, m and n independently are integers of 1-5, R is a nucleus of a glycol selected from the group of lower alkylene glycols and polyalkylene glycols of up to about 600 molecular weight, Z is an organic radical from a cyclic organic acid anhydride having 4-20 carbon atoms, and r is an integer of 1-5.Also covers a method of preparing said polyester polycarbonates as well as polyurethanes derived therefrom, as well as polyisocyanurate polymers containing both isocyanurate linkages and urethane linkages.
摘要翻译：包括以下结构的聚酯聚碳酸酯：其中X和Y独立地是H，甲基或乙基，m和n独立地为1-5的整数，R是选自低级亚烷基的二醇的核心乙二醇和高达约600分子量的聚亚烷基二醇，Z是具有4-20个碳原子的环状有机酸酐的有机基团，r是1-5的整数。还涉及制备所述聚酯聚碳酸酯的方法以及由其衍生的聚氨酯，以及含有异氰脲酸酯键和氨基甲酸酯键的聚异氰脲酸酯聚合物。

42. 发明授权

US4021383A Infused polymer containing monohydric compounds and polyurethane compositions based thereon 失效
标题翻译：含有一羟基化合物的输入聚合物和基于其的聚氨酯组合物
公开(公告)号：US4021383A
公开(公告)日：1977-05-03
申请号：US642979
申请日：1975-12-22
申请人： Michael Cuscurida , Lee G. Meyer , Lewis W. Watts, Jr.
发明人： Michael Cuscurida , Lee G. Meyer , Lewis W. Watts, Jr.
IPC分类号： C08F283/06 , C08F299/02 , C08G18/28 , C08G18/62 , C08G18/63 , C08G18/67 , C08G18/69 , C08G18/76 , C08G18/14
CPC分类号： C08G18/69 , C08F283/06 , C08F299/02 , C08G18/283 , C08G18/62 , C08G18/635 , C08G18/6795 , C08G18/7607
摘要： Disclosed is a novel infused polymer containing monohydric composition useful in producing improved urethane products. The novel composition is characterized as a polymer containing monohydric composition wherein the polymeric moiety is chemically attached or "infused" into the unsaturation sites of an oxyalkadienyl moiety which is covalently bonded to an acyclic monohydric compound.
摘要翻译：公开了一种含有一羟基化合物的新型注入聚合物，其可用于生产改进的聚氨酯产品。该新型组合物的特征在于含有一元组合物的聚合物，其中聚合物部分化学连接或“注入”共价连接到无环一羟基化合物的氧化烯二烯基部分的不饱和位点。

43. 发明授权

US5723565A Epoxy curing agents 失效
标题翻译：环氧固化剂
公开(公告)号：US5723565A
公开(公告)日：1998-03-03
申请号：US44791
申请日：1993-04-12
申请人： Michael Cuscurida , Kathy Beth Sellstrom
发明人： Michael Cuscurida , Kathy Beth Sellstrom
IPC分类号： C08G59/50 , C08L63/00 , C08L69/00 , C08G59/62
CPC分类号： C08L63/00 , C08G59/50 , C08L69/00
摘要： An epoxy resin composition comprises the cured reaction product of an epoxy base resin and a curing agent mixture. The curing agent mixture comprises an amino curative and a polyoxyalkylene polycarbonate. Liquid epoxy base resins cured with polyoxyalkyleneamines in the presence of polyoxyalkylene polycarbonates were harder and displayed improved tensile modulus, flexural strength and flexural modulus.
摘要翻译：环氧树脂组合物包含环氧基树脂和固化剂混合物的固化反应产物。固化剂混合物包含氨基固化剂和聚氧化烯聚碳酸酯。在聚氧化烯聚碳酸酯存在下用聚氧化烯胺固化的液态环氧基树脂更硬，显示出更好的拉伸模量，弯曲强度和弯曲模量。

44. 发明授权

US5405977A Process for removing organic halides from alkylene carbonates 失效
标题翻译：从碳酸亚烷基酯中除去有机卤化物的方法
公开(公告)号：US5405977A
公开(公告)日：1995-04-11
申请号：US45
申请日：1993-01-04
申请人： Michael Cuscurida , Edward T. Marquis
发明人： Michael Cuscurida , Edward T. Marquis
IPC分类号： C07D317/36 , C07B301/32
CPC分类号： C07D317/36
摘要： A method for removing organic halide contaminants from alkylene carbonates is disclosed. Organic halide contaminants are removed from alkylene carbonates by contacting the contaminated alkylene carbonate with hydrotalcite.
摘要翻译：公开了一种从碳酸亚烷基酯中除去有机卤化物污染物的方法。通过使污染的碳酸亚烷基酯与水滑石接触，从碳酸亚烷基酯中除去有机卤化物污染物。

45. 发明授权

US5344996A Catalyst removal from alcohol alkoxylates using acid clays 失效
标题翻译：使用酸性粘土从醇烷氧基化物中除去催化剂
公开(公告)号：US5344996A
公开(公告)日：1994-09-06
申请号：US955214
申请日：1992-10-01
申请人： Edward C. Nieh , Michael Cuscurida
发明人： Edward C. Nieh , Michael Cuscurida
IPC分类号： B01J20/12 , B01J38/00 , C07C41/36 , C07C41/44 , C07C43/04 , C08G65/02 , C08G65/30 , C07C43/11 , C07C41/00
CPC分类号： C08G65/30 , C07C41/36 , C07C41/44
摘要： The removal of basic alkaline earth metal catalysts from alcohol alkoxylate product streams using acid days wetted with water is described. The catalyst level may be reduced to 1 ppm or less in many instances. Effective acid days include, but are not limited to silica days, silica magnesia clays, alumina, montmorillonite days, mixtures thereof and the like. Contacting of the day with the alcohol alkoxylate may take place at ambient to 120.degree. C.
摘要翻译：描述了使用酸洗天然的水从醇烷氧基化物产物流中除去碱式碱土金属催化剂。在许多情况下，催化剂水平可以降低至1ppm或更低。有效的酸天包括但不限于二氧化硅天数，二氧化硅氧化镁粘土，氧化铝，蒙脱石天，以及它们的混合物等。一天与醇烷氧基化物的接触可以在环境温度至120℃下进行。

46. 发明授权

US5103062A Modified normally liquid, water-soluble polyoxyalkylene polyamines 失效
标题翻译：改性常规液体，水溶性聚氧化烯多胺
公开(公告)号：US5103062A
公开(公告)日：1992-04-07
申请号：US36955
申请日：1987-04-10
申请人： Michael Cuscurida , Ernest L. Yeakey
发明人： Michael Cuscurida , Ernest L. Yeakey
IPC分类号： C08G65/32 , C07C209/16 , C08G65/28
CPC分类号： C07C209/16
摘要： In accordance with the process of the present invention normally liquid, water-soluble poly(oxyethylene/oxypropylene) polyamine products are prepared using an initiator, which may contain oxyethylene groups. In a series of alkoxylation reaction steps the initiator is reacted with predetermined weight percentages of ethylene oxide and propylene oxide, said process comprising the steps of:a. Charging a predetermined percentage of initiator to an alkoxylation reaction zone,b. Alkoxylating said initiator therein with predetermined percentages of ethylene oxide and propylene oxide to provide an intermediate polyol,c. Propoxylating said intermediate polyol with a predetermined percentage of propylene oxide to provide a normally liquid, water-soluble precursor polyol, andd. Catalytically reductively aminating said precursor polyol in the presence of a reductive amination catalyst in a reaction zone under reductive amination conditions in the presence of ammonia and hydrogen to provide said water-soluble poly(oxyethylene/oxypropylene) polyamine product.
摘要翻译：根据本发明的方法，通常使用可含有氧乙烯基的引发剂来制备通常为水溶性的聚（氧乙烯/氧丙烯）多胺产物。在一系列烷氧基化反应步骤中，引发剂与预定重量百分比的环氧乙烷和环氧丙烷反应，所述方法包括以下步骤：a。将预定百分比的引发剂装入烷氧基化反应区，b。用预定百分比的环氧乙烷和环氧丙烷对所述引发剂进行烷氧基化以提供中间体多元醇，c。用预定百分比的环氧丙烷丙氧基化所述中间体多元醇以提供通常为液体的水溶性前体多元醇，和d。在还原胺化条件下，在氨和氢的存在下，在还原胺化催化剂存在下，在反应区域催化还原胺化所述前体多元醇，以提供所述水溶性聚（氧乙烯/氧丙烯）多胺产物。

47. 发明授权

US5072020A Aliphatic polyamines from polynitro compounds 失效
标题翻译：聚氨酯化合物的聚氨酯
公开(公告)号：US5072020A
公开(公告)日：1991-12-10
申请号：US496725
申请日：1990-03-21
申请人： George P. Speranza , Michael Cuscurida , Wei-Yang Su
发明人： George P. Speranza , Michael Cuscurida , Wei-Yang Su
IPC分类号： C07C271/26 , C07C269/00 , C07C271/28 , C08G18/10 , C08G18/83
CPC分类号： C07C271/28 , C07C269/00 , C08G18/10
摘要： Disclosed is a novel route to diamines and triamines comprising reacting nitroalcohols with isocyanates to prepare di- and trinitro compounds which are subsequently reduced over a metal hydrogenation catalyst to the corresponding polyamino compound.

48. 发明授权

US5059247A Method for the preparation of foundry sand compositions 失效
标题翻译：铸造砂组合物的制备方法
公开(公告)号：US5059247A
公开(公告)日：1991-10-22
申请号：US569896
申请日：1990-08-20
申请人： Wheeler C. Crawford , Michael Cuscurida
发明人： Wheeler C. Crawford , Michael Cuscurida
IPC分类号： B22C1/00 , B22C1/10 , B22C1/18 , B22C1/22 , B22C5/04
CPC分类号： B22C1/188
摘要： A foundry sand composition that is self-hardening after a working life of about 10-20 minutes that is composed of a foundry sand, a sodium silicate binder and a specifically defined polyester polycarbonate hardener is prepared by:a) mixing a foundry sand with about 2-6 wt. %, based on the foundry sand, of an aqueous solution containing about 40-60 wt. % of sodium silicate, the ratio of SiO.sub.2 /Na.sub.2 O of the sodium silicate about 2.2 to 3, to form an initial sand mixture, andb) then adding about 5-15 wt. % of the polyester polycarbonate hardener, based on the weight of the aqueous solution of sodium silicate, to provide the foundry sand composition.

49. 发明授权

US4996294A Preparation of aminotetramines 失效
标题翻译：氨基四胺的制备
公开(公告)号：US4996294A
公开(公告)日：1991-02-26
申请号：US429673
申请日：1989-10-31
申请人： Michael Cuscurida , Wei-Yang Su , George P. Speranza
发明人： Michael Cuscurida , Wei-Yang Su , George P. Speranza
IPC分类号： C08G18/50 , C08G65/26 , C08G65/28 , C08G65/325 , C08L63/00
CPC分类号： C08G65/3255 , C08G18/5024 , C08G65/2609 , C08L63/00 , C08G2120/00
摘要： A process in which an amine tetrol prepared by oxyalkylation of a propanediol with propylene oxide is catalytically aminated to provide, for example, an aminotetramine is disclosed. The aminotetramines are useful for preparing polyurea products and as curing agents for epoxy resins.
摘要翻译：公开了其中通过丙二醇与环氧丙烷的烷氧基化制备的胺四醇被催化胺化以提供例如氨基四胺。氨基四胺可用于制备聚脲产物和用作环氧树脂的固化剂。

50. 发明授权

US4761465A Difunctional isocyanate-terminated polyoxyalkylene diamine prepolymers and polymer coatings applications 失效
标题翻译：二异氰酸酯封端的聚氧亚烷基二胺预聚物和聚合物涂料应用
公开(公告)号：US4761465A
公开(公告)日：1988-08-02
申请号：US78314
申请日：1987-07-27
申请人： George P. Speranza , Jiang-Jen Lin , Michael Cuscurida
发明人： George P. Speranza , Jiang-Jen Lin , Michael Cuscurida
IPC分类号： C08G18/08 , C08G18/10 , C08G18/28 , C08G18/32 , C08G18/50 , C08G18/73 , C08G18/75 , C08G18/76 , C08G18/80
CPC分类号： C08G18/8061 , C08G18/0852 , C08G18/089 , C08G18/10 , C08G18/282 , C08G18/3228 , C08G18/5024 , C08G18/73 , C08G18/75 , C08G18/765 , C08G18/8038
摘要： Diisocyanate and polyoxyalkylene diamine reaction products which contain as the principle reaction component, a diamine having the formula: ##STR1## wherein R' independently represents hydrogen or methyl and x is a number having an average value of at least 1 to about 60 and a diisocyanate of the formula: ##STR2## The products of the invention are obtained by reacting a polyoxyalkylene diamine with an excess of diisocyanate in the presence of a polar solvent to obtain products with the following general structures: ##STR3## where B is alkyl group from diisocyanates. These products and the corresponding blocked isocyanate prepolymer are further used to prepare coatings by reaction with polyoxyalkylene polyamine.
摘要翻译：含有作为主要反应组分的二异氰酸酯和聚氧亚烷基二胺反应产物，具有下式的二胺：其中R'独立地表示氢或甲基，x是平均值至少为1至约60的数，和二异氰酸酯通过在极性溶剂的存在下使聚氧亚烷基二胺与过量的二异氰酸酯反应获得本发明的产物，得到具有以下一般结构的产物：其中B是二异氰酸酯的烷基。这些产物和相应的封端异氰酸酯预聚物进一步用于通过与聚氧化烯多胺反应来制备涂层。

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