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41. 发明授权

US08063560B2 Glass package that is hermetically sealed with a frit and method of fabrication 有权
标题翻译：用玻璃料和制造方法气密密封的玻璃包装
公开(公告)号：US08063560B2
公开(公告)日：2011-11-22
申请号：US11521888
申请日：2006-09-15
申请人： Bruce G. Aitken , Joel P. Carberry , Steven E. DeMartino , Henry E. Hagy , Lisa A. Lamberson , Richard J. Miller, II , Robert Morena , Joseph F. Schroeder, III , Alexander Streltsov , Sujanto Widjaja
发明人： Bruce G. Aitken , Joel P. Carberry , Steven E. DeMartino , Henry E. Hagy , Lisa A. Lamberson , Richard J. Miller, II , Robert Morena , Joseph F. Schroeder, III , Alexander Streltsov , Sujanto Widjaja
IPC分类号： H05B33/00
CPC分类号： C03C27/06 , C03C3/072 , C03C3/17 , C03C3/19 , C03C3/21 , C03C8/24 , C03C8/245 , C03C27/005 , H01L51/5246
摘要： A hermetically sealed glass package and method for manufacturing the hermetically sealed glass package are described herein using an OLED display as an example. Basically, the hermetically sealed OLED display is manufactured by providing a first substrate plate and a second substrate plate and depositing a frit onto the second substrate plate. OLEDs are deposited on the first substrate plate. An irradiation source (e.g., laser, infrared light) is then used to heat the frit which melts and forms a hermetic seal that connects the first substrate plate to the second substrate plate and also protects the OLEDs. The frit is glass that was doped with at least one transition metal and possibly a CTE lowering filler such that when the irradiation source heats the frit, it softens and forms a bond. This enables the frit to melt and form the hermetic seal while avoiding thermal damage to the OLEDs.
摘要翻译：这里使用OLED显示器作为示例来描述气密密封的玻璃封装和制造密封玻璃封装的方法。基本上，通过提供第一基板和第二基板并将玻璃料沉积到第二基板上来制造密封的OLED显示器。 OLED沉积在第一基板上。然后使用照射源（例如，激光，红外光）来加热玻璃料，其熔化并形成将第一衬底板连接到第二衬底板并且还保护OLED的气密密封。玻璃料是掺杂有至少一种过渡金属和可能的CTE降低填料的玻璃，使得当照射源加热玻璃料时，其软化并形成结合。这使得玻璃料熔化并形成气密密封，同时避免对OLED的热损伤。

42. 发明申请

US20100186449A1 HERMETICALLY SEALED GLASS PACKAGE AND METHOD OF FABRICATION 有权
标题翻译：密封玻璃包装和制造方法
公开(公告)号：US20100186449A1
公开(公告)日：2010-07-29
申请号：US12725648
申请日：2010-03-17
申请人： Bruce G. Aitken , Paul S. Danielson , James E. Dickinson, JR. , Stephan L. Longunov , Robert Morena , Mark L. Powley , Kamjula P. Reddy , Joseph F. Schroeder, III , Alexander Streltsov
发明人： Bruce G. Aitken , Paul S. Danielson , James E. Dickinson, JR. , Stephan L. Longunov , Robert Morena , Mark L. Powley , Kamjula P. Reddy , Joseph F. Schroeder, III , Alexander Streltsov
IPC分类号： C03B29/00
CPC分类号： C03B23/245 , C03C3/091 , C03C3/093 , C03C3/108 , C03C8/04 , C03C8/10 , C03C8/24 , C03C27/06 , H01L51/524 , H01L51/5246
摘要： A hermetically sealed glass package and method for manufacturing the hermetically sealed glass package are described herein using an OLED display as an example. In one embodiment, the hermetically sealed glass package is manufactured by providing a first substrate plate and a second substrate plate. The second substrate contains at least one transition or rare earth metal such as iron, copper, vanadium, manganese, cobalt, nickel, chromium, neodymium and/or cerium. A sensitive thin-film device that needs protection is deposited onto the first substrate plate. A laser is then used to heat the doped second substrate plate in a manner that causes a portion of it to swell and form a hermetic seal that connects the first substrate plate to the second substrate plate and also protects the thin film device. The second substrate plate is doped with at least one transition metal such that when the laser interacts with it there is an absorption of light from the laser in the second substrate plate, which leads to the formation of the hermetic seal while avoiding thermal damage to the thin-film device. Another embodiment of the hermetically sealed glass package and a method for manufacturing that hermetically sealed glass package are also described herein.
摘要翻译：这里使用OLED显示器作为示例来描述气密密封的玻璃封装和制造密封玻璃封装的方法。在一个实施例中，通过提供第一基板和第二基板制造密封的玻璃封装。第二基板包含至少一种过渡金属或稀土金属，例如铁，铜，钒，锰，钴，镍，铬，钕和/或铈。需要保护的敏感薄膜器件沉积到第一衬底板上。然后使用激光器以使其一部分膨胀并形成将第一衬底板连接到第二衬底板的气密密封件并且还保护薄膜器件的方式来加热掺杂的第二衬底板。第二衬底板掺杂有至少一种过渡金属，使得当激光与其相互作用时，吸收来自第二衬底板中的激光的光，这导致气密密封的形成，同时避免对薄膜装置。本文还描述了密封玻璃封装的另一个实施例以及密封玻璃封装的制造方法。

43. 发明授权

US07602121B2 Glass package that is hermetically sealed with a frit and method of fabrication 有权
标题翻译：用玻璃料和制造方法气密密封的玻璃包装
公开(公告)号：US07602121B2
公开(公告)日：2009-10-13
申请号：US11228803
申请日：2005-09-16
申请人： Bruce G. Aitken , Joel P. Carberry , Steven E. DeMartino , Henry E. Hagy , Lisa A. Lamberson , Richard J. Miller, II , Robert Morena , Joseph F. Schroeder, III , Alexander Streltsov , Sujanto Widjaja
发明人： Bruce G. Aitken , Joel P. Carberry , Steven E. DeMartino , Henry E. Hagy , Lisa A. Lamberson , Richard J. Miller, II , Robert Morena , Joseph F. Schroeder, III , Alexander Streltsov , Sujanto Widjaja
IPC分类号： H01J1/62
CPC分类号： C03C27/06 , C03C3/072 , C03C3/17 , C03C3/19 , C03C3/21 , C03C8/24 , C03C8/245 , C03C27/005 , H01L51/5246
摘要： A hermetically sealed glass package and method for manufacturing the hermetically sealed glass package are described herein using an OLED display as an example. Basically, the hermetically sealed OLED display is manufactured by providing a first substrate plate and a second substrate plate and depositing a frit onto the second substrate plate. OLEDs are deposited on the first substrate plate. An irradiation source (e.g., laser, infrared light) is then used to heat the frit which melts and forms a hermetic seal that connects the first substrate plate to the second substrate plate and also protects the OLEDs. The frit is glass that was doped with at least one transition metal and possibly a CTE lowering filler such that when the irradiation source heats the frit, it softens and forms a bond. This enables the frit to melt and form the hermetic seal while avoiding thermal damage to the OLEDs.
摘要翻译：这里使用OLED显示器作为示例来描述气密密封的玻璃封装和制造密封玻璃封装的方法。基本上，通过提供第一基板和第二基板并将玻璃料沉积到第二基板上来制造密封的OLED显示器。 OLED沉积在第一基板上。然后使用照射源（例如，激光，红外光）来加热玻璃料，其熔化并形成将第一衬底板连接到第二衬底板并且还保护OLED的气密密封。玻璃料是掺杂有至少一种过渡金属和可能的CTE降低填料的玻璃，使得当照射源加热玻璃料时，其软化并形成结合。这使得玻璃料熔化并形成气密密封，同时避免对OLED的热损伤。

44. 发明授权

US06756333B2 Devitrification-resistant chalcogenide glasses 有权
标题翻译：耐脱氮化硫族化物玻璃
公开(公告)号：US06756333B2
公开(公告)日：2004-06-29
申请号：US10290738
申请日：2002-11-08
申请人： Bruce G. Aitken
发明人： Bruce G. Aitken
IPC分类号： C03C332
CPC分类号： C03C3/321 , C03C4/10
摘要： The invention resides in a molecular, inorganic glass and a method of making the glass, the glass being vitreous and resistant to devitrification, that is composed, in substantial part at least, of thermally-stable, zero-dimensional clusters or molecules, composed of four atoms of arsenic and three atoms of sulfur, the glass further containing up to 12 atomic percent of germanium, adjoining clusters being bonded to each other primarily by van der Waals forces, and at least 95% of the glass composition consisting of 42-60% arsenic, 37-48% sulfur plus selenium, the selenium being 0-14%.
摘要翻译：本发明在于一种分子，无机玻璃和一种制造玻璃，玻璃是玻璃体并且耐失透的方法，其至少部分地由热稳定的零维簇或分子组成，其由四个原子的砷和三个原子的硫，玻璃还含有最多12原子％的锗，相邻的簇主要通过范德华力彼此结合，并且至少95％的玻璃组合物由42-60 ％砷，37-48％硫加硒，硒为0-14％。

45. 发明授权

US06573026B1 Femtosecond laser writing of glass, including borosilicate, sulfide, and lead glasses 有权
标题翻译：玻璃的飞秒激光写入，包括硼硅酸盐，硫化物和铅玻璃
公开(公告)号：US06573026B1
公开(公告)日：2003-06-03
申请号：US09628666
申请日：2000-07-28
申请人： Bruce G. Aitken , Nicholas F. Borrelli , David L. Morse , Alexander Streltsov
发明人： Bruce G. Aitken , Nicholas F. Borrelli , David L. Morse , Alexander Streltsov
IPC分类号： G02B618
CPC分类号： G11C13/041 , B23K26/0624 , C03C23/0025 , G02B6/13 , G02B2006/12107 , G02B2006/12147 , G02B2006/12171 , G11C13/04 , Y10S430/146
摘要： A method of writing a pattern, such as a waveguide, in a bulk glass substrate. The bulk glass substrate can be formed from, for example, borosilicate or sulfide or lead glass. A pulsed laser beam is focused within the substrate while the focus is translated relative to the substrate along a scan path at a scan speed effective to induce an increase in the refractive index of the material along the scan path. Substantially no laser induced physical damage of the material is incurred along the scan path. Various optical devices can be made using this method.
摘要翻译：在散装玻璃基板中写入诸如波导的图案的方法。散装玻璃基板可以由例如硼硅酸盐或硫化物或铅玻璃形成。脉冲激光束聚焦在衬底内，同时沿扫描路径相对于衬底平移焦点，扫描速度有效地引起材料沿着扫描路径的折射率的增加。基本上没有激光引起材料的物理损伤沿着扫描路径。可以使用这种方法制造各种光学装置。

46. 发明授权

US06520689B2 Optical fiber splicing method and device 失效
标题翻译：光纤拼接方法及装置
公开(公告)号：US06520689B2
公开(公告)日：2003-02-18
申请号：US09907351
申请日：2001-07-17
申请人： Steven E. DeMartino , Michael E. DeRosa , Bruce G. Aitken
发明人： Steven E. DeMartino , Michael E. DeRosa , Bruce G. Aitken
IPC分类号： G02B6255
CPC分类号： G02B6/3801 , G02B6/2551
摘要： A method for splicing optical fibers is disclosed. The fibers are held by ferrules with a softening temperature at least 30° C. below that of the lower of the glass transition temperatures of the fibers. The ends of the fibers are actively aligned and brought into contact, then energy is applied to fuse the ferrules together, maintaining the alignment of the ends of the fibers. The ferrules may be a low-melting inorganic glass, such as a lead bismuth borosilicate glass. The method and ferrules of the present invention are especially useful in splicing fibers of dissimilar thermomechanical properties.
摘要翻译：公开了一种拼接光纤的方法。纤维被软管温度保持在低于纤维的玻璃化转变温度较低的30℃以下的套管。纤维的端部被主动对准并且接触，然后施加能量以将套圈熔合在一起，保持纤维端部的对准。套圈可以是低熔点无机玻璃，例如硼酸铅铋硼玻璃。本发明的方法和套圈特别适用于不同的热机械性能的拼接纤维。

47. 发明授权

US06344425B1 Fluorotellurite, amplifier glasses 失效
标题翻译：荧光粉，放大镜
公开(公告)号：US06344425B1
公开(公告)日：2002-02-05
申请号：US09443903
申请日：1999-11-19
申请人： Bruce G. Aitken
发明人： Bruce G. Aitken
IPC分类号： C03C315
CPC分类号： H01S3/17 , C03C3/23 , C03C13/048 , H01S3/173
摘要： A family of fluorotellurite glasses, the composition of which consist essentially of, as calculated in mole percent, 30-75% TeO2, 15-60% ZnF2 and 0.005-10% of an oxide of erbium, thulium or holmium, and amplifying optical components produced from these glasses.
摘要翻译：一种含氟碲化物玻璃的组合物，其组成基本上由摩尔百分比计算为30-75％TeO 2，15-60％ZnF 2和0.005-10％铒，ium或钬氧化物，以及放大光学组分从这些眼镜生产。

48. 再颁专利

USRE36513E Gallium sulfide glasses 失效
标题翻译：硫化镓玻璃
公开(公告)号：USRE36513E
公开(公告)日：2000-01-18
申请号：US775706
申请日：1996-12-17
申请人： Bruce G. Aitken , Mark A. Newhouse
发明人： Bruce G. Aitken , Mark A. Newhouse
IPC分类号： G02B6/12 , C03C3/32 , C03C4/10 , C03C13/04 , C03C3/23
CPC分类号： C03C3/323 , C03C13/043 , C03C13/044 , C03C3/321 , C03C4/10 , Y10S501/904 , Y10T428/2929
摘要： This invention is directed broadly to transparent glasses exhibiting excellent transmission far into the infrared region of the electromagnetic radiation spectrum, those glasses consisting essentially, expressed in terms of mole percent, of 40-80% Ga.sub.2 S.sub.3, 0-35% RS.sub.x, wherein R is at least one network forming cation selected from the group consisting of aluminum, antimony, arsenic, germanium, and indium, 1-50% Ln.sub.2 S.sub.3, wherein Ln is at least one cation selected from the group consisting of a rare earth metal cation and yttrium, 1-45% MS.sub.x, wherein M is at least one modifying metal cation selected from the group consisting of barium, cadmium, calcium, lead, lithium, mercury, potassium, silver, sodium, strontium, thallium, and tin, and 0-10% total chloride and/or fluoride. Glass compositions consisting essentially, expressed in terms of mole percent, of 5-30% Ga.sub.2 S.sub.3, 0-10% R.sub.2 S.sub.3, wherein R is at least one network forming cation selected from the group consisting of aluminum, antimony, arsenic, and indium, 55-94.5% GeS.sub.2, 0.5-25% MS.sub.x, wherein M is at least one modifying metal cation selected from the group consisting of barium, cadmium, calcium, lead, lithium, potassium, silver, sodium, strontium, tin, yttrium, and a rare earth metal of the lanthanide series, 0-10% total selenide, 0-25% total chloride and/or fluoride, and wherein the sulfur and/or selenium content can vary between 85-125% of the stoichiometric value when doped with Pr demonstrate exceptionally high values of .tau..
摘要翻译：本发明广泛地涉及在电磁辐射光谱的红外区域中表现出优异透射性的透明玻璃，基本上以摩尔百分数表示的40-80％Ga 2 S 3，0-35％RS x的玻璃，其中R是选自铝，锑，砷，锗和铟的至少一种网络形成阳离子，1-50％的Ln2S3，其中Ln是至少一种选自稀土金属阳离子和钇的阳离子， 1-45％的MS x，其中M是选自钡，镉，钙，铅，锂，汞，钾，银，钠，锶，铊和锡中的至少一种改性金属阳离子，以及0-10 总氯化物和/或氟化物。基本上以摩尔百分比表示的5-30％Ga 2 S 3，0-10％R 2 S 3的玻璃组合物，其中R是选自铝，锑，砷和铟的至少一种形成网络的阳离子，55 -94.5％GeS2,0.5-25％MSx，其中M是选自钡，镉，钙，铅，锂，钾，银，钠，锶，锡，钇中的至少一种改性金属阳离子和稀土金属镧系，0-10％总硒，0-25％总氯化物和/或氟化物，其中硫和/或硒含量可以在化学计量值的85-125％之间变化，当掺杂Pr 表现出非常高的tau值。

49. 发明授权

US5367012A Stabilizer for glass/polymer alloys 失效
标题翻译：玻璃/聚合物合金稳定剂
公开(公告)号：US5367012A
公开(公告)日：1994-11-22
申请号：US100835
申请日：1993-08-09
申请人： Bruce G. Aitken , Dana C. Bookbinder , James E. Dickinson, Jr. , Brent M. Wedding
发明人： Bruce G. Aitken , Dana C. Bookbinder , James E. Dickinson, Jr. , Brent M. Wedding
IPC分类号： C03C3/16 , C03C14/00 , C08K3/00 , C08K3/22 , C08K3/26 , C08K3/40 , C08L101/00 , C08K3/32 , C08L23/00 , C08L67/00 , C08L71/00
CPC分类号： C03C14/00 , C08K3/22 , C08K3/26 , C08K3/40 , C03C2214/12
摘要： This invention is directed to an alloy, and a method of producing an alloy, of increased resistance to moisture, comprising a melt mixture of at least one phosphate glass, at least one organic thermoplastic or thermosetting polymer, and an amount of a water soluble stabilizer component which provides a source of metal cations having a valency of 2.sup.+ or higher The amount of the stabilizer component added is that amount effective to improve the alloy's resistance to moisture. Preferably, the alloy is comprised of: (a) 5-80% of the matrix material; (b) 15-90% of the phosphate glass; and, (c) 0.1 to 40% of the stabilizer component. Additionally, the metal cations which are found in the stabilizer component and which form part of the insoluble surface layer are preferably selected from the group consisting of Ba.sup.2+, Mg.sup.2+, Ca.sup.2+, Al.sup.3+, Zn.sup.2+, Sr.sup.+2 and Fe.sup.3+.
摘要翻译：本发明涉及一种具有增加的抗水分性的合金和合金的制造方法，包括至少一种磷酸盐玻璃，至少一种有机热塑性或热固性聚合物的熔融混合物和一定量的水溶性稳定剂提供具有2+或更高价态的金属阳离子源的组分。添加的稳定剂组分的量是有效改善合金耐湿性的量。优选地，该合金由以下组成：（a）5-80％的基质材料; （b）15-90％的磷酸盐玻璃; 和（c）0.1〜40％的稳定剂成分。此外，在稳定剂组分中发现并形成不溶性表面层的一部分的金属阳离子优选选自Ba2 +，Mg2 +，Ca2 +，Al3 +，Zn2 +，Sr +2和Fe3 +。

50. 发明授权

US5346865A Rare earth-doped, stabilized cadmium halide glasses 失效
标题翻译：稀土掺杂，稳定的镉卤化物玻璃
公开(公告)号：US5346865A
公开(公告)日：1994-09-13
申请号：US86048
申请日：1993-07-06
申请人： Bruce G. Aitken , Frank A. Annunziata , Roger F. Bartholomew , Mark A. Newhouse , Mark L. Powley , Andrea L. Sadd
发明人： Bruce G. Aitken , Frank A. Annunziata , Roger F. Bartholomew , Mark A. Newhouse , Mark L. Powley , Andrea L. Sadd
IPC分类号： C03C3/32 , C03C4/00 , C03C4/10 , H01S3/16 , H01S3/17
CPC分类号： C03C4/10 , C03C3/32 , C03C3/325 , C03C4/0071 , H01S3/17 , H01S3/1603 , Y10S501/904
摘要： This invention is directed to the production of transparent glasses exhibiting transmission far into the infrared regime of the radiation spectrum. The glasses consist essentially, in mole percent, of 42-55% CdF.sub.2 and/or CdCl.sub.2, 30-40% NaF and/or NaCl, 2-20% total of BaF.sub.2 and/or BaCl.sub.2 +KF and/or KCl, consisting of 0-15% BaF.sub.2 and/or BaCl.sub.2 and 0-7% KF and/or KCl, 1-12% total of at least one stabilizing metal halide selected from the group LiX, BeX.sub.2, MgX.sub.2, MnX.sub.2, PbX.sub.2, TlX, COX.sub.2, and ZnX.sub.2, and 0,005-0.5% REX.sub.3, wherein Re is at least one rare earth metal selected from the lanthanide series of rare earth metals and X is at least one halide selected from the group consisting of fluoride, chloride, and bromide. The preferred glasses contain at least 2% each of BaF.sub.2 and/or BaCl.sub.2 and KF and/or KCl.
摘要翻译：本发明涉及透明玻璃的生产，该透明玻璃显示出远离辐射光谱的红外区域的传播。玻璃基本上以摩尔百分数计含42-55％的CdF2和/或CdCl2，30-40％的NaF和/或NaCl，2-20％的BaF 2和/或BaCl 2 + KF和/或KCl，由 0-15％BaF 2和/或BaCl 2和0-7％KF和/或KCl，1-12％的至少一种选自LiX，BeX2，MgX2，MnX2，PbX2，TlX，COX2，和ZnX2和0.005-0.5％的REX3，其中Re是选自镧系稀土金属中的至少一种稀土金属，X是选自氟化物，氯化物和溴化物中的至少一种卤化物。优选的玻璃含有至少2％的BaF 2和/或BaCl 2和KF和/或KCl。

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