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41. 发明申请

US20100191018A1 PROCESS FOR PREPARING PURE CYCLODODECANONE 有权
标题翻译：制备纯环己酮的方法
公开(公告)号：US20100191018A1
公开(公告)日：2010-07-29
申请号：US12694815
申请日：2010-01-27
申请人： Joaquim Henrique Teles , Beatrice Rößler-Feigel , Alexander Hauk , Anton Meier , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus , Rolf Pinkos , Gerd-Dieter Tebben
发明人： Joaquim Henrique Teles , Beatrice Rößler-Feigel , Alexander Hauk , Anton Meier , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus , Rolf Pinkos , Gerd-Dieter Tebben
IPC分类号： C07C45/27
CPC分类号： C07C45/82 , C07C45/28 , C07C45/62 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising one cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) in order to obtain a composition (A2), and (b) distillative treatment of the composition (A2) from step (a2) in order to obtain a composition (B), comprising the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group and less than 1.0% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, where Z can be 1, 2, 3 or 4.
摘要翻译：本发明涉及一种制备具有Z环和至少具有7至16个碳原子的酮基的至少一种环状化合物的方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少包含一个环状烯烃，Z循环和7至16个碳原子和至少两个C-C双键，借助于一氧化二氮，得到组合物（A1），（a2）以Z循环分离至少一种环状烯烃， 16个碳原子与来自组合物（A1）的至少两个C-C双键，以获得组合物（A2），和（b）从步骤（a2）中的组合物（A2）的蒸馏处理，以获得组合物（B），其包含至少一种Z循环的环状化合物和具有酮基的7至16个碳原子和小于1.0重量％的至少一种具有Z-1循环和7至16个碳原子的化合物，至少一个醛基，其中Z可以是1,2,3或4个。

42. 发明授权

US07754925B2 Method for the hydrogenation of mass fluxes containing aldehyde 失效
标题翻译：含醛的质量流量的氢化方法
公开(公告)号：US07754925B2
公开(公告)日：2010-07-13
申请号：US11995518
申请日：2006-07-11
申请人： Rolf Pinkos , Gerd-Dieter Tebben , Alexander Hauk , Christian Mueller , Harald Rust
发明人： Rolf Pinkos , Gerd-Dieter Tebben , Alexander Hauk , Christian Mueller , Harald Rust
IPC分类号： C07C45/00
CPC分类号： C07C45/62 , C07C45/85 , C07C49/413 , C07C47/228
摘要： The present application relates to a process for reacting a composition I comprising at least one aldehyde with hydrogen in the presence of a catalyst in at least one main reactor and at least one postreactor, wherein at least 50% of the fresh hydrogen fed to the reaction system is fed into at least one postreactor. In a preferred embodiment, composition I comprises at least one further organic compound.
摘要翻译：本申请涉及在至少一个主反应器和至少一个后反应器中在催化剂存在下使包含至少一种醛的组合物I与氢反应的方法，其中将至少50％的进料到反应中的新鲜氢气系统进料至少一个后反应器。在优选的实施方案中，组合物I包含至少一种其它有机化合物。

43. 发明授权

US07649119B2 Method for the production of cyclic ketones 失效
标题翻译：环酮生产方法
公开(公告)号：US07649119B2
公开(公告)日：2010-01-19
申请号：US12306841
申请日：2007-06-27
申请人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Gerd Tebben , Christian Müller
发明人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Gerd Tebben , Christian Müller
IPC分类号： C07C45/27
CPC分类号： C07C45/28 , C07C45/62 , C07C45/85 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps (a) oxidation of a composition (I) comprising at least one cyclic olefin which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A), (b) treatment of the composition (A) with at least one base to give a composition (B).
摘要翻译：本发明涉及一种制备具有7至16个碳原子的环酮的方法，其至少包括步骤（a）包含至少一种具有7至16个碳原子的环烯烃的组合物（I）的氧化和至少一个CC双键，得到组合物（A），（b）用至少一个碱处理组合物（A）以得到组合物（B）。

44. 发明申请

US20090326277A1 METHOD FOR PURIFYING CYCLIC KETONES 有权
标题翻译：纯化循环克隆的方法
公开(公告)号：US20090326277A1
公开(公告)日：2009-12-31
申请号：US12306807
申请日：2007-06-27
申请人： Rolf Pinkos , Gerd Tebben , Alexander Hauk , Christian Müller , Harald Rust
发明人： Rolf Pinkos , Gerd Tebben , Alexander Hauk , Christian Müller , Harald Rust
IPC分类号： C07C45/00
CPC分类号： C07C45/85 , C07C45/33 , C07C45/34 , C07C45/58 , C07C45/62 , C07C45/80 , C07C45/81 , C07C45/82 , C07C49/413 , C07C49/607
摘要： The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with at least one acid and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization, Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one acid for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with the acid.
摘要翻译：本发明涉及一种纯化包含至少一种具有7至16个碳原子的环酮的组合物（I）的方法，其包括用至少一种酸对组合物（I）进行热处理，并进一步通过选自蒸馏，萃取和结晶的方法。此外，本发明涉及一种制备环十二烷酮的方法，其包括这种纯化，以及使用至少一种酸来纯化至少包含（I）的组合物一种具有7-16个碳原子的环酮，通过组合物（I）与酸的热处理。

45. 发明申请

US20090326276A1 METHOD FOR THE PRODUCTION OF CYCLIC KETONES 失效
标题翻译：生产环状酮的方法
公开(公告)号：US20090326276A1
公开(公告)日：2009-12-31
申请号：US12306827
申请日：2007-06-27
申请人： Joaquim Henrique Teles , Beatrice Rößler , Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
发明人： Joaquim Henrique Teles , Beatrice Rößler , Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
IPC分类号： C07C45/27
CPC分类号： C07C45/28 , C07C45/62 , C07C45/80 , C07C45/81 , C07C45/82 , C07C45/85 , C07C2601/18 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps(a) oxidation of a composition (I) comprising at least one cyclic alkene which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A),(b) treatment of the composition (A) with at least one base to give a composition (B),(c) hydrogenation of the composition (B) in the presence of at least one catalyst to give a composition (C),(d) purification of the composition (C), comprising at least the steps(di) thermal treatment of the composition (C) with at least one acid or at least one catalyst comprising at least one transition metal,(dii) further purification by a method selected from the group consisting of distillation, extraction and crystallization.
摘要翻译：本发明涉及一种制备具有7至16个碳原子的环酮的方法，其至少包括步骤（a）氧化包含至少一个具有7至16个碳原子的环烯烃的组合物（I）和至少一个CC双键，得到组合物（A），（b）用至少一种碱处理组合物（A），得到组合物（B），（c）组合物的氢化（B）在至少一种催化剂的存在下，得到组合物（C），（d）组合物（C）的纯化，至少包括步骤（ii）组合物（C）的热处理至少一种酸或至少一种包含至少一种过渡金属的催化剂，（dii）通过选自蒸馏，萃取和结晶的方法进一步纯化。

46. 发明申请

US20090318733A1 METHOD FOR PURIFYING CYCLIC KETONES 有权
标题翻译：纯化循环克隆的方法
公开(公告)号：US20090318733A1
公开(公告)日：2009-12-24
申请号：US12306815
申请日：2007-06-27
申请人： Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
发明人： Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
IPC分类号： C07C45/78
CPC分类号： C07C45/85 , C07C45/34 , C07C45/62 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with a catalyst comprising at least one transition metal and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization. Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one catalyst comprising at least one transition metal for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with a catalyst comprising at least one transition metal.
摘要翻译：本发明涉及一种纯化包含至少一种具有7至16个碳原子的环酮的组合物（I）的方法，其包括用包含至少一种过渡金属的催化剂热处理组合物（I）并进一步纯化通过选自蒸馏，萃取和结晶的方法。此外，本发明涉及一种制备环十二烷酮的方法，其包括这种纯化，以及至少一种包含至少一种过渡金属的催化剂用于纯化组合物（I）的用途，所述组合物（I）包含至少一种具有7〜 16个碳原子通过用包含至少一种过渡金属的催化剂热处理组合物（I）。

47. 发明申请

US20090227815A1 PROCESS FOR THE PREPARATION OF CYCLODODECANONE 有权
标题翻译：制备环十二烷酮的方法
公开(公告)号：US20090227815A1
公开(公告)日：2009-09-10
申请号：US12470994
申请日：2009-05-22
申请人： Joaquim Henrique Teles , Beatrice Rossler , Rolf Pinkos , Thomas Genger , Thomas Preiss
发明人： Joaquim Henrique Teles , Beatrice Rossler , Rolf Pinkos , Thomas Genger , Thomas Preiss
IPC分类号： C07C45/28
CPC分类号： C07C45/28 , C07C2601/20 , C07C49/413
摘要： A process for preparing cyclododecanone by reacting cyclododecene with dinitrogen monoxide, comprising in particular steps (I) and (II): (I) preparing cyclododecene by partially hydrogenating cyclododecatriene; (II) reacting cyclododecene obtained in (I) with dinitrogen monoxide to obtain cyclododecanone.
摘要翻译：通过环十二碳烯与一氧化二氮反应制备环十二烷酮的方法，特别包括步骤（I）和（II）：（I）通过部分氢化环十二碳三烯制备环十二烯; （II）使得（I）中得到的环十二碳烯与一氧化二氮反应，得到环十二酮。

48. 发明申请

US20090134066A1 Method for producing alkyl-aromatic compounds by direct alkylation of aromatic hydrocarbons with alkanes 审中-公开
标题翻译：通过芳族烃与烷烃直接烷基化生产烷基芳族化合物的方法
公开(公告)号：US20090134066A1
公开(公告)日：2009-05-28
申请号：US11659422
申请日：2005-08-04
申请人： Nils Bottke , Michael Triller , Ulrich Muller , Rolf Pinkos , Thomas Heidemann
发明人： Nils Bottke , Michael Triller , Ulrich Muller , Rolf Pinkos , Thomas Heidemann
IPC分类号： C10G35/06 , C07C2/58
CPC分类号： C07C303/06 , C07C2/76 , C07C15/02 , C07C309/31
摘要： The present invention relates to a process for preparing alkylaromatics by reacting aromatic compounds with C1-C14-alkanes in the presence of a heterogeneous catalyst, which comprises using as the catalyst a crystalline, micro- and/or mesoporous solid comprising silicon and at least one father element selected from the group consisting of the transition metals and the main group elements gallium and tin, and activating said catalysts by a reducing pretreatment. Furthermore, the present invention relates to a process for preparing alkylarylsulfonates by sulfonating and neutralizing the alkyl aromatic compounds.
摘要翻译：本发明涉及在非均相催化剂存在下使芳族化合物与C 1 -C 14烷烃反应制备烷基芳族化合物的方法，该方法包括使用包含硅和至少一种以上的硅的结晶，微孔和/或介孔固体作为催化剂父元素选自过渡金属和主要元素镓和锡，并通过还原预处理活化所述催化剂。此外，本发明涉及通过磺化和中和烷基芳族化合物来制备烷基芳基磺酸盐的方法。

49. 发明授权

US07524996B2 Method for the separation of polymeric by-products from 1,4-butynediol 有权
标题翻译：从1,4-丁炔二醇分离聚合副产物的方法
公开(公告)号：US07524996B2
公开(公告)日：2009-04-28
申请号：US12065815
申请日：2006-08-23
申请人： Rudolf Erich Lorenz , Rolf Pinkos , Michael Steiniger , Gerd Schaefer
发明人： Rudolf Erich Lorenz , Rolf Pinkos , Michael Steiniger , Gerd Schaefer
IPC分类号： C07C29/76 , C07C29/74 , C07C29/86
CPC分类号： C07C29/172 , C07C29/17 , C07C29/76 , C07C33/035 , C07C31/207 , C07C33/046
摘要： The present invention relates to a process for purifying 1,4-butynediol, which comprises processing 1,4-butynediol in a dynamic mixing apparatus in an inert gas atmosphere at from 25 to 150° C. at a shear rate in the radial gap between rotor and stator of the mixing apparatus of more than 100 000 sec−1, awaiting phase separation at temperatures of from 25 to 150° C. and separating off the bottom phase, and a process for the hydrogenation of 1,4-butynediol to 1,4-butenediol and 1,4-butanediol using the purified 1,4-butynediol.
摘要翻译：本发明涉及纯化1,4-丁炔二醇的方法，该方法包括在惰性气体气氛中在25至150℃下以动态混合装置处理1,4-丁炔二醇，其剪切速率为混合装置的转子和定子超过100 000秒-1，等待25至150℃的相分离和分离底相，以及将1,4-丁炔二醇氢化成1 ，4-丁烯二醇和1,4-丁二醇，使用纯化的1,4-丁炔二醇。

50. 发明授权

US07459571B2 Catalyst extrudates based on copper oxide and their use for hydrogenating carbonyl compounds 有权
标题翻译：基于氧化铜的催化剂挤出物及其用于氢化羰基化合物的用途
公开(公告)号：US07459571B2
公开(公告)日：2008-12-02
申请号：US11934266
申请日：2007-11-02
申请人： Stephan Schlitter , Olga Schubert , Michael Hesse , Sabine Borchers , Markus Roesch , Rolf Pinkos , Alexander Weck , Gunther Windecker
发明人： Stephan Schlitter , Olga Schubert , Michael Hesse , Sabine Borchers , Markus Roesch , Rolf Pinkos , Alexander Weck , Gunther Windecker
IPC分类号： C07D307/00 , C07D307/02
CPC分类号： B01J23/72 , B01J21/04 , B01J23/94 , B01J35/002 , B01J35/1019 , B01J35/1038 , B01J35/108 , B01J37/0009 , B01J37/18 , B01J38/10 , B01J38/12 , C07C29/149 , C07D315/00 , Y02P20/584
摘要： Catalyst in the form of an extrudate which comprises from 5 to 85% by weight of copper oxide and in which the same oxidic support material is present in the active composition and as binder, and the use of the catalyst for the hydrogenation of carbonyl compounds.
摘要翻译：挤出物形式的催化剂，其包含5至85重量％的氧化铜，其中相同的氧化性载体材料存在于活性组合物中并作为粘合剂，以及使用催化剂用于羰基化合物的氢化。

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