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31. 发明授权

US5092157A Vapor collector/desorber with metallic ribbon 失效
标题翻译：蒸气收集器/解吸器与金属色带
公开(公告)号：US5092157A
公开(公告)日：1992-03-03
申请号：US81918
申请日：1987-07-08
申请人： Eugene K. Achter , Alf L. Carroll , David P. Rounbehler , David H. Fine , Freeman W. Fraim
发明人： Eugene K. Achter , Alf L. Carroll , David P. Rounbehler , David H. Fine , Freeman W. Fraim
IPC分类号： G01N1/00 , G01N1/02 , G01N1/22 , G01N1/28 , G01N1/40 , G01N21/76 , G01N27/417 , G01N30/02 , G01N30/06 , G01N30/08 , G01N30/12 , G01N30/14 , G01N30/16 , G01N30/30 , G01N30/40 , G01N30/46 , G01N30/62 , G01N30/64 , G01N30/72 , G01N30/84 , G01N31/12 , G01N33/00 , G01N33/22 , G01V9/00
CPC分类号： G01N30/461 , G01N1/02 , G01N30/08 , G01N30/12 , G01N30/84 , G01N33/0057 , G01V9/007 , G01N1/2214 , G01N1/2226 , G01N1/28 , G01N1/40 , G01N2001/022 , G01N2001/028 , G01N2030/025 , G01N2030/065 , G01N2030/085 , G01N2030/121 , G01N2030/122 , G01N2030/123 , G01N2030/125 , G01N2030/126 , G01N2030/143 , G01N2030/167 , G01N2030/3007 , G01N2030/3046 , G01N2030/3053 , G01N2030/3061 , G01N2030/3069 , G01N2030/3076 , G01N2030/3084 , G01N2030/626 , G01N2030/642 , G01N2030/8405 , G01N21/76 , G01N30/14 , G01N30/40 , G01N30/62 , G01N30/72
摘要： A highly selective, sensitive, fast detection system and method are disclosed for detecting vapors of specific compounds in air. Vapors emanating from compounds such as explosives, or stripped from surfaces using heat and suction from a hand-held sample gun, are collected on surfaces coated with gas chromatograph (GC) material which trap explosives vapors but repel nitric oxide, then are desorbed and concentrated in one or more cold spot concentrators. A high speed gas chromatrograph (GC) separates the vapors, after which specific vapors are decomposed in two pyrolyzers arranged in parallel and the resulting nitric oxide is detected. A low temperature pyrolyzer with silver produces NO from nitramines or nitrite esters; a high temperature pyrolyzer decomposes all explosives vapors to permit detection of the remaining explosives. Also disclosed is a series arrangement of pyrolyzers and gas chromatographs and an NO detector to time-shift detection of certain vapors and facilitate very fast GC analyses. The use of hydrogen as a carrier gas, plus unique collectors and concentrators, high speed heaters, NO detectors, and very fast, temperature-programmable GC's enhance selectivity, sensitivity and speed of detection.
摘要翻译：公开了一种高选择性，灵敏，快速的检测系统和方法，用于检测空气中特定化合物的蒸气。从化合物如爆炸物或从手持式样品枪吸取热量从表面剥离的蒸气被收集在涂有气相色谱（GC）材料的表面上，该气相色谱（GC）材料捕获爆炸物蒸气但排斥一氧化氮，然后被解吸和浓缩在一个或多个冷点浓缩器中。高速气相色谱仪（GC）分离蒸汽，之后特定的蒸气在平行排列的两个热解器中分解，并检测到所产生的一氧化氮。含有银的低温热解器由硝胺或亚硝酸酯产生NO; 高温热解器分解所有炸药蒸气，以便检测剩余的炸药。还公开了热解器和气相色谱仪的串联布置和用于某些蒸气的时移检测的NO检测器，并且促进非常快速的GC分析。使用氢气作为载气，加上独特的收集器和浓缩器，高速加热器，NO检测器和非常快速的温度可编程GC增强了选择性，灵敏度和检测速度。

32. 发明授权

US5083450A Gas chromatograph-mass spectrometer (GC/MS) system for quantitative analysis of reactive chemical compounds 失效
标题翻译：用于反应性化学化合物定量分析的气相色谱 - 质谱仪（GC / MS）系统
公开(公告)号：US5083450A
公开(公告)日：1992-01-28
申请号：US525798
申请日：1990-05-18
申请人： Quirinus G. Grindstaff
发明人： Quirinus G. Grindstaff
IPC分类号： G01N27/62 , G01N30/30 , G01N30/72
CPC分类号： G01N30/30 , G01N30/7206 , G01N2030/3007 , G01N2030/3038 , G01N2030/3046
摘要： Described is a new gas chromatograph-mass spectrometer (GC/MS) system and method for quantitative analysis of reactive chemical compounds. All components of such a GC/MS system external to the oven of the gas chromatograph are programmably temperature controlled to operate at a volatilization temperature specific to the compound(s) sought to be separated and measured.
摘要翻译：描述了一种新的气相色谱 - 质谱仪（GC / MS）系统和反应性化合物定量分析方法。在气相色谱仪的烘箱外部的这种GC / MS系统的所有组分都可编程地温度控制，以在试图分离和测量的化合物特异性的挥发温度下操作。

33. 发明授权

US4662914A Flow-limited direct GC/MS interface 失效
标题翻译：流量限制直接GC / MS接口
公开(公告)号：US4662914A
公开(公告)日：1987-05-05
申请号：US712840
申请日：1985-03-18
申请人： Stuart C. Hansen , Jean-Luc Truche
发明人： Stuart C. Hansen , Jean-Luc Truche
IPC分类号： G01N30/30 , G01N30/72 , H01J49/04 , B01D15/08
CPC分类号： H01J49/0422 , G01N30/7206 , G01N2030/3007 , G01N2030/3038 , G01N30/7293
摘要： A capillary-direct interface, suitable for connecting a gas chromatograph to a mass spectrometer, having a flow restrictor that is to be mounted at the entrance to the ionization chamber of the mass spectrometer to prevent damage to the mass spectrometer if the column of the gas chromatograph is removed from the mass spectrometer or breaks inside the interface. A preferred flow restrictor includes a hollow tube, the middle of which is connected to an exhaust port to enable a vacuum pump to remove gas from the middle of the tube. The hollow tube is enclosed by a high thermal conductivity tube that is thermally connected to a heat source to control the temperature of the hollow tube. A capillary GC column can be inserted entirely through the hollow tube into the ionization chamber to produce a capillary direct mode of coupling. Also, an additional capillary tube, inside the hollow tube and extending from the ionization and detection chamber to the end of the GC column, can be used to implement the open-split and jet separator modes of coupling.
摘要翻译：一种适用于将气相色谱仪连接到质谱仪的毛细管直接界面，具有限流器，该流量限制器将安装在质谱仪离子化室的入口处，以防止质谱仪损坏质谱仪色谱仪从质谱仪中除去或在界面内断裂。优选的流量限制器包括中空管，其中间管连接到排气口，以使得真空泵能够从管的中部移除气体。中空管由与热源热连接的高导热管包围，以控制中空管的温度。毛细管GC柱可以通过中空管完全插入电离室，以产生毛细管直接耦合模式。此外，在中空管内部并从电离和检测室延伸到GC柱的末端的另外的毛细管可以用于实现开放式分离和喷射分离器的耦合模式。

34. 发明授权

US4251219A Apparatus for and method of determining contaminants on low pressure condensate 失效
标题翻译：用于确定低压冷凝物污染物的方法和方法
公开(公告)号：US4251219A
公开(公告)日：1981-02-17
申请号：US955914
申请日：1978-10-30
申请人： Thurston E. Larson , Russell W. Lane , Chester H. Neff
发明人： Thurston E. Larson , Russell W. Lane , Chester H. Neff
IPC分类号： B01D3/32 , G01N27/06 , G01N30/30 , G01N30/96 , G01N33/18 , G01N27/46 , G05D9/00
CPC分类号： G01N27/06 , B01D3/322 , G01N30/96 , G01N2030/3007 , G01N33/18 , Y10T436/16 , Y10T436/173076 , Y10T436/18 , Y10T436/193333
摘要： Measurement is made of low levels of chloride, sulfate, phosphate, nitrate and other inorganic anions in a relatively low pressure condensate having a temperature preferably below 40.degree. C. The condensate is passed through a hydrogen exchange resin bed and the effluent from the resin bed is heated to atmospheric boiling temperature to eliminate gases such as carbon dioxide and ammonia. Heat to maintain a constant atmospheric boiling temperature is supplied by an electric heating element. A temperature sensor on the influent test water adjusts the voltage or current supplied to the electric heating element to maintain the constant atmospheric boiling temperature. A fail-safe device prevents electric heater failure on water flow stoppage. The conductivity of the heated water at or very close to atmospheric boiling point temperature is measured and is an indication of the contamination present in the relatively low pressure, low temperature test condensate.
摘要翻译：在温度优选低于40℃的相对低压缩合物中测量氯化物，硫酸盐，磷酸盐，硝酸盐和其他无机阴离子的水平。冷凝物通过氢交换树脂床，来自树脂床的流出物加热至常压沸腾温度以除去二氧化碳和氨等气体。保持恒定的沸腾温度的热量由电加热元件供应。进水试验水中的温度传感器调节供给电加热元件的电压或电流，以保持恒定的大气沸腾温度。故障安全装置可防止电热水器停水。测量或非常接近常压沸点温度的加热水的电导率是指相对低压，低温试验冷凝物中存在的污染的指示。

35. 发明授权

US4044593A Chromatograph 失效
标题翻译：色谱仪
公开(公告)号：US4044593A
公开(公告)日：1977-08-30
申请号：US442055
申请日：1974-02-13
申请人： Tatsuro Haruki , Yoshiro Hayashi
发明人： Tatsuro Haruki , Yoshiro Hayashi
IPC分类号： G01N30/30 , G01N30/88 , G01N31/08
CPC分类号： G01N30/30 , G01N2030/3007 , G01N2030/3084 , G01N2030/8881
摘要： A chromatograph having removable modular analysis units fitting into a chamber within the chromatograph housing, each unit including a column, sample introduction portion and detector. Each modular unit includes a block of thermally conductive material which encloses substantial portions of the sample introduction means and detector and is provided with an exposed surface adapted to contact heating means contained in the chromatograph housing.
摘要翻译：具有可拆卸模块分析单元的色谱仪，其装配到色谱室外壳内的室中，每个单元包括色谱柱，样品引入部分和检测器。每个模块单元包括一块导热材料块，其包围样品引入装置和检测器的实质部分，并且设置有暴露表面，该暴露表面适于接触包含在色谱仪外壳中的加热装置。

36. 发明公开

US20230273169A1 INSPECTION APPARATUS 审中-公开
公开(公告)号：US20230273169A1
公开(公告)日：2023-08-31
申请号：US18016202
申请日：2021-07-15
申请人： SHIMADZU CORPORATION
发明人： Akio IMAI , Koichi SHIMOTORI , Akioki NAKAMORI , Kiyuki NOTO
IPC分类号： G01N33/18 , G01N30/30 , G01N30/32 , G01N30/74
CPC分类号： G01N33/1846 , G01N30/30 , G01N30/32 , G01N30/74 , G01N2030/025 , G01N2030/3007 , G01N2030/3084
摘要： An object is to increase an efficiency of removing carbon dioxide derived from inorganic carbon. An inspection apparatus includes: a column that separates a group of substances contained in an aqueous sample by size; an addition unit that adds a reagent, which acidifies the aqueous sample, into a channel; a degassing unit provided downstream of the addition unit for degassing carbon dioxide; a measurement unit that measures organic carbon contained in each substance from which the carbon dioxide has been removed; and a temperature maintaining unit that maintains a temperature of each of the column and a container in which a gas-permeable tube of the degassing unit is housed.

37. 发明申请

US20170038345A1 PASSIVE COLUMN PRE-HEATER FOR USE IN CHROMATOGRAPHIC SYSTEMS 审中-公开
标题翻译：被动色谱柱预热器用于色谱系统
公开(公告)号：US20170038345A1
公开(公告)日：2017-02-09
申请号：US15303321
申请日：2015-04-10
申请人： Waters Technologies Corporation
发明人： Joshua A. Shreve , Kurt D. Joudrey
IPC分类号： G01N30/30 , G01N1/44
CPC分类号： G01N30/30 , G01N1/44 , G01N2030/3007
摘要： A passive pre-heater assembly includes a thermally conductive heat-spreading block and a plurality of passive pre-heaters in thermally conductive communication with the heat-spreading block. The plurality of the pre-heaters exchanges heat with the thermally conductive heat-spreading block. Each pre-heater includes a thermally conductive base in thermal communication with the heat-spreading block, and a plurality of thermally conductive fins is in thermal communication with the thermally conductive base. The plurality of fins of each pre-heater exchanges heat convectively with ambient air and conductively with the thermally conductive base of that pre-heater. A given one of the passive pre-heaters further comprises a tube in thermally conductive contact with the thermally conductive base of the given passive pre-heater. The thermally conductive heat-spreading block exchanges heat with a fluid passing through the tube of the given passive pre-heater.
摘要翻译：无源预热器组件包括导热散热块和与热扩散块导热连通的多个无源预热器。多个预热器与导热散热块交换热量。每个预热器包括与热扩散块热连通的导热基座，并且多个导热翅片与导热基底热连通。每个预热器的多个散热片与环境空气对流交换热量，并与该预热器的导热底座导电地交换。被动预热器中的给定的一个还包括与给定的无源预热器的导热底座导热接触的管。导热散热块与通过给定无源预热器的管的流体进行热交换。

38. 发明授权

US09228983B2 Process analytic device with improved thermal stability 有权
标题翻译：具有改善的热稳定性的工艺分析装置
公开(公告)号：US09228983B2
公开(公告)日：2016-01-05
申请号：US13826720
申请日：2013-03-14
申请人： Rosemount Analytical Inc.
发明人： Edward J. Bailey , Leighton M. Fields
IPC分类号： G01N30/30 , G01N30/66 , G01N30/02 , G01N30/72 , G01N30/88
CPC分类号： G01N30/30 , G01N30/66 , G01N30/7206 , G01N2030/025 , G01N2030/3007 , G01N2030/3046 , G01N2030/8886
摘要： A process analytic device has an input to receive a sample of interest. An analytic detector is operably coupled to receive the sample of interest and to provide an analytic output relative to the sample of interest. A heat pipe is thermally coupled to the analytic detector. In one embodiment, the process analytic device is a process gas chromatograph.
摘要翻译：过程分析设备具有接收感兴趣的样本的输入。分析检测器可操作地耦合以接收感兴趣的样品并提供相对于感兴趣样品的分析输出。热管与分析检测器热耦合。在一个实施方案中，过程分析装置是工艺气体色谱仪。

39. 发明申请

US20150260694A1 GAS CHROMATOGRAPHY DEVICE 有权
标题翻译：气相色谱仪
公开(公告)号：US20150260694A1
公开(公告)日：2015-09-17
申请号：US14427053
申请日：2012-09-11
申请人： Satoshi Matsuoka , Takahiro Nishimoto , Masaki Kanai , Masanori Nishino
发明人： Satoshi Matsuoka , Takahiro Nishimoto , Masaki Kanai , Masanori Nishino
IPC分类号： G01N30/30 , G01N30/16
CPC分类号： G01N30/30 , G01N30/16 , G01N30/54 , G01N2030/3007 , G01N2030/3046 , G01N2030/3084
摘要： A gas chromatography device includes a sample injection part, a detector, a separation column, and a transfer line connecting between the sample injection part and the separation column and between the sample injection part and the detector. Furthermore, a column temperature adjustment part for adjusting the temperature of the separation column, and a line temperature adjustment part for adjusting the temperature of the transfer line are provided. The line temperature adjustment part is structured to include a heat block which includes a heating element and which is in contact with the transfer line from one side, and a holding member which presses the transfer line toward the heat block side by being in contact from the other side, and to sandwich the transfer line by the heat block and the holding member.
摘要翻译：气相色谱装置包括样品注入部分，检测器，分离柱和连接在样品注射部分和分离柱之间以及样品注射部分和检测器之间的传输线。此外，提供了用于调节分离塔的温度的色谱柱温度调节部分和用于调节传输线的温度的管线温度调节部件。线路温度调节部构成为包括：加热元件，其与一侧的输送线接触的热块，以及通过与传热线接触从而将传送线朝向加热块侧按压的保持部件并且通过加热块和保持构件夹住输送线。

40. 发明申请

US20150157959A1 TECHNIQUES FOR ACCELERATING THERMAL EQUILIBRIUM IN A CHROMATOGRAPHIC COLUMN 审中-公开
标题翻译：在色谱柱中加热热平衡的技术
公开(公告)号：US20150157959A1
公开(公告)日：2015-06-11
申请号：US14406285
申请日：2013-06-26
申请人： Waters Technologies Corporation
发明人： Edouard S.P. Bouvier , Joseph Kareh
IPC分类号： B01D15/16 , G01N30/30 , B01D15/22
CPC分类号： B01D15/161 , B01D15/20 , B01D15/22 , G01N30/30 , G01N30/54 , G01N2030/027 , G01N2030/3007 , G01N2030/3015 , G01N2030/3038 , G01N2030/3046 , G01N2030/3053 , G01N2030/3061 , G01N2030/3069 , G01N2030/3076
摘要： Techniques are described for accelerating thermal equilibrium in a chromatographic column. An apparatus comprises a chromatography column, and a plurality of temperature control units in thermal contact with the chromatography column. A method of performing liquid chromatography comprises setting an inlet of a chromatography column to a first temperature using a first temperature control unit in thermal contact with said inlet, setting an outlet of the chromatography column to a second temperature using a second temperature control unit in thermal contact with the outlet, wherein the first temperature is less than the second temperature; and injecting a sample into a liquid stream that flows through the chromatography column after the inlet is set at the first temperature and the outlet is at the second temperature.
摘要翻译：描述了加速色谱柱热平衡的技术。一种装置包括色谱柱和与色谱柱热接触的多个温度控制单元。进行液相色谱的方法包括使用与所述入口热接触的第一温度控制单元将色谱柱的入口设定为第一温度，使用第二温度控制单元将色谱柱的出口设定为第二温度与所述出口接触，其中所述第一温度小于所述第二温度; 并且在入口被设定在第一温度并且出口处于第二温度之后，将样品注入流过色谱柱的液体流中。

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