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    • 31. 发明授权
    • Analysis of drilling fluids
    • 钻井液分析
    • US5306909A
    • 1994-04-26
    • US860879
    • 1992-03-31
    • Timothy JonesTrevor HughesPatrick Tomkins
    • Timothy JonesTrevor HughesPatrick Tomkins
    • E21B49/00G01N21/35G01V9/04
    • E21B49/005G01N21/3577
    • A method of quantitative analysis of drilling fluids comprising subjecting an untreated wet sample of the fluid to a reflectance infrared spectroscopy technique, typically attenuated total reflectance spectroscopy, and comparing the spectrum obtained with spectra obtained from calibration samples of fluids of known composition. The sample can be obtained directly from the flowing mud with no preparation or alternatively the sample might comprise a prepared sample which is re-suspended in a liquid phase carrier. The sample can also be analysed for non-spectral properties which might also provide useful information in conjunction with spectral data. The method requires little or no sample preparation and can be used to quantitatively analyse both water-based and oil-based drilling fluids using a continuous in-line and/or on-line arrangement.
    • 一种钻井液的定量分析方法,包括使未经处理的湿样品进行反射红外光谱技术,通常为衰减的全反射光谱,并将获得的光谱与从已知组合物的流体的校准样品获得的光谱进行比较。 样品可以直接从流动的泥浆中获得,无需制备,或者样品可能包含重新悬浮在液相载体中的制备样品。 还可以分析样品的非光谱性质,这也可能与光谱数据一起提供有用的信息。 该方法需要很少或不需要样品制备,并且可以用于使用连续的在线和/或在线布置来定量分析水基和油基钻井液。
    • 32. 发明申请
    • SEPARATION OF OIL DROPLETS FROM WATER
    • 从水中分离油滴
    • US20140076815A1
    • 2014-03-20
    • US14117835
    • 2012-05-14
    • Khooi Yeei TanTrevor HughesWilhelm HuckMichaela Nagl
    • Khooi Yeei TanTrevor HughesWilhelm HuckMichaela Nagl
    • C02F1/28
    • C02F1/288B01D17/0202
    • A treatment process for an aqueous phase which contains oil droplets, possibly of 10-50 nm diameter, in aqueous flow from a hydrocyclone separator, comprises bringing the water into contact with a surface subdivided into areas of differing surface energy and affinity for oil and such that when the surface is submerged in an aqueous phase, oil droplets adhere to it with an apparent contact angle in a range from 90 to 150 degrees. Areas of the surface may reduce their affinity for oil in response to an external stimulus causing controlled release of droplets adhering to the surface. The process may be used to remove oil droplets from water produced by an oil or gas well, after downhole oil water separation or after production at a at a well head, or used to coalesce droplets in such water to a larger size to enable conventional separation.
    • 含水相的处理方法,其水分可能为10-50nm,水力旋流分离器的水流中包括使水与表面细分的表面接触,表面能和对油的亲和性等 当表面浸没在水相中时,油滴粘附到其上,其表观接触角在90至150度的范围内。 表面的区域可能会降低其对油的亲合力,以响应外部刺激,从而控制释放附着在表面上的液滴。 该方法可以用于从油井或气井产生的水中,在井下油水分离之后或在井口产生后除去油滴,或者用于将这种水中的液滴聚结成更大的尺寸以使常规分离 。
    • 33. 发明申请
    • FORECASTING ASPHALTIC PRECIPITATION
    • 预测ASPHALTIC降序
    • US20110172924A1
    • 2011-07-14
    • US12988869
    • 2009-04-23
    • Trevor HughesGary TustinAlexander WilsonCarlos AbadShiyi Wang
    • Trevor HughesGary TustinAlexander WilsonCarlos AbadShiyi Wang
    • G06F19/00
    • E21B43/164C09K8/594Y02P20/544
    • The magnitude of asphaltic precipitation when injecting a viscosity reducing diluent into a reservoir formation, notably to assist oil recovery therefrom, is forecast by (i) determining a relationship between asphaltic precipitation and a solubility parameter for the diluted oil, and then (ii) utilizing that relationship to forecast the magnitude of asphaltic precipitation when injecting a predetermined viscosity reducing diluent into the formation. Making this forecast may be followed by injecting a viscosity reducing diluent into the formation to assist oil recovery. The diluent may in particular be supercritical carbon dioxide or other asphaltene precipitant mixed with a more polar material in proportions designed by forecasting asphaltic precipitation by candidate materials in possible proportions.
    • 通过(i)确定沥青沉淀与稀释油的溶解度参数之间的关系,然后(ii)利用(i)确定沥青沉淀与稀释油的溶解度参数之间的关系,预测将注入减粘稀释剂注入储层形成中的沥青沉淀的大小, 该关系可以预测在将预定的减粘稀释剂注入到地层中时沥青沉淀的大小。 进行此预测之后,可以将降粘稀释剂注入地层以辅助石油回收。 稀释剂可以特别是超临界二氧化碳或其他沥青质沉淀剂与较极性的材料混合,其比例是以可能的比例预测候选材料的沥青沉淀所设计的比例。
    • 35. 发明申请
    • USE OF ENCAPSULATED TRACERS
    • 使用牵引器
    • US20100307745A1
    • 2010-12-09
    • US12477502
    • 2009-06-03
    • Valerie LafitteTrevor HughesSlaheddine KefiMathew MillerGary TustinShiyi Wang
    • Valerie LafitteTrevor HughesSlaheddine KefiMathew MillerGary TustinShiyi Wang
    • E21B47/00
    • C09K8/62E21B43/26E21B47/1015
    • A process of making observations of a subterranean reservoir penetrated by a wellbore uses distinguishable sets of tracer particles and comprises steps of: (i) delivering a plurality of sets of tracer particles to respective subterranean locations via the wellbore, the particles in each set comprising a tracer substance which distinguishes that set form the other sets; (ii) causing or allowing the tracer substances to flow out from the tracer particles whilst the particles are at the respective subterranean locations; (iii) causing or allowing production of fluid out of said reservoir via the wellbore; and (iv) detecting the presence or absence of the tracer substances in the produced fluid. The tracer substances are sufficiently distinguishable from each other to enable a tracer substance detected in the produced fluid to identify the set of tracer particles from which it has come and hence identify the location from which it has come. The process may be used in conjunction with hydraulic fracturing, placing sets of particles at different locations within a fracture and/or in different fractures extending from a single wellbore.
    • 对井眼穿透的地下储层进行观测的过程使用可区分的示踪剂颗粒组,并且包括以下步骤:(i)经由井孔将多组示踪剂颗粒递送到相应的地下位置,每组中的颗粒包括 跟踪物质,其区别于其他集合; (ii)当所述颗粒在相应的地下位置时,导致或允许示踪物质从示踪剂颗粒流出; (iii)导致或允许通过井筒从所述储存器中产生流体; 和(iv)检测产生的流体中示踪物质的存在或不存在。 示踪剂物质彼此充分区分,以使在所产生的流体中检测到的示踪物质能够识别来自其​​的示踪剂颗粒组,并因此识别出来的位置。 该方法可以与水力压裂结合使用,将一组颗粒放置在裂缝内的不同位置和/或从单个井眼延伸的不同裂缝中。
    • 40. 发明授权
    • Method for the determination of the ionic content of drilling mud
    • 用于确定钻井泥浆的离子含量的方法
    • US5140527A
    • 1992-08-18
    • US446895
    • 1989-12-06
    • Timothy JonesTrevor HughesPhilip Fletcher
    • Timothy JonesTrevor HughesPhilip Fletcher
    • E21B21/08E21B49/00G01N30/02
    • E21B49/005E21B21/08G01N30/02
    • In the rotary drilling of oil wells a drilling mud is used both to transport the cuttings up to the surface and to impose an hydrostatic pressure on the walls of the borehole. For these functions the mud must for example have an acceptable viscosity and density. It is therefore important to monitor the characteristics of the mud, and to keep them within certain limits. Only recently, however, has drilling practice recognized the importance of monitoring the mud's ionic composition. The various techniques proposed involve separation of the mud into liquid and solid portions, and analysis of these. Though they have proven useful, yet there are a number of problems. For example, the separation has not always been easy, and the available techniques often may not satisfactorily remove the fines. The invention suggests that these two problems, at least, can be overcome by the relatively simple expedient of first acidifying the mud sample, for acidification both causes the mud particles to flocculate, and so be more easily separated off, and causes the active fines to dissolve. In a preferred embodiment hydrobromic acid is employed, together with tetramethylammonium bromide (a displacement agent enabling the mud solid's Cationic Exchange Capacity to be measured), the separation is by filtration, and the analysis is by ion chromatography--and the results are fed into a computer model that then calculates the original mud components.