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31. 发明授权

US6080899A Method of producing fluorinated organic compounds 失效
标题翻译：氟化有机化合物的制备方法
公开(公告)号：US6080899A
公开(公告)日：2000-06-27
申请号：US236880
申请日：1999-01-25
申请人： David E. Bradley , Kevin Benson , David Nalewajek , Alagappan Thenappan
发明人： David E. Bradley , Kevin Benson , David Nalewajek , Alagappan Thenappan
IPC分类号： C07C17/20 , C07C17/08
CPC分类号： C07C17/206
摘要： A process for producing a fluorinated organic compound comprising: (a) reacting an organic starting material with hydrogen fluoride in the presence of a fluorination catalyst and an HFC reaction solvent to produce a product stream containing the fluorinated organic compound wherein the reaction solvent has a boiling point higher than that of the fluorinated organic compound; and (b) recovering the fluorinated organic compound from the product stream.
摘要翻译：一种氟化有机化合物的制造方法，其特征在于，包括：（a）在氟化催化剂和HFC反应溶剂的存在下，使有机原料与氟化氢反应，制造含有氟化有机化合物的产物流，其中，反应溶剂为沸点高于氟化有机化合物; 和（b）从产物流中回收氟化有机化合物。

32. 发明授权

US5352375A Azeotrope-like compositions of 1,1,1,2,2,3,3,-heptafluoropentane, C.sub.1 -C.sub.3 alkanol and optionally nitromethane 失效
标题翻译： 1,1,1,2,2,3,3， - 七氟戊烷，C 1 -C 3链烷醇和任选的硝基甲烷的类共沸组合物
公开(公告)号：US5352375A
公开(公告)日：1994-10-04
申请号：US108207
申请日：1993-08-17
申请人： E. L. Swan , David Nalewajek , L. Ellis
发明人： E. L. Swan , David Nalewajek , L. Ellis
IPC分类号： C11D7/50 , C23G5/028 , B08B3/00 , C11D7/30
CPC分类号： C11D7/5081 , C23G5/02803
摘要： Stable azeotrope-like compositions of 1,1,1,2,2,3,3-heptafluoropentane, C.sub.1 -C.sub.3 alkanol and optionally nitromethane have been discovered which are useful as degreasing agents and as solvents in a variety of industrial cleaning applications including cold cleaning and defluxing of printed circuit boards and dry cleaning.
摘要翻译：已经发现1,1,1,2,2,3,3-七氟戊烷，C 1 -C 3链烷醇和任选的硝基甲烷的稳定的类共沸组合物可用作各种工业清洁应用中的脱脂剂和溶剂，包括冷清洁和去除印刷电路板和干洗。

33. 发明授权

US5162587A Method for fluorinating by using N-fluoropyridinium pyridine heptafluorodiborate 失效
标题翻译：通过使用N-氟吡啶鎓吡啶氢溴酸盐来氟化的方法
公开(公告)号：US5162587A
公开(公告)日：1992-11-10
申请号：US778556
申请日：1991-10-18
申请人： Michael Van Der Puy , David Nalewajek , George A. Shia , William J. Wagner
发明人： Michael Van Der Puy , David Nalewajek , George A. Shia , William J. Wagner
IPC分类号： C07D213/89 , C07F5/02
CPC分类号： C07D213/89 , C07F5/022
摘要： The present invention provides a novel compound represented as ##STR1## The present novel compound is prepared by reacting fluorine with pyridine-boron trifluoride and is useful as a fluorinating agent in the fluorination of organic compounds.
摘要翻译：本发明提供了一种新化合物，其表示为本发明的新化合物，其通过氟与吡啶 - 三氟化硼反应制备，并且可用作有机化合物的氟化中的氟化剂。

34. 发明授权

US5086190A Method of fluorinating by using N-fluoropyridinium pyridine heptafluorodiborate 失效
标题翻译：使用N-氟吡啶鎓吡啶七氟二硼酸酯进行氟化的方法
公开(公告)号：US5086190A
公开(公告)日：1992-02-04
申请号：US647101
申请日：1991-01-29
申请人： Michael Van Der Puy , David Nalewajek , George A. Shia , William J. Wagner
发明人： Michael Van Der Puy , David Nalewajek , George A. Shia , William J. Wagner
IPC分类号： C07B39/00 , C07C45/51 , C07C45/54 , C07C45/56 , C07D213/89 , C07F5/02 , C07J1/00 , C07J41/00 , C07J51/00
CPC分类号： C07D213/89 , C07B39/00 , C07C45/511 , C07C45/54 , C07C45/56 , C07F5/022 , C07J1/0011 , C07J1/0025 , C07J41/0005 , C07J51/00
摘要： The present invention provides a novel compound represented as ##STR1## The present novel compound is prepared by reacting fluorine with pyridine-boron trifluoride and is useful as a fluorinating agent in the fluorination of organic compounds.
摘要翻译：本发明提供了一种新化合物，其表示为本发明的新化合物，其通过氟与吡啶 - 三氟化硼反应制备，并且可用作有机化合物的氟化中的氟化剂。

35. 发明授权

US4584184A Separation and recovery of molybdenum values from uranium process waste 失效
标题翻译：从铀工艺废物中分离和回收钼值
公开(公告)号：US4584184A
公开(公告)日：1986-04-22
申请号：US612282
申请日：1984-05-21
申请人： David Nalewajek , Lynn E. McCurry , David J. Friedland , Richard E. Eibeck
发明人： David Nalewajek , Lynn E. McCurry , David J. Friedland , Richard E. Eibeck
IPC分类号： C01G39/00 , C01G39/02 , C01G43/00 , C01G43/01 , C22B7/00 , C22B34/34 , C22B60/02
CPC分类号： C01G43/01 , C01G39/00 , C01G39/02 , C01G43/00 , C22B34/34 , C22B60/0247 , C22B7/008 , C01P2006/80 , Y02P10/234
摘要： A method for treating process waste consisting of uranium hexafluoride, UF.sub.6, molybdenum hexafluoride, MoF.sub.6 and molybdenum oxytetrafluoride, MoOF.sub.4 is provided wherein the foregoing mixture is hydrolyzed in an aqueous solution of ammonium carbonate and ammonium hydroxide. The resulting mother liquor is digested at 60.degree.-80.degree. C. to drive off carbon dioxide and convert the ammonium uranyl carbonate, (NH.sub.4).sub.4 UO.sub.2 (CO.sub.3).sub.3 to ammonium diuranate, (NH.sub.4).sub.2 U.sub.2 O.sub.7. The pH is maintained above 9 to prevent premature precipitation of the molybdenum values as molybdic acid or uranyl molybdate.The ammonium diuranate which forms as a yellow solid is filtered, slurried in aqueous ammonium hydroxide, filtered and dried. The yield is quantitative. Pyrolysis results in conversion of the diuranate salt to uranium oxide, U.sub.3 O.sub.8, of suitable purity to be recycled in the uranium hexafluoride production process. The combined filtrates which contain the molybdenum values and ammonium fluoride by-product are diluted, and stirred, with 95% ethanol to precipitate white, crystalline, ammonium molybdate, (NH.sub.4).sub.2 MoO.sub.4. The ammonium fluoride remains soluble. The ammonium molybdate is filtered, dried and calcined at 600.degree. C. for 2 hours to yield molybdenum trioxide, MoO.sub.3 in >90% yield and essentially free of uranium contamination. Fluoride contamination in either of the reprocessed materials is minimal.
摘要翻译：一种用于处理由六氟化铀，UF 6，六氟化钼，MoF 6和四氟化钼组成的处理废物的方法，其中上述混合物在碳酸铵和氢氧化铵的水溶液中水解。将得到的母液在60°-80℃下消化以除去二氧化碳，并将碳酸铀酸铵（NH4）4UO2（CO3）3转化成二氢铀酸铵（NH4）2U2O7。 pH值保持在9以上，以防止钼值过早沉淀为钼酸或钼酸铀。过滤形成黄色固体的二异氰酸铵，在氢氧化铵水溶液中浆化，过滤并干燥。产量是定量的。热解导致将二铀酸盐转化为具有合适纯度的氧化铀U3O8，以在六氟化铀生产过程中再循环。将含有钼值和氟化铵副产物的合并滤液稀释，并用95％乙醇搅拌，沉淀出白色，结晶，钼酸铵（NH 4）2 OO 4。氟化铵保持溶解。将钼酸铵过滤，干燥并在600℃下煅烧2小时，得到三氧化钼，MoO 3> 90％产率，基本上不含铀污染物。任何一种后处理材料中的氟化物污染最小。

36. 发明授权

US4548763A Preparation of vinylphosphonate diesters 失效
标题翻译：乙烯基膦酸二酯的制备
公开(公告)号：US4548763A
公开(公告)日：1985-10-22
申请号：US557782
申请日：1983-12-05
申请人： David Nalewajek , David S. Soriano , Ralph J. Borowski
发明人： David Nalewajek , David S. Soriano , Ralph J. Borowski
IPC分类号： C07F9/40
CPC分类号： C07F9/4015
摘要： Allylphosphonate diesters are converted to vinyl phosphonate diesters by isomerization with a catalytic amount of a ruthenium catalyst. Vinyl phosphonate derivatives are produced directly from an organo pentavalent phosphorus compound. In a particular reaction conversion of allylic phosphonate diesters to vinylic phosphonate diesters is accomplished by the transition metal mediated isomerization of the alkylphosphonate derivatives with tetrakis(triphenylphosphine)dihydrido ruthenium(II).
摘要翻译：烯丙基膦酸酯二酯通过用催化量的钌催化剂异构化而转化为乙烯基膦酸二酯。乙烯基膦酸酯衍生物直接由有机五价磷化合物生产。在烯丙基膦酸酯二酯转化为乙烯基膦酸酯二酯的特定反应中，通过四烷基膦酸酯衍生物与四（三苯基膦）二氢钌（II）的过渡金属介导的异构化来实现。

37. 发明授权

US08901360B2 Process for cis 1,1,1,4,4,4-hexafluoro-2-butene 有权
标题翻译：顺式1,1,1,4,4,4-六氟-2-丁烯的方法
公开(公告)号：US08901360B2
公开(公告)日：2014-12-02
申请号：US13110979
申请日：2011-05-19
申请人： Andrew Joseph Poss , David Nalewajek , Haridasan K. Nair , Michael Van Der Puy
发明人： Andrew Joseph Poss , David Nalewajek , Haridasan K. Nair , Michael Van Der Puy
IPC分类号： C07C21/18 , C07C17/278 , C07C17/04 , C07C17/20 , C07C17/23 , C07C17/25 , C07C17/354
CPC分类号： C07C17/278 , C07C17/04 , C07C17/206 , C07C17/23 , C07C17/25 , C07C17/354 , C07C19/10 , C07C21/22 , C07C21/18
摘要： Disclosed is a process for preparing cis-1,1,1,4,4,4-hexafluorobutene comprising the steps of (a) reacting CCl4 with a compound having the formula CF3CX═CXH, where each X is independently halogen or hydrogen, to form a compound having the formula CF3CXClCXHCCl3; (b) fluorinating the compound formed in step (a) to form a compound having the formula CF3CXHCXHCF3; (c) converting the compound formed in step (b) by a reaction selected from the group consisting of dehydrohalogenation, dehalogenation and both reactions, to form a compound having the formula CF3C≡CCF3; and (d) catalytically reducing the compound formed in step (c) with hydrogen to form the compound having the formula:
摘要翻译：公开了一种制备顺式-1,1,1,4,4,4-六氟丁烯的方法，包括以下步骤：（a）使CCl4与具有式CF 3 C X = C X H的化合物反应，其中每个X独立地为卤素或氢，形成式CF3CXClCXHCCl3的化合物; （b）氟化步骤（a）中形成的化合物以形成具有式CF 3 C XHCXHCF 3的化合物; （c）通过选自脱卤化氢，脱卤和两种反应的反应转化步骤（b）中形成的化合物，以形成具有式CF 3C≡CCF3的化合物; 和（d）用氢气将步骤（c）中形成的化合物催化还原以形成具有下式的化合物：

38. 发明申请

US20110252694A1 COMPOSITIONS FOR DRIP FUMIGATION 审中-公开
标题翻译： DRIP FUMIGATION的组成
公开(公告)号：US20110252694A1
公开(公告)日：2011-10-20
申请号：US12762801
申请日：2010-04-19
申请人： Andrew Joseph Poss , Rajiv Ratna Singh , David Nalewajek , Cheryl Cantlon
发明人： Andrew Joseph Poss , Rajiv Ratna Singh , David Nalewajek , Cheryl Cantlon
IPC分类号： A01M13/00 , A01P13/00 , A01P5/00 , A01N29/00 , A01P3/00
CPC分类号： A01N29/00 , A01N25/04 , A01N2300/00
摘要： Soil fumigation compositions are provided herein that include methyl iodide, at least one fluorocarbon or hydrofluorocarbon, at least one surfactant, and water. The fumigant can be produced by combining the water and surfactant with an initial mixture that is an azeotropic or azeotrope-like mixture of methyl iodide and at least one fluorocarbon or hydrofluorocarbon. The fumigant compositions can be utilized in drip fumigation processes, and have increased volatility as compared to methyl iodide alone, which can reduce the risk of water contamination when utilizing methyl iodide as a fumigant.
摘要翻译：本文提供了包括甲基碘，至少一种碳氟化合物或氢氟烃，至少一种表面活性剂和水的土壤熏蒸组合物。熏蒸剂可以通过将水和表面活性剂与初始混合物（其是甲基碘和至少一种碳氟化合物或氢氟烃的共沸或类共沸混合物）混合来制备。熏蒸剂组合物可用于滴水熏蒸方法，并且与单独的甲基碘相比具有增加的挥发性，当使用甲基碘作为熏蒸剂时，这可以降低水污染的风险。

39. 发明申请

US20110198756A1 Organometallic Precursors and Related Intermediates for Deposition Processes, Their Production and Methods of Use 审中-公开
标题翻译：有机金属前体及相关中间体，用于沉积过程，其生产和使用方法
公开(公告)号：US20110198756A1
公开(公告)日：2011-08-18
申请号：US12067285
申请日：2006-08-25
申请人： ü Thenappan , Chien-Wei Li , David Nalewajek , Martin Cheney , Jingyu Lao , Eric Eisenbraun , Min Li , Nathaniel Berliner , Mikko Ritala , Markku Leskela , kaupo Kukli , Linda Cheney
发明人： ü Thenappan , Chien-Wei Li , David Nalewajek , Martin Cheney , Jingyu Lao , Eric Eisenbraun , Min Li , Nathaniel Berliner , Mikko Ritala , Markku Leskela , kaupo Kukli , Linda Cheney
IPC分类号： H01L21/3205 , H01L29/43 , H01L23/48
CPC分类号： C07F17/02 , C23C16/18
摘要： Vapor deposition precursors that can deposit conformal thin ruthenium films on substrates with a very high growth rate, low resistivity and low levels of carbon, oxygen and nitrogen impurities have been provided. The precursors described herein include a compound having the formula CMC′, wherein M comprises a metal or a metalloid; C comprises a substituted or unsubstituted acyclic alkene, cycloalkene or cycloalkene-like ring structure; and C′ comprises a substituted or unsubstituted acyclic alkene, cycloalkene or cycloalkene-like ring structure; wherein at least one of C and C′ further and individually is substituted with a ligand represented by the formula CH(X)R1, wherein X is a N, P, or S-substituted functional group or hydroxyl, and R1 is hydrogen or a hydrocarbon. Methods of production of the vapor deposition precursors and the resulting films, and uses and end uses of the vapor deposition precursors and resulting films are also described.
摘要翻译：已经提供了可以在非常高的生长速率，低电阻率和低水平的碳，氧和氮杂质的基底上沉积保形薄钌薄膜的气相沉积前体。本文所述的前体包括具有式CMC'的化合物，其中M包含金属或准金属; C包括取代或未取代的无环烯烃，环烯烃或环烯烃环结构; 和C'包括取代或未取代的无环烯烃，环烯烃或环烯烃环结构; 其中C和C'中的至少一个进一步和单独地被式CH（X）R 1表示的配体取代，其中X是N，P或S-取代的官能团或羟基，并且R 1是氢或烃。还描述了气相沉积前体和所得膜的生产方法，以及气相沉积前体和所得膜的用途和最终用途。

40. 发明申请

US20090269478A1 CARRIER SOLVENT FOR FINGERPRINT FORMULATIONS 失效
标题翻译：载体溶液用于指纹制剂
公开(公告)号：US20090269478A1
公开(公告)日：2009-10-29
申请号：US12422260
申请日：2009-04-11
申请人： David Nalewajek , Cheryl L. Cantlon , Andrew J. Poss , Rajiv Ratna Singh , Ian Shankland
发明人： David Nalewajek , Cheryl L. Cantlon , Andrew J. Poss , Rajiv Ratna Singh , Ian Shankland
IPC分类号： A61B5/117 , C09D11/00
CPC分类号： A61B5/1172
摘要： A method and composition for transforming a latent physiological biometric into a visible physiological biometric are provided, the method comprising: providing a latent biometric disposed on a surface of an article, wherein said biometric comprises at least one eccrine-derived compound; contacting said latent biometric with a developing solution, wherein said developing solution comprises at least one imaging reagent selected from ninhydrin and 1,8-diazafluoren-9-one and a carrier solvent comprising at least one C3-C4 hydrofluorocarbon; and reacting said imaging reagent with said eccrine-derived compound to produce a visible physiological biometric.
摘要翻译：提供了一种用于将潜在生理学生物转化为可见生理生物学的方法和组合物，所述方法包括：提供设置在制品表面上的潜伏生物测定，其中所述生物测定包含至少一种衍生化合物; 使所述潜在生物测定与显影溶液接触，其中所述显影溶液包含至少一种选自茚三酮和1,8-二氮杂芴-9-酮的成像试剂和包含至少一种C 3 -C 4氢氟烃的载体溶剂; 并使所述成像试剂与所述外分泌衍生的化合物反应以产生可见的生理学生物学特征。

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