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31. 发明申请

US20120292501A1 MASS SPECTROMETER 有权
标题翻译：质谱仪
公开(公告)号：US20120292501A1
公开(公告)日：2012-11-22
申请号：US13574788
申请日：2011-01-21
申请人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa
发明人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa
IPC分类号： H01J49/12
CPC分类号： H01J49/105 , H01J27/16 , H05H1/2406 , H05H2001/2443
摘要： A mass spectrometer of ionizing a sample by a dielectric barrier discharge under a reduced pressure. An ionization with inconsiderable fragmentation can be carried out highly sensitively by the present invention.
摘要翻译：一种质谱仪，其通过介电阻挡放电在减压下离子化样品。通过本发明可以高度敏感地进行具有不可忽视的碎裂的电离。

32. 发明申请

US20120292495A1 MASS SPECTROMETER AND MASS SPECTROMETRY 有权
标题翻译：质谱仪和质谱仪
公开(公告)号：US20120292495A1
公开(公告)日：2012-11-22
申请号：US13519587
申请日：2010-12-22
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Masuyuki Sugiyama , Hiroyuki Satake
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Masuyuki Sugiyama , Hiroyuki Satake
IPC分类号： H01J49/26
CPC分类号： H01J49/423
摘要： A mass spectrometer possessing both high resolution and durability in a simple, compact structure compared to mass spectrometers of the related art, and characterized in possessing a linear ion trap unit containing a multipolar rod electrode including rod electrodes having fine orifices to allow passage of electrons or ions; a mechanism to move the ions inside the linear ion trap unit along the axis of the multipolar rod electrode; and a detector to selectively detect by mass, ions ejected from the linear ion trap unit.
摘要翻译：质谱仪与现有技术的质谱仪相比在简单，紧凑的结构中具有高分辨率和耐久性，并且其特征在于具有线性离子阱单元，其包含多极杆电极，其包括具有细孔以允许电子通过的棒状电极或离子沿着多极棒电极的轴线移动线性离子阱单元内的离子的机构; 以及用于选择性地检测从线性离子阱单元喷出的离子的检测器。

33. 发明授权

US07592589B2 Method of mass spectrometry and mass spectrometer 有权
标题翻译：质谱法和质谱仪
公开(公告)号：US07592589B2
公开(公告)日：2009-09-22
申请号：US11716615
申请日：2007-03-12
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Takashi Baba , Izumi Waki
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Takashi Baba , Izumi Waki
IPC分类号： H01J49/42
CPC分类号： H01J49/427 , H01J49/067 , H01J49/4225
摘要： A mass spectrometry device includes an ion source for ionizing a sample, an ion trap for trapping ions ionized by the ion source. A control unit for controlling voltages applied to lenses forming part of the ion trap, and a detection unit for detecting the ions trapped by said ion trap. The control unit causes a trap potential to be generated on a central axis of quadrupole rods forming part of the ion trap, causes part of the trapped ions to be oscillated in an intermediate direction between the quadrupole rods which are mutually adjacent to each other, and applies a voltage for ejecting the oscillated ions in a central-axis direction of the quadrupole rods by generating an extraction field.
摘要翻译：质谱装置包括用于离子化样品的离子源，用于捕获由离子源离子化的离子的离子阱。用于控制施加到形成所述离子阱的一部分的透镜的电压的控制单元，以及用于检测由所述离子阱捕获的离子的检测单元。控制单元在形成离子阱的一部分的四极杆的中心轴上产生捕获电位，使被捕获的离子的一部分在彼此相邻的四极棒之间的中间方向振荡，并且通过产生提取场来施加用于在四极棒的中心轴方向上弹出振荡的离子的电压。

34. 发明授权

US07566870B2 Mass spectrometer 有权
标题翻译：质谱仪
公开(公告)号：US07566870B2
公开(公告)日：2009-07-28
申请号：US11446141
申请日：2006-06-05
申请人： Hideki Hasegawa , Yuichiro Hashimoto , Izumi Waki
发明人： Hideki Hasegawa , Yuichiro Hashimoto , Izumi Waki
IPC分类号： H01J49/42
CPC分类号： H01J49/4225 , H01J49/4265
摘要： A mass spectrometer capable of realizing a high-sensitivity ion analysis and a high ion selectivity performance. The mass spectrometer includes the ion source where ions are produced, the ion trap where ions are accumulated, isolated, dissociated, and ejected, the detector to detect ions to be detected, and the controller to control operations of the ion trap. It has the features that the total ion accumulation in or just before each period is calculated based on the result obtained from the mass spectrometry in the preceding period, and that in at least one out of all periods, the condition of voltage applied to the ion trap is corrected depending on the total ion accumulation. Compared to the related art, the mass spectrometer of the present invention provides much improved performance in analysis sensitivity and ion selectivity.
摘要翻译：能够实现高灵敏度离子分析和高离子选择性的质谱仪。质谱仪包括产生离子的离子源，其中离子聚集，分离，离解和喷射的离子阱，检测器检测要被检测的离子，以及控制器来控制离子阱的操作。其特征在于，基于从前一期间的质谱获得的结果计算出每个周期之前或之前的总离子积聚，并且在至少一个周期内计算施加到离子的电压的条件根据总离子积聚校正捕获阱。与现有技术相比，本发明的质谱仪在分析灵敏度和离子选择性方面提供了大大改进的性能。

35. 发明申请

US20080116372A1 MASS SPECTROMETER AND METHOD OF MASS SPECTROMETRY 有权
标题翻译：质谱仪和质谱法
公开(公告)号：US20080116372A1
公开(公告)日：2008-05-22
申请号：US11745516
申请日：2007-05-08
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki , Masuyuki Sugiyama
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki , Masuyuki Sugiyama
IPC分类号： H01J49/42
CPC分类号： H01J49/4225 , H01J49/429
摘要： A linear trap having high ejection efficiency and low ejection energy is realized. In a mass spectrometer in which ion generated by an ion source are introduced to a quadrupole rod structure applied with RF voltage and ejected from the quadrupole rod structure so as to be detected by a detection mechanism, a mass dependent potential is formed in the axial direction of the quadrupole rod structure and ions are ejected mass selectively from the vicinity of a minimum point of the potential, the mass dependent potential being formed by applying electrostatic voltage and RF voltage to an insertion electrode inserted in the quadrupole rods.
摘要翻译：实现了具有高喷射效率和低喷射能量的线性阱。在质谱仪中，将由离子源产生的离子引入施加有RF电压的四极杆结构并从四极棒结构喷出以便通过检测机构检测，质量依赖电位在轴向上形成的四极杆结构和离子从电位的最小点附近选择性地排出，质量依赖电位通过将静电电压和RF电压施加到插入四极棒中的插入电极而形成。

36. 发明授权

US07348554B2 Mass spectrometer 有权
标题翻译：质谱仪
公开(公告)号：US07348554B2
公开(公告)日：2008-03-25
申请号：US11146157
申请日：2005-06-07
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Takashi Baba , Hiroyuki Satake , Izumi Waki
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Takashi Baba , Hiroyuki Satake , Izumi Waki
IPC分类号： B01D59/44 , H01J49/00
CPC分类号： H01J49/4225 , H01J49/004 , H01J49/4265
摘要： A mass spectrometer includes: an ion source for ionizing a specimen to generate ions, an ion transport portion for transporting the ions, a linear ion trap portion for accumulating the transported ions by a potential formed axially, and a control portion of ejecting the ions within a second m/z range different from a first m/z range, from the linear ion trap portion, and substantially at the same timing as the timing of accumulating the ions within the first m/z range from the transport portion into the linear ion trap portion. The ion transportation portion having a mass selection means for selecting the ions in the first m/z range.
摘要翻译：质谱仪包括：离子源，用于离子化样品以产生离子;离子传输部分，用于输送离子;线性离子捕获部分，用于通过轴向形成的电位积聚所运送的离子;以及控制部分，与线性离子阱部分不同于第一m / z范围的第二m / z范围，并且基本上与从运输部分到线性离子的离子在第一m / z范围内的积累时间基本相同的时刻陷阱部分。该离子传送部分具有用于选择第一m / z范围内的离子的质量选择装置。

37. 发明申请

US20070181804A1 Method of mass spectrometry and mass spectrometer 有权
标题翻译：质谱法和质谱仪
公开(公告)号：US20070181804A1
公开(公告)日：2007-08-09
申请号：US11716615
申请日：2007-03-12
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Takashi Baba , Izumi Waki
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Takashi Baba , Izumi Waki
IPC分类号： B01D59/44
CPC分类号： H01J49/427 , H01J49/067 , H01J49/4225
摘要： A mass spectrometry device includes an ion source for ionizing a sample, an ion trap for trapping ions ionized by the ion source. A control unit for controlling voltages applied to lenses forming part of the ion trap, and a detection unit for detecting the ions trapped by said ion trap. The control unit causes a trap potential to be generated on a central axis of quadrupole rods forming part of the ion trap, causes part of the trapped ions to be oscillated in an intermediate direction between the quadrupole rods which are mutually adjacent to each other, and applies a voltage for ejecting the oscillated ions in a central-axis direction of the quadrupole rods by generating an extraction field.
摘要翻译：质谱装置包括用于离子化样品的离子源，用于捕获由离子源离子化的离子的离子阱。用于控制施加到形成所述离子阱的一部分的透镜的电压的控制单元，以及用于检测由所述离子阱捕获的离子的检测单元。控制单元在形成离子阱的一部分的四极杆的中心轴上产生捕获电位，使被捕获的离子的一部分在彼此相邻的四极棒之间的中间方向振荡，并且通过产生提取场来施加用于在四极棒的中心轴方向上弹出振荡的离子的电压。

38. 发明申请

US20060219896A1 Mass spectrometer and mass analysis method 有权
标题翻译：质谱仪和质量分析方法
公开(公告)号：US20060219896A1
公开(公告)日：2006-10-05
申请号：US11325444
申请日：2006-01-05
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki
IPC分类号： H01J49/00 , B01D59/44
CPC分类号： H01J49/0027 , H01J49/4225
摘要： A linear trap which allows for charge separation and ion mobility separation in a speedy manner, and enables measurement with high duty cycle. A mass spectrometer comprises an ion source, an ion trap for trapping ions ionized by the ion source, an ion trap controller for controlling a voltage on an electrode included in the ion trap, and a detector for detecting the ions ejected from the ion trap. The ion trap controller includes a table for each mass-to-charge ratio, the table containing a frequency of the voltage used for charge separation, and a gain of the voltage for ejecting a first ion with a first charge outside the ion trap, and retaining in the ion trap a second group of ions with a second charge that is lower than that of the first charge. The ion trap controller controls the voltage based on the mass-to-charge ratio set. The mass spectrometer has significantly improved sensitivity, as compared to the prior art.
摘要翻译：线性阱可以快速分离电荷和离子迁移分离，并能够以高占空比进行测量。质谱仪包括离子源，用于捕获由离子源离子化的离子的离子阱，用于控制离子阱中包含的电极上的电压的离子阱控制器和用于检测从离子阱排出的离子的检测器。离子阱控制器包括用于每个质荷比的表，该表包含用于电荷分离的电压的频率，以及用于在离子阱外部用第一电荷喷射第一离子的电压的增益，以及在离子阱中保留具有低于第一电荷的第二组电荷的第二组离子。离子阱控制器根据设定的质荷比来控制电压。与现有技术相比，质谱仪具有显着提高的灵敏度。

39. 发明申请

US20060071159A1 Ion-mobility spectrometer and ion-mobility analysis method 有权
标题翻译：离子迁移谱仪和离子迁移率分析方法
公开(公告)号：US20060071159A1
公开(公告)日：2006-04-06
申请号：US11072267
申请日：2005-03-07
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki
IPC分类号： H01J49/40
CPC分类号： G01N27/622
摘要： There is provided an ion-mobility spectrometer. This apparatus includes the following configuration components: An ion source for generating first ions, a first drift unit for separating the first ions by flight drift times, an ion dissociation unit for generating second ions by dissociating the first ions separated, and a second drift unit for separating the second ions by flight drift times. Moreover, the first drift unit, the ion dissociation unit, and the second drift unit are located inside a chamber whose pressure is set at 10 mTorr or higher. This apparatus allows execution of low-cost and high-resolving-power ion separation and detection.
摘要翻译：提供了离子迁移谱仪。该装置包括以下配置组件：用于产生第一离子的离子源，用于通过飞行漂移时间分离第一离子的第一漂移单元，用于通过解离分离的第一离子产生第二离子的离子解离单元和第二漂移单元用于通过飞行漂移时间分离第二离子。此外，第一漂移单元，离子解离单元和第二漂移单元位于压力设定在10mTorr以上的室内。该装置允许执行低成本和高分辨率的离子分离和检测。

40. 发明申请

US20050269504A1 Mass spectrometer 有权
标题翻译：质谱仪
公开(公告)号：US20050269504A1
公开(公告)日：2005-12-08
申请号：US11146157
申请日：2005-06-07
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Takashi Baba , Hiroyuki Satake , Izumi Waki
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Takashi Baba , Hiroyuki Satake , Izumi Waki
IPC分类号： G01N27/62 , H01J49/06 , H01J49/16 , H01J49/40 , H01J49/42
CPC分类号： H01J49/4225 , H01J49/004 , H01J49/4265
摘要： A mass spectrometer using a linear ion trap capable of efficiently suppressing the space charge and enabling scanning for a wide m/z range at a high Duty Cycle is provided. The mass spectrometer comprises: an ion source for ionizing a specimen to generate ions, an ion transport portion for transporting the ions, a linear ion trap portion for accumulating the transported ions by a potential formed axially, and a control portion of ejecting the ions within a second m/z range different from a first m/z range from the linear ion trap portion substantially at the same timing as the timing of accumulating the ions within the first m/z range to the linear ion trap portion, in which the control portion conducts control of ejecting the ions mass selectively from the linear ion trap portion by any of voltage application of (1) applying a supplemental AC voltage between at least a pair of linear ion trap rods constituting the linear ion trap portion, (2) applying a supplemental AC voltage to an end lens constituting the linear ion trap portion, and (3) applying a supplemental AC voltage between inserted lenses, the inserted lenses constituting the linear ion trap portion. The ion transportation portion having a mass selection means for selecting the ions in the first m/z range.
摘要翻译：提供了使用能够有效地抑制空间电荷且能够在高占空比下扫描宽m / z范围的线性离子阱的质谱仪。该质谱仪包括：用于离子化离子的离子源，用于输送离子的离子传输部分，用于通过轴向形成的电势积聚运送的离子的线性离子捕获部分，以及将离子排出的控制部分基本上与在线性离子阱部分内将离子累积到第一m / z范围内的时刻相同的定时，与线性离子阱部分的第一m / z范围不同的第二m / z范围，其中控制通过施加（1）在构成线性离子阱部分的至少一对线性离子阱捕获棒之间施加补充AC电压的任何电压施加（2）施加的线性离子阱部分，构成线性离子阱部分的端部透镜的补充AC电压，以及（3）在插入的透镜之间施加补充AC电压，构成线性离子阱po的插入透镜 rtion。该离子传送部分具有用于选择第一m / z范围内的离子的质量选择装置。

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