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31. 发明申请

US20080132600A1 N-Substituted Imides As Polymerization Initiators 有权
公开(公告)号：US20080132600A1
公开(公告)日：2008-06-05
申请号：US11666887
申请日：2005-10-31
申请人： Peter Nesvadba , Johannes Benkhoff , Lucienne Bugnon , Karin Powell , Tunja Jung
发明人： Peter Nesvadba , Johannes Benkhoff , Lucienne Bugnon , Karin Powell , Tunja Jung
IPC分类号： C08L79/08 , C07D209/48 , C07D221/06 , C07D207/46 , C07D209/56
CPC分类号： C07D207/404 , B33Y70/00 , C07D207/46 , C07D209/48 , C07D221/14 , C08F4/00
摘要： The invention relates to novel N-substituted imides and polymerizable compositions comprising these N-substituted imides. The invention further relates to the use of N-substituted imides as polymerization initiators. The imides are compounds of the formula (I) and (II) wherein n is 1 or 2; m is 1 or 2; R1 and R2 are each, independently of one another, hydrogen, C1-C18alkyl, C1-C18alkenyl C6-C14aryl, aralkyl, C5-C12cycloalkyl, each of which may be substituted by halogen, C1-C4-alkyl, hydroxy, C1-C6alkoxy, carbonyl, C1-C6alkoxycarbonyl; or R1 and R2 together with the adjacent —CO—N—CO— group may form a monocyclic, bicyclic or polycyclic ring, said ring having up to 50 non hydrogen atoms and wherein said ring may contain the structural element (formula III) more than once; R3 if n is 1, is C1-C18alkyl, C6-C14aryl, aralkyl, C5-C12cycloalkyl, OR10 or SR11, NR12R13; wherein R3 if n is 2, is C2-C12alkylene, C6-C14arylene, xylylene R4 and R5, correspond to R1 and R2; R6 if n is 1, is hydrogen, C1-C18alkyl, C6-C14aryl, aralkyl, C5-C12cycloalkyl, NR14R15; wherein R6 if n is 2, is C2-C12alkylene, C6-C14arylene, xylylene; R7 is hydrogen, C1-C18alkyl, C6-C14aryl, aralkyl, C5-C12cycloalkyl, each of which may be substituted by halogen, C1-C4-alkyl, hydroxy, C1-C6alkoxy, carbonyl, C1-C6alkoxy-carbonyl; or R7 and R14 or R7 and R15 form together with the N-atom attached to R7 a 5-6 membered ring, optionally interrupted by —NH—, —N(C1-C8alkyl)-, —O- and/or S-atoms.

32. 发明授权

US07279200B2 Process for producing coatings using surface-active photoinitiators 有权
标题翻译：使用表面活性光引发剂生产涂料的方法
公开(公告)号：US07279200B2
公开(公告)日：2007-10-09
申请号：US10343620
申请日：2001-08-07
申请人： Gisèle Baudin , Tunja Jung
发明人： Gisèle Baudin , Tunja Jung
IPC分类号： B05D3/06 , G03C1/00
CPC分类号： G03F7/0757 , B33Y70/00 , C07C69/738 , C08F2/50 , C09D4/06 , G03F7/029 , C08F290/067
摘要： A process for producing stable, scratch-resistant coatings comprising the preparation of a photocurable formulation containing certain siloxane photoinitiators as surface-active initiators, application of the formulation to a substrate and the curing of the formulation by exposure to electromagnetic radiation with wavelengths from 200 nm into the IR region and prior, simultaneous or subsequent exposure to heat.
摘要翻译：一种用于生产稳定的耐划伤涂层的方法，包括制备含有某些硅氧烷光引发剂作为表面活性引发剂的光固化制剂，将配方施用于基材和通过暴露于波长为200nm的电磁辐射固化该制剂进入IR区域，并在之前，同时或随后的暴露于热量。

33. 发明申请

US20050129859A1 Curing of coating induced by plasma 有权
标题翻译：固化由等离子体引起的涂层
公开(公告)号：US20050129859A1
公开(公告)日：2005-06-16
申请号：US10511578
申请日：2003-04-17
申请人： Ljubomir Misev , Andreas Valet , Peter Simmendinger , Tunja Jung
发明人： Ljubomir Misev , Andreas Valet , Peter Simmendinger , Tunja Jung
IPC分类号： B05D7/24 , B05D3/14 , C01B32/336 , C08F2/44 , C08F2/50 , C08F2/52 , C08J7/00 , C09D4/00 , C09D7/12 , C09D11/00 , H05H1/00 , B05D3/02
CPC分类号： B05D3/147
摘要： The Application relates to a method of curing various polymerisable compositions, comprising a suitable photoinitiator, the curing being effected by means of a plasma in plasma discharge chamber.
摘要翻译：本申请涉及一种固化各种可聚合组合物的方法，其包含合适的光引发剂，该固化通过等离子体放电室中的等离子体进行。

34. 发明授权

US06376568B1 Surface-active photoinitiators 有权
标题翻译：表面活性光引发剂
公开(公告)号：US06376568B1
公开(公告)日：2002-04-23
申请号：US09618821
申请日：2000-07-18
申请人： Giséle Baudin , Tunja Jung
发明人： Giséle Baudin , Tunja Jung
IPC分类号： C08F246
CPC分类号： C07F7/21 , C07F7/0838 , C08F2/50 , Y10S522/905 , Y10T428/31663
摘要： The invention relates to the use of surface-active photoinitiators of formula I the units being arranged randomly or in blocks, and wherein n is a number from 1 to 1000; m is a number from 0 to 100; p is a number from 0 to 10 000; x is the number 1, or, when n is 1, x may also be the number 2; A1 and A2 are, for example, C1-C18alkyl; or A1 and A2 together are a single bond; R1, R2 and R3 are, for example, each independently of the others C1-C18alkyl, phenyl or C5-C8cycloalkyl; R4 is, for example, unsubstituted or substituted C1-C18alkyl, unsubstituted or substituted phenyl or C5-C8cycloalkyl; IN, when x is 1, is a radical of formula or IN, when x is 2, is a radical of formula R13 and R14 are, for example, each independently of the other C1-C12alkyl; Y is, for example, —(CH2)a—O—; X is OR15 or N(R16)(R17); R15 is, for example, hydrogen or C1-C4alkyl; R16 and R17 are, for example, hydrogen or C1-C12alkyl; X1 has, for example, one of the meanings of X; and R18 is, for example, —(CH2)a—; in photochemically and combined photochemically and thermally crosslinkable formulations.
摘要翻译：本发明涉及式（I）的表面活性光引发剂的使用，其单位是随机或嵌段排列，其中n为1至1000的数; m是从0到100的数字; p是从0到10000的数字; x是数字1，或者当n是1时，x也可以是数字2; A1和A2是例如C1-C18烷基; 或A1和A2一起是单键; R 1，R 2和R 3例如各自独立地为C 1 -C 18烷基，苯基或C 5 -C 8环烷基; R4是例如未取代或取代的C1-C18烷基，未取代或取代的苯基或C5-C8环烷基; IN，当x为1时，是式IA的基团，当x为2时，为式R 13和R 14的基团，例如各自独立地为C 1 -C 12烷基; Y是例如 - （CH 2）a -O-; X是OR 15或N（R 16）（R 17）; R 15是例如氢或C 1 -C 4烷基; R 16和R 17是例如氢或C 1 -C 12烷基; X1具有例如X的含义之一; 并且R 18是例如 - （CH 2）a - ;在光化学和组合的光化学和热交联的制剂中。

35. 发明授权

US08003169B2 Curing of coating induced by plasma 有权
标题翻译：固化由等离子体引起的涂层
公开(公告)号：US08003169B2
公开(公告)日：2011-08-23
申请号：US10511578
申请日：2003-04-17
申请人： Ljubomir Misev , Andreas Valet , Peter Simmendinger , Tunja Jung
发明人： Ljubomir Misev , Andreas Valet , Peter Simmendinger , Tunja Jung
IPC分类号： B05D3/02 , C08J7/18 , H05H1/00 , C08F2/46
CPC分类号： B05D3/147
摘要： The Application relates to a method of curing various polymerisable compositions, comprising a suitable photoinitiator, the curing being effected by means of a plasma in plasma discharge chamber.
摘要翻译：本申请涉及一种固化各种可聚合组合物的方法，其包含合适的光引发剂，该固化通过等离子体放电室中的等离子体进行。

36. 发明申请

US20070240609A1 Photoinitiators 有权
公开(公告)号：US20070240609A1
公开(公告)日：2007-10-18
申请号：US11578595
申请日：2005-04-11
申请人： Rinaldo Husler , Thomas Horni , Andre Fuchs , Tunja Jung , Reinhard Sommerlade
发明人： Rinaldo Husler , Thomas Horni , Andre Fuchs , Tunja Jung , Reinhard Sommerlade
IPC分类号： D21H17/07 , C08F2/48 , C08J3/28
CPC分类号： C07C45/46 , B33Y70/00 , C07C45/58 , C07C45/63 , C07C45/64 , C07C45/71 , C07C45/74 , C07C49/792 , C07C49/82 , C07C49/83 , C07C49/84 , C07C69/96 , C07C271/12 , C07C317/24 , C07D295/108 , C07D295/112 , C07D493/08 , C08F2/50 , C07C49/76 , C07C49/80 , C07C49/813
摘要： The invention relates to novel photoinitators of formulae (V), (II), (III), (IV), (V) and (VI) wherein R1 and R2 are each independently of the other C1-C8alkyl; C1-C4alkyl substituted by OH, C1-C4alkoxy, —COO(C1-C8alkyl), (C1-C4alkyl)-COO—, —CN, benzyl, phenyl or by —N(R15)(R16); C3-C6alkerlyl, benzyl, —CH2—C6H4—(C1-C4alkyl) or phenyl; or R1 and R2 together are unbranched or branched C2-C9alkylene or C3-C6-oxa- or -azaalkylene; R3, R4, R5 and R6 are each independently of the others hydrogen, C1-C8alkyl, C3-C6alkenyl, benzyl, —CH2—C6H4—(C1-C4alkyl) or phenyl; R3 and R4 together and/or R5 and R6 together are unbranched or branched C2-C9alkylene; A is Cl, Br, —O—R9, —N(R11)(R12) or —S—R18, A′ is —O—, —NH— or —NR11—; A″ is Cl, Br, —O—R9, —N(R11)(R12) or —S—R18 or hydrogen, X is —O—R10 or —N(R13)(R14), n is an integer from 1 to 10, preferably an integer from 1 to 4, especially 1, 2 or 3; R7 is a linker; R8 is a bivalent C2-C3alkylele radical.

37. 发明申请

US20070093576A1 Reinforced coatings with improved scratch resistance 审中-公开
标题翻译：具有改善耐刮擦性的增强涂层
公开(公告)号：US20070093576A1
公开(公告)日：2007-04-26
申请号：US10574766
申请日：2004-10-06
申请人： Martin Albrecht , Tunja Jung , Andreas Muhlebach
发明人： Martin Albrecht , Tunja Jung , Andreas Muhlebach
IPC分类号： B60C1/00
CPC分类号： C08K3/01 , C08K3/36 , C09D7/60 , C09D7/61 , C09D7/67 , C09D7/68
摘要： The instant invention discloses a coating composition comprising a) an organic film-forming binder, and b) an inorganic additive of small particle size dispersed in an aqueous or alcoholic solvent prepared by a process which comprises the hydrolysis of a metal alcoholate or a compound of the formula (I) in which R1 is C1-C8alkyl, C5-C8cycloalkyl, phenyl or C1-C4alkyl substituted phenyl; R2 is C1-C8salkyl, and n is 0, 1, 2 or 3; with a base. These coatings for protecting surfaces are reinforced and show improved scratch resistance.
摘要翻译：本发明公开了一种涂料组合物，其包含a）有机成膜粘合剂，和b）分散在水溶液或醇溶剂中的小粒径的无机添加剂，该无机添加剂通过包括水解金属醇化物或其中R 1是C 1 -C 8烷基，C 5 -C 6烷基的式（I）苯基或C 1 -C 4烷基取代的苯基; C 1 -C 4烷基取代的苯基; R 2是C 1 -C 8烷基，n是0,1,2或3; 与一个基地。这些用于保护表面的涂层被加强并显示出改善的耐划伤性。

38. 发明授权

US07105582B2 Surface-active siloxane photoinitiators 有权
标题翻译：表面活性硅氧烷光引发剂
公开(公告)号：US07105582B2
公开(公告)日：2006-09-12
申请号：US10503320
申请日：2003-01-28
申请人： Gisèle Baudin , Tunja Jung
发明人： Gisèle Baudin , Tunja Jung
IPC分类号： C08F2/50
CPC分类号： C08F2/50 , B33Y70/00
摘要： Compounds of the formula I are suitable photoinitiators which accumulates at the surface of the formulation in which R is for example phenyl and A is a surface-active radical of the formula III Y is a divalent group C3–C12cycloalkylene, C6–C12bicycloalkylene; C1–C6alkylenen-C3–C12cycloalkylene, C1–C6alkylene- C6–C12bicycloalkylene or C1–C10alkylene interrupted by one or more non-consecutive C3–C12cycloalkylene, —U—C3–C12cycloalkylene, C6–C12bicycloalkylene or —U—C6–C12bicycloalkylene; C1–C10alkylene interrupted by one or more non-consecutive O and C3–C12cycloalkylene, —U—C3–C12cycloalkylene, C6–C12bicycloalkylene and/or —U—C6–C12bicycloalkylene; U is U′ or U″ U′ is —(CH2)aCOO—; U″ is —Si(CH3)(CH3)— or —(CH2)a—Si(CH3)(CH3)—, a is a number from 1 to 10; b is a number from 0 to 10; with the proviso that they are, however, at least 1 if the methylene group in question is between two oxygen atoms.
摘要翻译：式I的化合物是在制剂的表面积聚的适合的光引发剂，其中R是例如苯基，A是式III的表面活性基团Y是二价基团C 3 - C 12亚环烷基，C 6 -C 12亚环烷基; C 1 -C 6亚烷基-C 3 -C 12亚环烷基，C 1〜 C 1 -C 6亚烷基-C 6亚烷基或C 1 -C 10亚烷基-C 12 - 由一个或多个非连续C 3 -C 12亚环烷基，-UC 3 -C 12间隔的亚烷基亚烷基，亚烷基，C 6 -C 12亚环烷基或-CUC 6 -C 12二环亚烷基; 被一个或多个不连续的O和C 3 -C 12亚环烷基间隔的C 1 -C 10亚烷基，-CUC 3 -C 12亚环烷基，C 6 -C 12二环亚烷基和/或-UC _{6 -C 12二环亚烷基; U是U'或U“U'是 - （CH 2）n CO 2 - U“是-Si（CH 3）3（CH 3） - 或 - （CH 2 CH 2）a - -Si（CH 3 3）（CH 3） - ，a为1至10的数; b是从0到10的数字; 但是，如果所讨论的亚甲基在两个氧原子之间，则它们至少为1。}

39. 发明授权

US07005281B2 Enzymatic process for preparing organosilicon group containing photoinitiators 有权
公开(公告)号：US07005281B2
公开(公告)日：2006-02-28
申请号：US10506698
申请日：2003-02-25
申请人： Reinhold Öhrlein , Kai-Uwe Schöning , Gabriele Baisch , Jemima Schmidt , Gisèle Baudin , Tunja Jung
发明人： Reinhold Öhrlein , Kai-Uwe Schöning , Gabriele Baisch , Jemima Schmidt , Gisèle Baudin , Tunja Jung
IPC分类号： C12P7/62 , C12P7/26 , C12P13/02
CPC分类号： C07F7/0889 , C12P9/00
摘要： The invention relates to a process for preparing organosilicon group containing photoinitiators of the formula (I), wherein m is a number from 1 to 200; q is 0 or 1; A is IN-C(O)—O—CHR3—Y— or IN-C(O)—NH—CHR3—Y—; A′ is A or R1′; R1 and R1′, R2 and R2′ are C1–C18alkyl or phenyl, or —(O)q—SiR1R1′R2; R3 is hydrogen or C1–C6alkyl, Y is a divalent group selected from C1–C10alkeylene, C2–C10alkenylene or —(CH2)b—O—(CH2)a—; and b are each independently of the other a number of 1 to 6; IN is a photolabile functional moiety of the formula (II) or (III), wherein R4 is hydrogen or —C(O)—C(O)—OH or —C(O)—C(O)—OC1–C6alkyl and n is 1–3; R5 and R6 are C1–C12alkyl or together are cycloC5–C7alkyl; R7 is hydroxy, C1–C6alkoxy or morpholinyl; X is —(CH2)a—, —(CH2)b—O—(CH2)a— or —(CH2)b—O—CO—(CH2)a—; a and b are each independently of the other a number of 1 to 6; whereby the process is characterized in that a photolabile functional moiety containing a carboxy group (IN-COOH) or an alkoxycarbonyl group (IN-CO—OC1–C6alkyl) is reacted with a carbinol- or amino terminated organosilicon compound of the formula (IV), wherein m, R1 and R1′, R2 and R2′ are as defined above and B is —Y—CHR3—OH or —Y—CHR3—NH2; B′ is B or R1′, in the presence of an enzyme which catalyzes the esterification, transesterification or amidation reaction.

40. 发明授权

US06906113B2 Surface-active photoinitiators 失效
标题翻译：表面活性光引发剂
公开(公告)号：US06906113B2
公开(公告)日：2005-06-14
申请号：US10343617
申请日：2001-08-07
申请人： Gisèle Baudin , Tunja Jung
发明人： Gisèle Baudin , Tunja Jung
IPC分类号： C07C69/716 , C07C69/738 , C07F7/08 , C08F2/00 , C08F2/46 , C08F2/50 , C08L83/06 , C09D4/00 , C09D4/06 , C09D5/00 , C07D307/93
CPC分类号： C07C69/738 , B33Y70/00 , C07F7/0838 , C08F2/50 , Y10S522/905
摘要： Compounds of formula Ia, Ib and Ic, (Ic), in which R, R1 and R2 are e.g. phenyl, naphthyl, anthracyl, phenanthryl or a heterocyclic radical, are suitable as photoinitiators which accumulate at the surface of coatings.
摘要翻译：式Ia，Ib和Ic，（Ic）的化合物，其中R 1，R 1和R 2是例如。苯基，萘基，蒽基，菲基或杂环基，适合作为在涂层表面积聚的光引发剂。

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