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31. 发明授权

US4297455A Process for the preparation of carbonic acid aryl esters of polyester-diols lengthened via carbonate groups and their use for the preparation of polyester-diol bis-diphenol carbonates and polyester/polycarbonates 失效
标题翻译：通过碳酸酯基延长的聚酯二醇的碳酸芳酯的制备方法及其用于制备聚酯 - 二醇双二酚碳酸酯和聚酯/聚碳酸酯的用途
公开(公告)号：US4297455A
公开(公告)日：1981-10-27
申请号：US910986
申请日：1978-05-30
申请人： Christian Lindner , Carlhans Suling , Herbert Bartl , Manfred Schreckenberg , Dieter Freitag , Klaus Konig
发明人： Christian Lindner , Carlhans Suling , Herbert Bartl , Manfred Schreckenberg , Dieter Freitag , Klaus Konig
IPC分类号： C08G63/64 , C08G63/00 , C08G63/76
CPC分类号： C08G63/64
摘要： The present invention relates to a process for the preparation of bis-carbonic acid aryl esters of polyester-diols, lengthened via --OCOO-- groups, characterized in that polyester-diols with molecular weights Mn (number-average) of over 250, preferably over 600, are heated with carbonic acid bis-aryl esters at temperatures between about 100.degree. C. and 200.degree. C., preferably between about 110.degree. C. and 180.degree. C., in vacuo below about 35 mm Hg, preferably between about 25 and 1 mm Hg, in the presence of catalysts, less than one mol of carbonic acid bis-aryl ester being employed per OH group of the polyester-diol and the hydroxyaryl compounds formed being distilled off.The invention further relates to the bis-carbonic acid aryl esters of polyester-diols lengthened via --OCOO-- groups obtained according to the instant invention and their use for the preparation of polyester diol bis-diphenol carbonates, lengthened via carbonate groups, characterized in that polyester-diol bis-aryl carbonates are reacted with a diphenol at a temperature of from about 100.degree. to about 200.degree. C. in vacuo below about 35 mm Hg in the presence of a catalyst, wherein more than 1 mol of diphenol is employed per mol of carbonic acid aryl ester groups of the polyester-diol bis-aryl carbonate, lengthened via carbonate groups, and the resulting hydroxyaryl compound is distilled off.The invention finally relates to the polyester-diol bis-diphenol carbonates, lengthened via carbonate groups obtained according to the instant invention and their use for the preparation of polyester/polycarbonates and the polycarbonate/polyesters so prepared.
摘要翻译：本发明涉及通过-OCOO-基团延长的聚酯二醇的双碳酸芳基酯的制备方法，其特征在于分子量Mn（数均分子）超过250的聚酯二醇优选超过 600，在约100℃至200℃之间，优选约110℃至180℃之间的温度下，用碳酸双芳基酯加热，真空度低于约35mmHg，优选约25mm 和1mm Hg，在催化剂的存在下，每聚酯二醇的OH基和所形成的羟基芳基化合物使用少于1摩尔的碳酸双芳基酯。本发明还涉及通过根据本发明获得的-OCOO-基团延长的聚酯二醇的双碳酸芳基酯及其用于制备通过碳酸酯基团延长的聚酯二醇双 - 二酚酚酸酯的用途，其特征在于在催化剂存在下，聚酯 - 二醇双芳基碳酸酯与二酚在约100至约200℃的温度下在真空下在约35mm Hg下真空反应，其中每次使用多于1mol的二酚将通过碳酸酯基延长的聚酯 - 二醇双芳基碳酸酯的碳酸芳基酯基和所得羟基芳基化合物蒸馏出。本发明最终涉及通过根据本发明获得的碳酸酯基团延长的聚酯 - 二醇双 - 二酚碳酸酯及其制备聚酯/聚碳酸酯和如此制备的聚碳酸酯/聚酯的用途。

32. 发明授权

US4217437A Process for the preparation of carbonic acid bis-diphenol esters of polyalkylene oxide-diols lengthened via carbonate groups and their use for the preparation of high-molecular, segmented polyether/polycarbonates which can be processed as thermoplastics 失效
标题翻译：通过碳酸酯基加成的聚环氧烷 - 二醇的碳酸双 - 二酚酯的制备方法及其用于制备高分子，分段聚醚/聚碳酸酯的方法，可以加工成热塑性塑料
公开(公告)号：US4217437A
公开(公告)日：1980-08-12
申请号：US913773
申请日：1978-06-08
申请人： Manfred Schreckenberg , Dieter Freitag , Christian Lindner , Carlhans Suling , Herbert Bartl , Klaus Konig
发明人： Manfred Schreckenberg , Dieter Freitag , Christian Lindner , Carlhans Suling , Herbert Bartl , Klaus Konig
IPC分类号： C08G63/00 , B01J31/00 , C07B61/00 , C07C67/00 , C07C69/96 , C07C313/00 , C07C315/04 , C07C317/22 , C07C319/20 , C07C323/20 , C08G64/00 , C08G64/16 , C08G64/18 , C08G64/20 , C08G64/22 , C08G64/24 , C08G64/30 , C08G63/62
CPC分类号： C08G64/183
摘要： The present invention relates to the transesterification of the carbonic acid aryl esters obtainable according to German Published Patent Specification No. 2,650,533 with an excess of diphenol for the preparation of polyalkylene oxide-diol bis-diphenol carbonates lengthened via carbonate groups. The present invention also relates to the polyalkylene oxide-diol bis-diphenol carbonates, lengthened via carbonate groups, obtained according to the invention and their use for the preparation of polyether/polycarbonates. Finally, the present invention relates to the polyether/polycarbonates, obtained according to the invention, with an improved phase separation between the elastomeric segment and hard segment, which leads to better technological properties of the corresponding polycarbonate elastomers.
摘要翻译：本发明涉及根据德国公开专利说明书2,650,533可得到的碳酸芳基酯与过量的二酚的酯交换反应，用于制备通过碳酸酯基团延长的聚亚烷基氧化物 - 二醇双酚酚碳酸酯。本发明还涉及根据本发明获得的通过碳酸酯基延长的聚环氧烷 - 二醇双 - 二酚碳酸酯及其在制备聚醚/聚碳酸酯中的用途。最后，本发明涉及根据本发明获得的聚醚/聚碳酸酯，其在弹性链段和硬链段之间具有改进的相分离，这导致相应的聚碳酸酯弹性体的更好的技术性能。

33. 发明授权

US4217297A Process for the preparation of carbonic acid aryl esters of polyester-diols lengthened via carbonate groups 失效
标题翻译：通过碳酸酯基团延长的聚酯二醇的碳酸芳酯的制备方法
公开(公告)号：US4217297A
公开(公告)日：1980-08-12
申请号：US886212
申请日：1978-03-13
申请人： Christian Lindner , Carlhans Suling , Herbert Bartl , Manfred Schreckenberg , Dieter Freitag , Klaus Konig
发明人： Christian Lindner , Carlhans Suling , Herbert Bartl , Manfred Schreckenberg , Dieter Freitag , Klaus Konig
IPC分类号： C08G63/00 , C08G63/64 , C08G63/66 , C07C68/06 , C08G63/62
CPC分类号： C08G63/64
摘要： The present invention relates to a process for the preparation of bis-carbonic acid monoaryl esters of polyester-diols, lengthened via --OCOO-- groups, characterized in that polyester-diols with molecular weights Mn (number-average) of over 250, preferably over 600, are heated with carbonic acid bis-aryl esters at temperatures between about 100.degree. C. and 200.degree. C., preferably between about 110.degree. C. and 180.degree. C., in vacuo below about 35 mm Hg, preferably between about 25 and 1 mm Hg, in the presence of catalysts, less than one mol of carbonic acid bis-aryl ester being employed per mol of OH group of the polyester-diol and the hydroxyaryl compounds formed being distilled off.The invention further relates to the bis-carbonic acid aryl esters of polyester-diols lengthened via --OCOO-- groups.
摘要翻译：本发明涉及通过-OCOO-基团来制备聚酯二醇的双碳酸单芳基酯的方法，其特征在于分子量Mn（数均分子）超过250的聚酯二醇优选超过 600，在约100℃至200℃之间，优选约110℃至180℃之间的温度下，用碳酸双芳基酯加热，真空度低于约35mmHg，优选约25mm 和1mm Hg，在催化剂的存在下，每摩尔聚酯二醇的OH基和所形成的羟基芳基化合物使用少于1摩尔的碳酸双芳基酯。本发明还涉及通过-OCOO-基团延长的聚酯二醇的双碳酸芳基酯。

34. 发明授权

US3941756A New water-insoluble preparations of peptide materials, their production and their use 失效
标题翻译：肽材料的新型水不溶性制剂，其生产及其用途
公开(公告)号：US3941756A
公开(公告)日：1976-03-02
申请号：US481225
申请日：1974-06-20
申请人： Fritz Huper , Erich Rauenbusch , Gunter Schmidt-Kastner , Bruno Bomer , Herbert Bartl
发明人： Fritz Huper , Erich Rauenbusch , Gunter Schmidt-Kastner , Bruno Bomer , Herbert Bartl
IPC分类号： C08F8/00 , C08F20/20 , C12N11/08 , C08F220/20 , C08F222/04
CPC分类号： C12N11/08 , C08F20/20 , C08F8/00
摘要： There are disclosed water-insoluble proteinic preparations in which a protein or polypeptide is bound to a copolymer, which preparations are useful for binding enzymes in order to carry out enzyme-catalyzable reactions. These preparations comprise a peptide material bound to a crosslinked copolymer comprising the following copolymerized units:A. about 0.1 to 30 wt. % of at least one .alpha.,.beta.-monoolefinically unsaturated dicarboxylic acid anhydride having about 4 to 9 carbon atoms;B. about 35 to 90 wt. % of at least one di- and/or poly(meth)acrylate of a diol and/or polyol as hereinafter defined; andC. about 5 to 60 wt. % of at least one hydrophilic monomer,The copolymer having a bulk volume of 1.4 to 30 ml/g and a specific surface area of about 1 to 500 m.sup.2 /g, and containing, after saponification of the anhydride groups, about 0.01 to 14 milliequivalents of acid per gram.
摘要翻译：公开了其中蛋白质或多肽与共聚物结合的水不溶性蛋白质制剂，该制剂可用于结合酶以进行酶促催化反应。这些制剂包含与包含以下共聚单元的交联共聚物结合的肽材料：

35. 发明授权

US5616529A Process for the preparation of branched low-pressure polyethylene, new low-pressure polyethylenes, and preformed bifunctional catalysts 失效
标题翻译：制备支链低压聚乙烯，新型低压聚乙烯和预制双功能催化剂的方法
公开(公告)号：US5616529A
公开(公告)日：1997-04-01
申请号：US607651
申请日：1996-02-27
申请人： Karl-Heinz A. Ostoja-Starzewski , Josef Witte , Herbert Bartl , Karl-Heinz Reichert , Georgios Vasiliou
发明人： Karl-Heinz A. Ostoja-Starzewski , Josef Witte , Herbert Bartl , Karl-Heinz Reichert , Georgios Vasiliou
IPC分类号： C08F4/78 , C08F4/00 , C08F4/02 , C08F4/22 , C08F4/24 , C08F4/60 , C08F4/72 , C08F4/80 , C08F8/00 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16 , C08F4/26 , C08F210/02
CPC分类号： C08F10/02 , C08F10/00 , C08F110/02 , C08F210/16
摘要： Branched low-pressure polyethylenes are prepared by oligomerization of ethylene on a nickel-containing catalyst and polymerization of the oligomers obtained, if appropriate in the presence of ethylene, on a chromium-containing catalyst.
摘要翻译：分支的低压聚乙烯是通过在含镍催化剂上乙烯低聚而制备的，如果合适的话，在含铬催化剂上聚合获得的低聚物。

36. 发明授权

US4620021A Organic nickel compounds, production and use thereof as catalysts in the polymerization of olefins 失效
标题翻译：有机镍化合物，其在烯烃聚合中的生产和用途作为催化剂
公开(公告)号：US4620021A
公开(公告)日：1986-10-28
申请号：US654227
申请日：1984-09-25
申请人： Karl-Heinz A. O. Starzewski , Josef Witte , Herbert Bartl
发明人： Karl-Heinz A. O. Starzewski , Josef Witte , Herbert Bartl
IPC分类号： C08L67/00 , C07F15/04 , C08F4/26 , C08F4/60 , C08F4/80 , C08F10/00 , C08J3/24 , C08L69/00
CPC分类号： C07F15/04 , C08F10/00
摘要： Olefins such as ethylene can be polymerized with a catalyst which comprises nickel compounds obtained by reacting a nickel-(O) compound or a nickel compound which may be converted in situ into a nickel-(O) compound with an adduct or a mixture of a quinoid compound and a tertiary phosphine and with a compound corresponding to the following general formula: ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 independently represent C.sub.1 -C.sub.20 alkyl, C.sub.2 -C.sub.20 alkenyl, C.sub.6 -C.sub.12 aryl or C.sub.3 -C.sub.8 cycloalkyl optionally substituted by halogen, hydroxy, C.sub.1 -C.sub.20 alkoxy, nitro or C.sub.6 -C.sub.12 aryloxy; also C.sub.6 -C.sub.12 aryl-C.sub.1 -C.sub.20 alkyl, C.sub.6 -C.sub.12 aryl-C.sub.2 -C.sub.20 alkenyl, C.sub.1 -C.sub.20 alkyl-C.sub.6 -C.sub.12 aryl, C.sub.1 -C.sub.20 alkyl-C.sub.3 -C.sub.8 cycloalkyl and C.sub.6 -C.sub.12 aryl-C.sub.3 -C.sub.8 cycloalkyl, di-C.sub.1 -C.sub.4 alkylamino, optionally substituted phenoxy or alkoxy; R.sup.4, R.sup.5 and R.sup.6 represent hydrogen, silyl, halogen, cyano or R.sup.1 andX represents O, NR.sub.4 or ##STR2##
摘要翻译：烯烃如乙烯可以与催化剂聚合，所述催化剂包括通过使镍 - （O）化合物或镍化合物原位转化成镍 - （O）化合物而获得的镍化合物与加合物或其混合物喹啉化合物和叔膦，并具有对应于下列通式的化合物：其中R 1，R 2和R 3独立地表示C 1 -C 20烷基，C 2 -C 20烯基，C 6 -C 12芳基或C 3 -C 8环烷基任选被卤素，羟基，C 1 -C 20烷氧基，硝基或C 6 -C 12芳氧基取代; 还有C 6 -C 12芳基-C 1 -C 20烷基，C 6 -C 12芳基-C 2 -C 20烯基，C 1 -C 20烷基-C 6 -C 12芳基，C 1 -C 20烷基-C 3 -C 8环烷基和C 6 -C 12芳基-C 3 -C 8环烷基，二-C 1 -C 4烷基氨基，任选取代的苯氧基或烷氧基; R4，R5和R6表示氢，甲硅烷基，卤素，氰基或R1，X表示O，NR4或

37. 发明授权

US4602056A Use of grafted ethylene-vinylacetate copolymers for the production of hotmelt adhesives 失效
标题翻译：使用接枝乙烯 - 乙酸乙烯酯共聚物来生产热熔胶
公开(公告)号：US4602056A
公开(公告)日：1986-07-22
申请号：US733239
申请日：1985-05-10
申请人： Helmut Waniczek , Gerhard Hohmann , Herbert Bartl , Ludwig Mott
发明人： Helmut Waniczek , Gerhard Hohmann , Herbert Bartl , Ludwig Mott
IPC分类号： C09J151/00 , C09J151/06 , C08L23/08 , C08L31/04 , C08L51/00
CPC分类号： C09J151/06 , Y10S525/904
摘要： The invention relates to the use of grafted ethylene-vinylacetate copolymers (EVA-copolymers) for the production of hotmelt adhesives.
摘要翻译：本发明涉及接枝乙烯 - 乙酸乙烯酯共聚物（EVA-共聚物）用于生产热熔粘合剂的用途。

38. 发明授权

US4506045A Cellulose ester-aliphatic polycarbonate thermoplastic moulding compositions 失效
标题翻译：纤维素酯 - 脂族聚碳酸酯热塑性成型组合物
公开(公告)号：US4506045A
公开(公告)日：1985-03-19
申请号：US532238
申请日：1983-09-14
申请人： Helmut Waniczek , Christian Lindner , Carlhans Suling , Herbert Bartl , Walter Uerdingen
发明人： Helmut Waniczek , Christian Lindner , Carlhans Suling , Herbert Bartl , Walter Uerdingen
IPC分类号： C08L1/10 , C08L69/00 , G02B1/04
CPC分类号： C08L1/10 , C08L69/00 , Y10S525/932
摘要： Thermoplastic moulding compositions consisting of from 1 to 99% by weight of at least one cellulose ester or cellulose mixed ester, from 99 to 1% by weight of an aliphatic polyester or polyether containing carbonate groups and, optionally, standard auxiliaries and additives.
摘要翻译：由1至99重量％的至少一种纤维素酯或纤维素混合酯，99至1重量％的含有碳酸酯基团的脂族聚酯或聚醚或任选的标准助剂和添加剂组成的热塑性模塑组合物。

39. 发明授权

US4347341A Process for the production of ethylene graft copolymers containing anhydride or carboxyl groups 失效
标题翻译：制备含有酸酐或羧基的乙烯接枝共聚物的方法
公开(公告)号：US4347341A
公开(公告)日：1982-08-31
申请号：US295642
申请日：1981-08-24
申请人： Herbert Bartl , Klaus Schuster
发明人： Herbert Bartl , Klaus Schuster
IPC分类号： C08F255/00 , C08F255/02 , C08F263/00 , C08F263/02 , C08F263/04
CPC分类号： C08F263/02 , C08F255/02
摘要： A process for the production of ethylene graft copolymers containing anhydride or carboxyl groups in homogeneous or heterogeneous phase in tert.-butanol or methylene chloride wherein (A) from 5 to 70% by weight of a monomer mixture of: (a) from 10 to 80% by weight of a vinyl ester of an aliphatic C.sub.1 -C.sub.18 -monocarboxylic acid; and (b) from 90 to 30% by weight of maleic acid anhydride and/or its C.sub.1 -C.sub.20 -alkyl semiesters; are radically polymerized in the presence of (B) from 95 to 30% by weight of an ethylene homopolymer or an ethylene/vinyl ester copolymer as the graft substrate.
摘要翻译：一种在叔丁醇或二氯甲烷中制备均相或非均相含有酸酐或羧基的乙烯接枝共聚物的方法，其中（A）5-70重量％的单体混合物：（a）10〜 80重量％的脂族C1-C18-一元羧酸的乙烯基酯; 和（b）90至30重量％的马来酸酐和/或其C 1 -C 20烷基半酯; 在（B）95〜30重量％的乙烯均聚物或乙烯/乙烯基酯共聚物作为接枝基材的存在下自由基聚合。

40. 发明授权

US4256636A Azo-di-isobutyric acid-(N,N-hydroxyalkyl)-amidines 失效
标题翻译：偶氮二异丁酸 - （N，N-羟烷基） - 脒
公开(公告)号：US4256636A
公开(公告)日：1981-03-17
申请号：US76235
申请日：1979-09-17
申请人： Ernst Roos , Herbert Bartl , Klaus Schuster , Adolf Schmidt
发明人： Ernst Roos , Herbert Bartl , Klaus Schuster , Adolf Schmidt
IPC分类号： C07C257/14 , C08F4/04 , C07C123/00
CPC分类号： C07C257/14 , C08F4/04
摘要： An azo di-isobutyric acid-(N,N'-hydroxyalkyl)-amidine corresponding to the formula (I): ##STR1## in which R and R', which may be the same or different, represent linear or branched alkylene radicals containing from 2 to 4 carbon atoms, andX represents R'-OH or H.They may be produced by reacting an azo-di-isobutyric acid iminoalkyl ether containing from 1 to 4 carbon atoms in the alkyl group with at least one mono-alkanolamine containing from 2 to 4 carbon atoms or with a mixture of at least one monoalkanolamine and at least one dialkanolamine each containing from 2 to 4 carbon atoms in an alkanol radical, the molar ratio of monoalkanolamines to dialkanolamines in the mixture amounting to substantially 1:1, in substantially equivalent quantitative ratios at a temperature in the range of from 0.degree. to 50.degree. C. The amidines may be used as polymerization initiators, as cross-linking agents and as blowing agents in the production of foams.
摘要翻译：对应于式（I）的偶氮二异丁酸 - （N，N'-羟基烷基） - 脒：其中R和R'可以相同或不同，表示直链或支链含有2至4个碳原子的亚烷基，X代表R'-OH或H.

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