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21. 发明授权

US5552008A Method for the preparation of high modulus carbon and graphite articles 失效
标题翻译：高模量碳和石墨制品的制备方法
公开(公告)号：US5552008A
公开(公告)日：1996-09-03
申请号：US355514
申请日：1994-12-14
申请人： Daniel H. Hecht , David A. Schulz
发明人： Daniel H. Hecht , David A. Schulz
IPC分类号： C01B31/04 , C04B35/52 , C04B35/83 , C04B38/00 , D01F9/12 , D01F9/14 , B65H81/00 , C01B31/00
CPC分类号： C04B35/83 , C04B2235/5252 , C04B2235/5268 , C04B2235/614 , C04B2235/77 , C04B2235/96 , C04B2235/9607 , Y10T428/30
摘要： Self-reinforcing, pitch-based carbon articles having an unique combination of excellent thermal conductivity and outstanding mechanical properties are produced by carbonizing acid-treated mesophase pitch fiber, preferably in the form of a preform structure. The carbon articles having varying degrees of porosity are particularly desirable for use in thermal management and stiffness applications, and in carbon vapor infiltration processes employed in making complex solid carbon articles.
摘要翻译：通过将酸处理的中间相沥青纤维碳化，优选以预成型结构的形式，生产具有优异导热性和优异机械性能的独特组合的自增强沥青基碳制品。具有不同程度孔隙率的碳制品特别适用于热管理和刚度应用以及用于制备复杂固体碳制品的碳蒸气渗透方法。

22. 发明授权

US5547363A Nozzle for spinning pitch-based carbon fibers 失效
标题翻译：用于纺丝沥青基碳纤维的喷嘴
公开(公告)号：US5547363A
公开(公告)日：1996-08-20
申请号：US462544
申请日：1995-06-05
申请人： Yasuyuki Takai , Tetsuo Yamada , Toshifumi Kawamura , Susumu Shimizu , Haruki Yamasaki
发明人： Yasuyuki Takai , Tetsuo Yamada , Toshifumi Kawamura , Susumu Shimizu , Haruki Yamasaki
IPC分类号： D01D4/00 , D01D4/02 , D01F9/14 , D01F9/32
CPC分类号： D01F9/322 , D01D4/02
摘要： Disclosed herein is a spinning nozzle having one or more discharge openings and one or more introduction openings located upstream the discharge openings for producing pitch-based carbon fibers characterized by the presence of one or more spiral members in each introduction openings. According to the nozzle of the present invention, part of the pitch which is introduced to the introduction opening flows down along the spiral member while the flow of the pitch is affected by the spiral member. The remaining pitch flows into the discharge opening without being in contact with the spiral member, and then both are spun after being mixed through the discharge opening to prepare carbon fibers having a random structure. Especially, the carbon fibers of higher performances can be prepared when a spiral having uneven outer diameters is employed.
摘要翻译：本文公开了一种纺丝喷嘴，其具有一个或多个排出口和位于排出口上游侧的一个或多个引入开口，用于生产沥青基碳纤维，其特征在于在每个导入开口中存在一个或多个螺旋构件。根据本发明的喷嘴，引入到引入口的间距的一部分沿着螺旋构件向下流动，而螺距的流动受螺旋构件的影响。剩余的沥青不与螺旋构件接触而流入排放口，然后在通过排出口混合后将其两者旋转以制备具有随机结构的碳纤维。特别地，当采用具有不均匀外径的螺旋时，可以制备更高性能的碳纤维。

23. 发明授权

US5389350A Gas separation using adsorbent activated carbonized polyarylamides 失效
标题翻译：使用吸附剂进行气体分离活性炭化聚芳酰胺
公开(公告)号：US5389350A
公开(公告)日：1995-02-14
申请号：US867686
申请日：1992-07-09
申请人： John J. Freeman , Frederick G. R. Gimblett , Robert A. Hayes , Kenneth S. W. Sing
发明人： John J. Freeman , Frederick G. R. Gimblett , Robert A. Hayes , Kenneth S. W. Sing
IPC分类号： B01D53/02 , B01D53/34 , B01D53/81 , B01J20/20 , C01B31/02 , C01B31/10 , D01F9/14 , D01F9/28 , D01F9/30 , C01B31/20 , C01B31/08 , C01C3/04
CPC分类号： D01F9/30
摘要： Novel polyarylamide derived activated carbon materials are provided by a process comprising the carbonization of polyarylamide fibre at a temperature in excess or 400.degree. C. followed by activation at elevated temperature. The novel materials have the ability to adsorb relatively large quantities or carbon dioxide compared to other activated carbonized polymer materials, Preferably the carbonization and activation steps are carried out by raising the temperature of the materials to between 840.degree. C. and 880.degree. C. in carbonizing/activating atmospheres respectively.
摘要翻译： PCT No.PCT / GB90 / 02008 Sec。 371日期：1992年7月9日 102（e）日期1992年7月9日PCT 1990年12月21日PCT PCT。 WO91 / 10000 PCT公开号日期：1991年7月11日。新型聚芳酰胺衍生的活性炭材料通过包括聚芳基酰胺纤维在过量或400℃的温度下碳化的方法提供，随后在升高的温度下活化。与其它活性碳化聚合物材料相比，新型材料具有吸附相对大量或二氧化碳的能力。优选地，碳化和活化步骤通过将材料的温度升高至840℃至880℃之间来进行碳化/活化气氛。

24. 发明授权

US5188893A Stabilized and carbonaceous expanded fibers 失效
标题翻译：稳定和碳纤维膨胀纤维
公开(公告)号：US5188893A
公开(公告)日：1993-02-23
申请号：US554778
申请日：1990-07-19
申请人： Kyung W. Suh , William G. Stobby , Francis P. McCullough
发明人： Kyung W. Suh , William G. Stobby , Francis P. McCullough
IPC分类号： D01F6/18 , D01F6/60 , D01F6/74 , D01F9/14 , D01F9/22 , D01F9/24 , D01F9/30 , D02G1/00
CPC分类号： D01F9/30 , D01F9/22 , D01F9/24 , Y10T428/2909 , Y10T428/2918 , Y10T428/2922 , Y10T428/2925 , Y10T428/2935 , Y10T428/2975
摘要： There is provided a non-flammable expanded fiber comprising carbonaceous polymeric substantially irreversibly heat set fiber having an LOI value of greater than 40, and the fibrous structures thereof. Also, provided are stabilized expanded polymeric fibers.

25. 发明授权

US5156831A Method for producing high strength, melt spun carbon fibers 失效
标题翻译：生产高强度熔融纺丝碳纤维的方法
公开(公告)号：US5156831A
公开(公告)日：1992-10-20
申请号：US34226
申请日：1987-04-02
申请人： Charles C. Fain , Danny D. Edie
发明人： Charles C. Fain , Danny D. Edie
IPC分类号： D01D5/253 , D01F9/14 , D01F9/155 , D01F9/22 , D01F9/32
CPC分类号： D01F9/32 , D01D5/253 , D01F9/14 , D01F9/155 , D01F9/22 , D01F9/322
摘要： Hollow carbon fibers and carbon fibers having a generally C-shaped transverse cross-sectional area are produced by extruding a carbonaceous anisotropic liquid precursor through a spinneret having a capillary with a generally C-shaped cross-sectional area, into a fiber filament, controlling the viscosity of the molten precursor, the pressure of the molten precursor and the linear take-up speed of the filament to yield a fiber filament having a cross-sectional area shaped substantially like the shape of the cross-sectional area of the capillary and further having a line-origin microstructure, rendering the filament infusible, heating the filament in an inert pre-carbonizing environment at a temperature in the range of 600.degree. C. to 1000.degree. C. for 1 to 5 minutes, and heating the filament in an inert carbonizing environment at a temperature in the range of 1550.degree. C. to 1600.degree. C. for 5 to 10 minutes, to substantially increase the tensile strength of the filament. The carbon fiber filament so produced has a line-origin microstructure in which the origin line is located and shaped substantially as a line which constitutes the line formed by uniformly collapsing the perimeter of the transverse cross-sectional area of the fiber filament upon itself. The carbon fiber filament has a tensile strength greater than 200 ksi and as high as the 700 to 800 ksi range, yet a modulus of elasticity on the order of 25-35 msi. The top to bottom outside diameter of the fiber's transverse cross-sectional area is on the order of 30 to 50 microns, and the wall thicknesses are on the order of 8 to 15 microns.
摘要翻译：通过将碳质各向异性液体前体通过具有大致C形横截面积的毛细管的喷丝头挤出到纤维丝中来制造具有大致C形横截面积的中空碳纤维和碳纤维，从而控制熔融前体的粘度，熔融前体的压力和丝的线性吸收速度，以产生纤维长丝，该纤维长丝的截面积基本上类似于毛细管的横截面积的形状，并且还具有线源微结构，使细丝不熔，在惰性预碳化环境中在600℃至1000℃的温度范围内加热丝，持续1至5分钟，并将惰性物质加热至惰性碳化环境在1550℃至1600℃的温度下进行5至10分钟，以显着提高长丝的拉伸强度。如此制造的碳纤维丝具有线状微结构，其中原点线基本上定位成线，该线构成通过将纤维丝的横截面积的周长均匀地折叠在其自身上而形成的线。碳纤维长丝的拉伸强度大于200ksi，高达700至800ksi的范围，弹性模量为25-35毫秒。纤维横向横截面积的顶部到底部的外径约为30至50微米，壁厚约为8至15微米。

26. 发明授权

US4983457A High strength, ultra high modulus carbon fiber 失效
标题翻译：高强度，超高模量碳纤维
公开(公告)号：US4983457A
公开(公告)日：1991-01-08
申请号：US484006
申请日：1990-02-22
申请人： Takashi Hino , Hiroyuki Kurodo , Kaoru Hirokawa
发明人： Takashi Hino , Hiroyuki Kurodo , Kaoru Hirokawa
IPC分类号： D01F9/14 , D01D4/06 , D01F9/145 , D01F9/32
CPC分类号： D01F9/322 , D01F9/145 , Y10T428/2918
摘要： A high strength, ultra high modulus carbon fiber is characterized by the presence of the (112) cross-lattice line and the resolution of the diffraction band into two distinct lines (100) and (101), which indicate the three-dimensional order of the crystallite of the fiber. It has an interlayer spacing (d.sub.002) of 3.371 to 3.40 .ANG.; a stack height (Lc.sub.002) of 150 to 500 .ANG.; and a layer size (La.sub.110) of 150 to 800 .ANG..

27. 发明授权

US4975263A Process for producing mesophase pitch-based carbon fibers 失效
标题翻译：生产中间相沥青基碳纤维的方法
公开(公告)号：US4975263A
公开(公告)日：1990-12-04
申请号：US303654
申请日：1989-01-30
申请人： Masatoshi Furuyama , Yasunori Sajiki , Takeshi Hamada , Tadao Tomioka
发明人： Masatoshi Furuyama , Yasunori Sajiki , Takeshi Hamada , Tadao Tomioka
IPC分类号： D01F9/14 , D01F9/145 , D01F9/15
CPC分类号： D01F9/145
摘要： A process for producing a carbon fiber by subjecting a pitch fiber, obtained by melt spinning a carbonaceous mesophase pitch, to stabilization, followed by a carbonization or graphitization treatment, wherein the stabilization is carried out under an oxidative atmosphere containing 0.1% to 40% by volume of NO.sub.2 and 4% to 40% by volume of H.sub.2 O at a temperature of from 100.degree. C. to 400.degree. C.
摘要翻译：通过将通过熔融纺丝含碳中间相沥青获得的沥青纤维进行稳定化，随后进行碳化或石墨化处理来制备碳纤维的方法，其中稳定化在含有0.1％至40％的氧化气氛下进行，体积的NO2和4〜40体积％的H 2 O在100〜400℃的温度下进行。

28. 发明授权

US4925604A Process for preparing a carbon fiber of high strength 失效
标题翻译：制备高强度碳纤维的方法
公开(公告)号：US4925604A
公开(公告)日：1990-05-15
申请号：US787428
申请日：1985-10-15
申请人： Takashi Ohsaki , Koichi Imai , Naomasa Miyahara
发明人： Takashi Ohsaki , Koichi Imai , Naomasa Miyahara
IPC分类号： D01F6/18 , D01F9/14 , D01F9/22
CPC分类号： D01F6/18 , D01F9/22
摘要： A carbon fiber of high strength is disclosed, each filament of which is substantially circular in its cross-section but which has circumferential ruggedness which extends in parallel to an axis of the filament to form pleats. The ruggedness has a depth of more than 0.1 .mu.m.The carbon fiber is prepared by extruding a spinning solution of an aqueous polyacrylonitrile/pure zinc chloride solution of a specified polymer content into a coagulating bath at a specified draft ratio, followed by washing, drying and stretching at a total stretching ratio of 10-20 folds to form a precursor which is then subjected to conventional stabilizing and carbonizing steps.
摘要翻译：公开了一种高强度的碳纤维，其每根细丝的横截面基本为圆形，但是具有平行于灯丝的轴线延伸的周向粗糙度以形成褶皱。崎岖深度超过0.1亩。碳纤维通过将特定聚合物含量的聚丙烯腈水溶液/纯氯化锌溶液的纺丝溶液以规定的吸气比挤出到凝固浴中，然后以10-20的总拉伸比进行洗涤，干燥和拉伸折叠形成前体，然后进行常规的稳定和碳化步骤。

29. 发明授权

US4900247A High-temperature heating furnace 失效
标题翻译：高温加热炉
公开(公告)号：US4900247A
公开(公告)日：1990-02-13
申请号：US343575
申请日：1989-04-27
申请人： Susumu Takahashi
发明人： Susumu Takahashi
IPC分类号： D02J13/00 , D01F9/133 , D01F9/14 , F27B9/06 , F27B9/08 , F27B9/32 , F27B9/34 , F27D1/00 , F27D1/14 , F27D99/00
CPC分类号： F27D99/0006 , F27B9/063 , F27B9/082 , F27B9/32 , F27B9/34 , F27D1/0006 , F27D1/145
摘要： In a high-temperature heating furnace, its central longitudinal passage in which articles to be heated are placed, and its inner support which makes a space between its inner surface and the above-mentioned passage for accommodating heaters therein and which makes also another space between its outer surface and a furnace shell for filling insulators therein, are both installed in the furnace by assembling a plurality of thin plates made of carbon fiber reinforced graphite or carbon compounds to cuboids which are coaxial to each other and have rectangular cross sections.
摘要翻译：在高温加热炉中，其中放置有待加热物品的中央纵向通道及其内部支撑件在其内表面和上述通道之间形成一个空间，用于在其中容纳加热器，并且还在其外表面和用于在其中填充绝缘体的炉壳均通过将由碳纤维增强石墨或碳化合物制成的多个薄板组装成彼此同轴且具有矩形横截面的立方体而安装在炉中。

30. 发明授权

US4895712A Process for producing carbon fiber and graphite fiber 失效
标题翻译：生产碳纤维和石墨纤维的方法
公开(公告)号：US4895712A
公开(公告)日：1990-01-23
申请号：US185110
申请日：1988-04-22
申请人： Kikuji Komine , Hisao Kato , Tsutomu Naito , Takashi Hino , Hiroyuki Kuroda
发明人： Kikuji Komine , Hisao Kato , Tsutomu Naito , Takashi Hino , Hiroyuki Kuroda
IPC分类号： D06M13/00 , D01F9/14 , D01F9/15 , D01F9/155 , D06M13/02 , D06M13/188 , D06M13/322 , D06M13/325 , D06M13/335 , D06M13/35 , D06M13/355 , D06M13/51 , D06M13/513 , D06M15/643 , D06M101/00 , D06M101/12 , D06M101/40
CPC分类号： D01F9/155 , D01F9/15
摘要： A process for producing carbon fiber or graphite fiber is provided. The process comprises spinning a carbonaceous pitch, doubling spun pitch fiber bundles, adding a heat resistant doubling treatment oil, passing the fiber bundles continuously and linearly through an oxygen rich gas, infusibilizing at a temperature of 350.degree. C. or less, then carbonizing or graphitizing infusibilized fiber bundles.

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