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21. 发明授权

US5569309A Disperse dye compositions 失效
标题翻译：分散染料组合物
公开(公告)号：US5569309A
公开(公告)日：1996-10-29
申请号：US444576
申请日：1995-05-19
申请人： Toshio Hihara , Kiyoshi Himeno
发明人： Toshio Hihara , Kiyoshi Himeno
IPC分类号： C09B29/00 , C09B67/00 , C09B67/10 , C09B67/22 , C09B29/033
CPC分类号： C09B67/0051 , C09B29/0059 , C09B67/0015 , C09B67/0028
摘要： A dye composition containing at least one turquoise blue monoazo dye of the formula (I): ##STR1## and at least one additional dye which is at least one yellow monoazo dye of the formula (II): ##STR2## or at least one blue anthraquinone dye of the formula (III): ##STR3## or at least one navy blue dye of the formula (IV): ##STR4##
摘要翻译：含有至少一种式（I）的青绿色蓝单偶氮染料：（I）和至少一种另外的染料是至少一种式（II）的黄色单偶氮染料的染料组合物：式（III）：（III）或至少一种式（IV）的海军蓝染料：

22. 发明授权

US5532344A Process for producing a monoazodye by diazo-coupling of a p-nitroanaline derivative with a N,N-substituted analine derivative 失效
标题翻译：通过对硝基苯胺衍生物与N，N-取代的分解衍生物的重氮偶合制备单偶极的方法
公开(公告)号：US5532344A
公开(公告)日：1996-07-02
申请号：US38813
申请日：1993-03-29
申请人： Kiyoshi Himeno , Toshio Hihara , Yoshiharu Hamano , Shinji Kubo
发明人： Kiyoshi Himeno , Toshio Hihara , Yoshiharu Hamano , Shinji Kubo
IPC分类号： C09B29/08 , C09B41/00 , C09B67/10 , C09B29/085
CPC分类号： C09B29/0813 , C09B29/0809 , C09B41/005 , C09B67/0015
摘要： A process for producing a monoazodye of the following formula (III): ##STR1## wherein X.sup.1 is nitro or halogen, X.sup.2 is halogen, R.sup.1 is lower alkoxy, R.sup.2 is lower alkyl, each of R.sup.3 and R.sup.4, which are independent of each other, is alkyl, cyanoalkyl or alkylcarbonyloxyalkyl, and each of m and n, which are independent of each other, is 0 or 1, which comprises diazotizing an aniline derivative of the following formula (I): ##STR2## wherein X.sup.1 and X.sup.2 are as defined above, followed by coupling with an aniline derivative of the following formula (II): ##STR3## wherein R.sup.1, R.sup.2, R.sup.3, R.sup.4, m and n are as defined above, wherein a reaction mixture obtained by the coupling reaction is heat-treated in the presence of a polyoxyethylene higher fatty acid ester type nonionic surfactant, followed by filtration to obtain said monoazo compound in the form of a cake.
摘要翻译：制备下式（III）的单偶氮的方法：其中X 1是硝基或卤素，X 2是卤素，R 1是低级烷氧基，R 2是低级烷基，R 3和R 4各自独立地是彼此是烷基，氰基烷基或烷基羰基氧基烷基，m和n彼此独立的各自为0或1，其包括将下式（I）的苯胺衍生物重氮化：其中X1和X2如上定义，然后与下式（II）的苯胺衍生物偶联：其中R 1，R 2，R 3，R 4，m和n如上所定义，其中反应通过偶联反应获得的混合物在聚氧乙烯高级脂肪酸酯型非离子表面活性剂的存在下进行热处理，然后过滤以获得饼状形式的所述单偶氮化合物。

23. 发明授权

US5527888A Thiophene-type monoazo dyes 失效
标题翻译：噻吩型单偶氮染料
公开(公告)号：US5527888A
公开(公告)日：1996-06-18
申请号：US399660
申请日：1995-03-07
申请人： Kiyoshi Himeno , Toshio Hihara , Ryouichi Sekioka
发明人： Kiyoshi Himeno , Toshio Hihara , Ryouichi Sekioka
IPC分类号： C09B29/00 , C09B29/08 , D06P3/54 , C09B29/033 , C09B29/09 , D06P3/36
CPC分类号： C09B29/0813 , C09B29/0088 , D06P3/54 , Y10S8/922
摘要： A monoazo dye of the following formula (I): ##STR1## wherein R is phenyl, phenoxy or benzyl, and D is a group of the formula (D1), (D2), (D3) or (D4): ##STR2## wherein each of X.sup.1, X.sup.2 and X.sup.3, which are independent of one another, is hydrogen or chlorine, X.sup.4 is hydrogen, chlorine, methyl or --NHCOR.sup.1, wherein R.sup.1 is C.sub.1-4 alkyl or phenyl; ##STR3## wherein X.sup.4 is as defined above, Y.sup.1 is hydrogen, chlorine or C.sub.1-4 alkoxy; ##STR4## wherein X.sup.5 is hydrogen, halogen, methyl or --NHZ, wherein Z is C.sub.1-4 alkylsulfonyl, C.sub.1-4 alkylcarbonyl, phenylsulfonyl, phenylcarbonyl, C.sub.1-2 alkoxy C.sub.1-2 alkylcarbonyl or aminocarbonyl, Y.sup.2 is hydrogen, methyl or C.sub.1-2 alkoxy, and Q.sup.1 is cyano or C.sub.1-4 alkylcarbonyl; ##STR5## wherein P is formyl, nitro or cyano, Q.sup.2 is cyano or nitro, T is halogen, methyl, phenyl or methylsulfonyl, X.sup.5 is as defined above, and Y.sup.3 is hydrogen or C.sub.1-2 alkoxy. The dyes of the formula (I) are useful for dyeing polyester fibers, particularly fine denier polyester fibers.
摘要翻译：下式（I）的单偶氮染料：其中R是苯基，苯氧基或苄基，D是式（D1），（D2），（D3）或（D4）的基团：（D1）其中X 1，X 2和X 3彼此独立地为氢或氯，X 4为氢，氯，甲基或-NHCOR 1，其中R 1为C 1-4烷基或苯基; （D2）其中X4如上所定义，Y 1是氢，氯或C 1-4烷氧基; （D3）其中X5是氢，卤素，甲基或-NHZ，其中Z是C1-4烷基磺酰基，C1-4烷基羰基，苯基磺酰基，苯基羰基，C1-2烷氧基C1-2烷基羰基或氨基羰基，Y2是氢，甲基或C 1-2烷氧基，Q 1为氰基或C 1-4烷基羰基; （D4）其中P是甲酰基，硝基或氰基，Q2是氰基或硝基，T是卤素，甲基，苯基或甲基磺酰基，X5如上所定义，Y 3是氢或C 1-2烷氧基。式（I）的染料可用于染色聚酯纤维，特别是细旦尼尔聚酯纤维。

24. 发明授权

US5494493A Disperse dye mixture 失效
标题翻译：分散染料混合物
公开(公告)号：US5494493A
公开(公告)日：1996-02-27
申请号：US346187
申请日：1994-11-22
申请人： Kiyoshi Himeno , Toshio Hihara
发明人： Kiyoshi Himeno , Toshio Hihara
IPC分类号： C09B67/22 , D06P1/18
CPC分类号： C09B67/0051 , D06P1/18 , Y10S8/922
摘要： A disperse dye mixture comprising dye (I) and dye (II) blended at a ratio of from 0.1 to 10 times by weight of dye (II) to dye (I): ##STR1## wherein X is halogen, nitro, cyano, thiocyanate, methylsulfonyl, C.sub.1 or C.sub.2 alkylcarbonyl, C.sub.1 -C.sub.4 alkoxycarbonyl or vinylsulfonyl, Y is hydrogen, halogen, cyano, trifluoromethyl or methylsulfonyl, W is hydrogen, halogen, C.sub.1 or C.sub.2 alkyl or C.sub.1 or C.sub.2 alkoxy, and each of R.sup.1 and R.sup.2 which are independent of each other, is hydrogen, C.sub.1 --C.sub.8 alkyl, or C.sub.2 -C.sub.4 alkyl substituted by halogen, hydroxyl, cyano, alkoxy, alkoxyalkoxy, a hydroxyalkoxy, hydroxyalkoxyalkoxy, acyloxyalkoxy or acyloxyalkoxyalkoxy, provided that each alkoxy has from 1 to 4 carbon atoms.
摘要翻译：一种分散染料混合物，其包含染料（II）与染料（I）的重量比为0.1-10倍的染料（I）和染料（II）：其中（I） X是卤素，硝基，氰基，硫氰酸酯，甲基磺酰基，C1或C2烷基羰基，C1-C4烷氧基羰基或乙烯基磺酰基，Y是氢，卤素，氰基，三氟甲基或甲磺酰基，W是氢，卤素，C1或C2烷基或C1或C2 烷氧基，卤素，羟基，氰基，烷氧基，烷氧基烷氧基，羟基烷氧基，羟基烷氧基烷氧基，酰氧基烷氧基或酰氧基烷氧基烷氧基取代的C 1 -C 8烷基或C 2 -C 4烷基，条件是每个烷氧基具有1至4个碳原子。

25. 发明授权

US4507476A Anthraquinone dyestuffs for cellulose-containing fibers 失效
标题翻译：蒽醌染料用于含纤维素纤维
公开(公告)号：US4507476A
公开(公告)日：1985-03-26
申请号：US568340
申请日：1984-01-05
申请人： Toshio Niwa , Kiyoshi Himeno , Toshio Hihara
发明人： Toshio Niwa , Kiyoshi Himeno , Toshio Hihara
IPC分类号： C09B1/32 , C09B1/503 , C09B1/514 , C09B1/52 , C09B1/54 , C09B1/56 , C09B1/58 , C07D251/42 , C07D251/48
CPC分类号： C09B1/32 , C09B1/503 , C09B1/514 , C09B1/547 , C09B1/585
摘要： This invention relates to an anthraquinone dyestuff for cellulose containing fibers represented by the formula: ##STR1## wherein R.sup.1 represents amino or hydroxyl, R.sup.2 represents hydrogen, chlorine, bromine, cyano or --SO.sub.2 R wherein R represents methyl, ethyl or phenyl, R.sup.3 and R.sup.4 each represents hydrogen, amino, hydroxyl, nitro, chlorine or bromine, Y represents a connecting group consisting of --O-- or --S--, one of X.sup.1 and X.sup.2 is hydrogen and the other is a group of the formula: ##STR2## wherein --Z-- represents a connecting group consisting of --O-- or --S--, --W.sup.1 represents phenyl or --NR.sup.6 R.sup.7, R.sup.5 represents hydrogen, methyl, ethyl, methoxy, ethoxy, chlorine or bromine, R.sup.6 and R.sup.7 each represents hydrogen or alkyl, alkenyl, cyclohexyl, aryl or aralkyl which may optionally be substituted by lower alkoxy, or NR.sup.6 R.sup.7 represents a 5-membered or 6-membered nitrogen-containing heterocyclic ring formed by combination of R.sup.6 and R.sup.7, and n is 0 or 1, with the proviso that where X.sup.2 is hydrogen, n is 0.
摘要翻译：本发明涉及由下式表示的含纤维素的纤维素染料：其中R1表示氨基或羟基，R2表示氢，氯，溴，氰基或-SO2R，其中R表示甲基，乙基或苯基，R3和R4 各自表示氢，氨基，羟基，硝基，氯或溴，Y表示由-O-或-S-组成的连接基团，X1和X2之一为氢，另一个为下式基团：其中 -Z-表示由-O-或-S-组成的连接基团，-W1表示苯基或-NR6R7，R5表示氢，甲基，乙基，甲氧基，乙氧基，氯或溴，R6和R7各自表示氢或烷基，烯基，环己基，芳基或芳烷基，其可任选被低级烷氧基取代，或NR 6 R 7表示通过R6和R7的组合形成的5元或6元含氮杂环，n为0或1，条件是其中X2是氢，n是0。

26. 发明授权

US4436906A Anthraquinone dyes for cellulose-containing fibers and process for producing the same 失效
标题翻译：用于含纤维素纤维的蒽醌染料及其制备方法
公开(公告)号：US4436906A
公开(公告)日：1984-03-13
申请号：US380320
申请日：1982-05-20
申请人： Toshio Niwa , Toshio Hihara
发明人： Toshio Niwa , Toshio Hihara
IPC分类号： C09B1/32 , C09B1/54 , C09B1/58 , C09B62/06 , D06P3/60 , D06P3/66 , C07D251/42
CPC分类号： C09B1/547 , C09B1/32 , C09B1/585 , C09B62/06 , D06P3/6041 , D06P3/66
摘要： An anthraquinone dye for cellulose-containing fibers having the formula (I) indicated below and a process for producing the same are disclosed: ##STR1## wherein R.sup.1 is an amino group or a hydroxyl group; R.sup.2 is a hydrogen atom, a chlorine atom, a bromine atom, a cyano group or --SO.sub.2 R (wherein R is a lower alkyl group or a phenyl group); R.sup.3 and R.sup.4 are each a hydrogen atom, an amino group, a hydroxyl group, a nitro group, a chlorine atom or a bromine atom; Y is a bonding group --O-- or --S--; one of X.sup.1 and X.sup.2 is a hydrogen atom and the other is ##STR2## (wherein Z is a bonding group --O-- or --S--; R.sup.5 is a lower alkyl group, a lower alkoxy group or a hydrogen atom; R.sup.6 and R.sup.7 are each a hydrogen atom or an alkyl group, an alkenyl group, a cyanohexyl group, an aryl group or an aralkyl group which may be substituted by a cyano group, a hydroxyl group, a lower alkoxy group or a dialkylamino group, or NR.sup.6 R.sup.7 represents a 5- or 6-membered nitrogen-containing heterocyclic ring formed by the bonding of R.sup.6 and R.sup.7 ; the sum of the carbon atoms of R.sup.6 and R.sup.7 is not more than 18); and n is 0 or 1, but n is 0 when X.sup.2 is a hydrogen atom.
摘要翻译：公开了下述的具有式（I）的含纤维素纤维的蒽醌染料及其制备方法：其中R1是氨基或羟基;（I）其中R1是氨基或羟基; R2是氢原子，氯原子，溴原子，氰基或-SO2R（其中R是低级烷基或苯基）; R3和R4各自为氢原子，氨基，羟基，硝基，氯原子或溴原子; Y是键合基团-O-或-S-; X1和X2之一是氢原子，另一个是（其中Z是键合基-O-或-S-; R5是低级烷基，低级烷氧基或氢原子; R6和R7 羟基，低级烷氧基或二烷基氨基可被取代的氢原子或烷基，烯基，氰基己基，芳基或芳烷基，NR 6 R 7表示通过键合R6和R7形成的5-或6-元含氮杂环; R6和R7的碳原子之和不大于18）; 且n为0或1，但当X2为氢原子时，n为0。

27. 发明授权

US4276047A Anthraquinone reactive dyes for cellulose-containing fibers 失效
标题翻译：用于含纤维素纤维的蒽醌活性染料
公开(公告)号：US4276047A
公开(公告)日：1981-06-30
申请号：US141375
申请日：1980-04-18
申请人： Seiichi Imahori , Toshio Hihara , Tomio Yomeyama , Takao Hirota
发明人： Seiichi Imahori , Toshio Hihara , Tomio Yomeyama , Takao Hirota
IPC分类号： C09B62/06 , D06P1/382 , D06P3/60 , D06P3/66 , D06P3/82
CPC分类号： D06P1/382 , C09B62/06 , D06P3/6041 , D06P3/8233 , Y10S8/918 , Y10S8/922
摘要： An anthraquinone dye for direct printing and pad dyeing of cellulose-containing fibers and of the formula: ##STR1## wherein A represents a phenylene group, Y represents a group --NH-- or --C.sub.2 H.sub.4 O--, X represents a carbamoyl group which may be substituted with a lower alkyl group or a lower alkoxy-lower alkyl group, a sulfamoyl group which may be substituted with a lower alkyl group or a lower alkoxy-lower alkyl group, a halogen atom or a cyano group, and Z represents an amino group, a mono- or di-alkylamino group having 1-6 carbon atoms in total, an anilino group, a lower alkoxy group or a group --O(R.sup.1 O).sub.n -R.sup.2 in which R.sup.1 represents an ethylene group or a propylene group, R.sup.2 represents a methyl group or an ethyl group and n is an integer of 1-5.
摘要翻译：一种用于直链印染和含纤维素纤维的垫染色的蒽醌染料，其分子式如下：其中A表示亚苯基，Y表示基团-NH-或-C2H4O-，X表示可被取代的氨基甲酰基低级烷基或低级烷氧基 - 低级烷基，可被低级烷基或低级烷氧基 - 低级烷基，卤素原子或氰基取代的氨磺酰基，Z表示氨基，总共1-6个碳原子的单 - 或二 - 烷基氨基，苯胺基，低级烷氧基或基团-O（R 1 O）n -R 2，其中R 1表示亚乙基或亚丙基，R 2表示甲基或乙基，n为1-5的整数。

28. 发明申请

US20050272920A1 Yellow disperse dye mixture which has a high level of light fastness 有权
标题翻译：具有高耐光性的黄色分散染料混合物
公开(公告)号：US20050272920A1
公开(公告)日：2005-12-08
申请号：US10523656
申请日：2003-08-02
申请人： Toshio Hihara , Hiroshi Inoue , Wataru Seto
发明人： Toshio Hihara , Hiroshi Inoue , Wataru Seto
IPC分类号： C09B67/22 , D06P1/16 , D06P1/18 , D06P1/20 , D06P3/54 , D06P3/82
CPC分类号： D06P1/18 , C09B67/0041 , D06P1/16 , D06P1/20 , D06P3/54 , Y10S8/922
摘要： The present inventions refers to a dye mixture comprising from 25 to 80% by weight with respect to the total dyestuff fraction of the yellow dyestuff represented by the structural formula [1] and from 75 to 20% by weight with respect to the total dyestuff fraction of a yellow dyestuff represented by the structural formula [2] wherein R denotes a C1 to C4 hydroxyalkyl group.
摘要翻译：本发明是指相对于由结构式[1]表示的黄色染料的总染料份数和相对于总染料份数为75〜20重量％的25〜80重量％的染料混合物的由结构式[2]表示的黄色染料，其中R表示C 1至C 4羟烷基。

29. 发明授权

US06388057B1 Crystalline modification of a water-insoluble monoazo dye 失效
标题翻译：水不溶性单偶氮染料的结晶改性
公开(公告)号：US06388057B1
公开(公告)日：2002-05-14
申请号：US09869672
申请日：2001-08-31
申请人： Toshio Hihara , Hiroshi Inoue , Yousuke Takahashi
发明人： Toshio Hihara , Hiroshi Inoue , Yousuke Takahashi
IPC分类号： C09B6748
CPC分类号： C09B67/0015 , C09B67/0029 , Y10S8/922
摘要： A water-insoluble monoazo dye represented by the following structural formula [I] having a crystal modification characterized by an X-ray diffraction pattern (CuK&agr;) showing one strong peak at a diffraction angle (2&thgr;) of 11.1±0.1° and also four intermediate peaks at 8.1±0.1°, 21.8±0.1°, 23.1±0.1° and 25.2±0.1°.
摘要翻译：具有以衍射角（2θ）为11.1±0.1°的一个强峰的X射线衍射图（CuKalpha）为特征的结晶改性的下述结构式[I]表示的水不溶性单偶氮染料，以及四个中间体峰位于8.1±0.1°，21.8±0.1°，23.1±0.1°和25.2±0.1°。

30. 发明授权

US5744588A Blue type disperse dye mixture and process for its preparation 失效
标题翻译：蓝色分散染料混合物及其制备方法
公开(公告)号：US5744588A
公开(公告)日：1998-04-28
申请号：US729027
申请日：1996-10-09
申请人： Kiyoshi Himeno , Toshio Hihara , Yousuke Takahashi
发明人： Kiyoshi Himeno , Toshio Hihara , Yousuke Takahashi
IPC分类号： C09B67/22 , C09B41/00
CPC分类号： C09B67/0051 , Y10S534/01 , Y10S8/922
摘要： A blue type disperse dye mixture comprising 1.0 part by weight of at least one dye of the formula (1), from 0 to 0.2 part by weight of at least one dye of the formula (2), from 0.05 to 1.0 part by weight of at least one dye of the formula (3) and from 0.05 to 1.0 part by weight of at least one dye of the formula (4): ##STR1## wherein X is a chlorine atom or a bromine atom, R.sup.1 is a C.sub.1-5 alkyl group, R.sup.2 is a C.sub.1-4 alkyl group, and R.sup.3 is a C.sub.1-5 alkyl group or an allyl group, provided that R.sup.1, R.sup.2 and R.sup.3 may, respectively, be the same or different among the formulae (1) to (4).
摘要翻译：一种蓝色分散染料混合物，其包含1.0重量份的至少一种式（1）的染料，0至0.2重量份的至少一种式（2）的染料，0.05至1.0重量份的式至少一种式（3）的染料和0.05至1.0重量份的至少一种式（4）的染料：（1）（2）原子或溴原子，R 1 是C1-5烷基，R2是C1-4烷基，R3是C1-5烷基或烯丙基，条件是R1，R2和R3可以分别相同或不同，在式（1）〜（4）。

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