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21. 发明授权

US4526726A Tertiaryalkyl peroxycarbonates 失效
标题翻译：过碳酸三烷基酯
公开(公告)号：US4526726A
公开(公告)日：1985-07-02
申请号：US430051
申请日：1982-09-30
申请人： Robert H. Tang
发明人： Robert H. Tang
IPC分类号： C07C409/38 , C07C409/40 , C08F299/04 , C07C179/18
CPC分类号： C07C409/40 , C08F299/045
摘要： Described are organic peroxycarbonates of the graphic formula: ##STR1## in which R.sub.1 is a C.sub.1 -C.sub.14 alkyl, phenyl or benzyl group, R.sub.2 and R.sub.3 are each selected from the group C.sub.1 -C.sub.4 alkyl, C.sub.5 -C.sub.7 cycloalkyl, C.sub.1 -C.sub.4 alkyl substituted C.sub.5 -.sub.7 cycloalkyl or participate in a cycloalkyl group of from 5 to 7 carbon atoms, provided that when one of R.sub.2 and R.sub.3 is a cycloalkyl group, the other is an alkyl group, A is cyano or alkoxycarbonyl, i.e., ##STR2## wherein R is a C.sub.1 -C.sub.8 alkyl or cyclohexyl group. Preferably R.sub.2 and R.sub.3 are each a C.sub.1 -C.sub.2 alkyl group or participate to form a cyclohexyl group, R.sub.1 is a C.sub.1 -C.sub.3 alkyl or phenyl and R is a C.sub.1 -C.sub.4 alkyl.The compounds can be used as initiators for the polymerization and copolymerization of ethylenically unsaturated monomers. The compounds also find application in connection with the curing of polyester resins and the vulcanization of silicone rubbers, e.g., hot air vulcanization.
摘要翻译：描述的是下式的有机过碳酸酯：其中R 1是C 1 -C 14烷基，苯基或苄基，R 2和R 3各自选自C 1 -C 4烷基，C 5 -C 7环烷基，C 1 -C 4烷基取代的C 5-7环烷基或参与5至7个碳原子的环烷基，条件是当R 2和R 3之一为环烷基时，另一个为烷基，A为氰基或烷氧基羰基，即，其中R是C1-C8烷基或环己基。 R2和R3优选为C1-C2烷基或参与形成环己基，R1为C1-C3烷基或苯基，R为C1-C4烷基。这些化合物可以用作烯属不饱和单体的聚合和共聚的引发剂。该化合物还可用于聚酯树脂的固化和硅橡胶的硫化，例如热空气硫化。

22. 发明授权

US09128343B2 Method of making an optical element having an electrochromic apodized aperture 有权
标题翻译：制造具有电致变色孔径的光学元件的方法
公开(公告)号：US09128343B2
公开(公告)日：2015-09-08
申请号：US13587284
申请日：2012-08-16
申请人： Forrest R. Blackburn , Jonathan Bork , John A. Charny , Stefan C. Dehaseth , Peter C. Foller , Andrew J. Lamb , Kevin W. Seybert , Michael A. Steimle , Robert H. Tang , Robert W. Walters
发明人： Forrest R. Blackburn , Jonathan Bork , John A. Charny , Stefan C. Dehaseth , Peter C. Foller , Andrew J. Lamb , Kevin W. Seybert , Michael A. Steimle , Robert H. Tang , Robert W. Walters
IPC分类号： G02F1/00 , G02F1/153 , G02B5/00 , G03B9/02 , G02B27/58 , B29D11/00
CPC分类号： G02F1/153 , B29D11/0074 , G02B5/005 , G02B27/58 , G03B9/02
摘要： A method of forming an optical element which includes an electrochromic apodized aperture having variable light transmittance through a clear aperture area in response to an applied electrical current is disclosed. The apodized aperture includes a body including an area defining the clear aperture area wherein a fluid containment area substantially overlapping the clear aperture area, and includes at least one fill passage extending from the fluid containment area to at least one fill port outside of the clear aperture area; an electrochromic fluid within the fluid containment area substantially overlapping the clear aperture area and having variable light transmittance in response to an applied electrical current; a cover attached with the electrochromic fluid between the cover and body; electrical contacts electrically coupled to the electrochromic fluid for supplying electrical current thereto; and at least one passage seal in each said fill passage positioned outside of the clear aperture area.
摘要翻译：公开了一种形成光学元件的方法，该光学元件包括响应于施加的电流通过透明孔径区域具有可变透光率的电致变色孔径。变迹孔包括主体，其包括限定透明孔径区域的区域，其中流体容纳区域基本上与透明孔径区域重叠，并且包括至少一个从流体容纳区域延伸到至少一个填充端口的填充通道，区; 所述液体容纳区域内的电致变色液体基本上与所述透明孔径区域重叠并且响应于施加的电流具有可变的透光率; 盖子和主体之间附着有电致变色流体的盖子; 电接触电耦合到电致变色流体以供应电流的电接触; 并且每个所述填充通道中的至少一个通道密封件位于透光孔区域的外部。

23. 发明申请

US20100134866A1 OPTICAL ELEMENT HAVING AN APODIZED APERTURE 有权
标题翻译：具有APODEDED APERTURE的光学元件
公开(公告)号：US20100134866A1
公开(公告)日：2010-06-03
申请号：US12629521
申请日：2009-12-02
申请人： Peter C. Foller , Robert H. Tang , Forrest R. Blackburn , Robert W. Walters , Kevin W. Seybert
发明人： Peter C. Foller , Robert H. Tang , Forrest R. Blackburn , Robert W. Walters , Kevin W. Seybert
IPC分类号： G02F1/153 , G02F1/161
CPC分类号： G02F1/163 , G02F1/1533 , G02F1/155 , G02F2001/291 , G03B9/02
摘要： Provided is an optical element with an electrochromic apodized aperture having variable light transmittance in response to the amplitude of an applied voltage. The apodized aperture includes (i) a first substrate having a planar inner surface and an outer surface, (ii) a second substrate having an outer surface and a non-planar inner surface opposing and spaced from the planar inner surface of the first substrate, wherein each of the planar inner surface of the first substrate and the non-planar inner surface of the second substrate has an at least partial layer of transparent conductive material thereover; and (iii) an electrochromic medium disposed between the planar inner surface of the first substrate and the non-planar inner surface of the second substrate.
摘要翻译：提供了具有电致变色孔径的光学元件，其响应于施加电压的幅度而具有可变的透光率。变迹孔包括（i）具有平面内表面和外表面的第一衬底，（ii）具有与第一衬底的平面内表面相对并间隔开的外表面和非平面内表面的第二衬底，其中所述第一基板的所述平面内表面和所述第二基板的所述非平面内表面中的每一个在其上具有至少部分透明导电材料层; 和（iii）设置在第一基板的平面内表面和第二基板的非平面内表面之间的电致变色介质。

24. 发明授权

US5900133A Method of converting amine hydrohalide into free amine 失效
标题翻译：将胺氢卤化物转化为游离胺的方法
公开(公告)号：US5900133A
公开(公告)日：1999-05-04
申请号：US914600
申请日：1997-08-18
申请人： Peter C. Foller , David G. Roberts , Robert H. Tang , James R. Franks
发明人： Peter C. Foller , David G. Roberts , Robert H. Tang , James R. Franks
IPC分类号： B01D61/44 , C25B3/00 , C25B1/00 , C25B7/00 , C25B15/00
CPC分类号： C25B3/00 , B01D61/44
摘要： Describes a method of electrochemically converting amine hydrohalide, e.g., ethyleneamine hydrochloride, into free amine, e.g., free ethyleneamine. A three compartment electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and anion exchange membrane, (2) an anolyte compartment containing an anode assembly comprising an anode and a cation exchange membrane, and (3) an intermediate compartment separated from the catholyte and anolyte compartments by the anion and cation exchange membranes respectively. An aqueous solution of amine hydrohalide is charged to the catholyte compartment, while hydrogen halide solutions are charged to the intermediate and anolyte compartments. Direct current is passed through the electrolytic cell and an aqueous solution comprising free amine is removed from the catholyte compartment.
摘要翻译：描述了将胺氢卤化物（例如乙烯胺盐酸盐）电化学转化成游离胺，例如游离亚乙基胺的方法。提供一种三室电解池，其具有（1）阴极电解室，其包含阴极组件和阴离子交换膜;（2）阳极室，其包含阳极和阳离子交换膜;以及（3）中间室分别通过阴离子和阳离子交换膜与阴极电解液和阳极电解质隔室分离。将胺氢卤化物的水溶液加入到阴极电解液室中，同时将卤化氢溶液装入中间体和阳极电解液室。直流电流通过电解槽，并从阴极电解液隔室除去包含游离胺的水溶液。

25. 发明授权

US4686266A Bis(allyl carbonate) monomer and method for polymerizing same 失效
标题翻译：双（碳酸烯丙酯）单体及其聚合方法
公开(公告)号：US4686266A
公开(公告)日：1987-08-11
申请号：US858316
申请日：1986-05-01
申请人： Robert H. Tang
发明人： Robert H. Tang
IPC分类号： C08F18/24 , C08F110/00
CPC分类号： C08F18/24
摘要： Fully cured, intact, solid castings of bis(allyl carbonate) resin, e.g., diethylene glycol bis(allyl carbonate), are prepared by polymerizing the resin with between about 0.75 and about 1.50 parts, per hundred parts of resin, of a monoperoxycarbonate, e.g., tertiarybutylperoxy isopropyl carbonate. An adhesion reducing amount, e.g., between about 25 and about 75 parts, per million parts of resin, of a mold release agent is incorporated into the liquid resin monomer to avoid cracking of the casting. Use of a mold release agent is not required when the resin is prepolymerized to about 15-20 percent allylic utilization.
摘要翻译：通过将树脂与每100份树脂的单过氧碳酸酯的约0.75至约1.50份聚合制备双（烯丙基碳酸酯）树脂的完全固化，完整的固体铸件，例如二甘醇双（碳酸烯丙酯）例如叔丁基过氧化异丙基碳酸酯。将每百万份树脂的脱模剂的粘合降低量例如约25至约75份加入到液态树脂单体中以避免铸件破裂。当树脂预聚合至约15-20％的烯丙基利用时，不需要使用脱模剂。

26. 发明授权

US4590008A Novel organic peroxydicarbonates 失效
标题翻译：新型有机过氧化二碳酸酯
公开(公告)号：US4590008A
公开(公告)日：1986-05-20
申请号：US618273
申请日：1984-06-07
申请人： Robert H. Tang , John C. Crano
发明人： Robert H. Tang , John C. Crano
IPC分类号： C07C409/34 , C08F4/34 , C07C69/003
CPC分类号： C08F4/34 , C07C409/32
摘要： Organic peroxydicarbonates such as bis[3-(isobutyryloxy)-2,2,4-trimethylpentyl] peroxydicarbonate are described. The peroxydicarbonates are useful as initiators for the polymerization or copolymerization of vinyl acetate and may be used in combination with the more commonly used peroxydicarbonates such as diisopropyl peroxydicarbonate.
摘要翻译：描述了有机过氧化二碳酸酯如双[3-（异丁酰氧基）-2,2,4-三甲基戊基]过氧化二碳酸酯。过氧二碳酸酯可用作乙酸乙烯酯的聚合或共聚的引发剂，并且可以与更常用的过氧化二碳酸酯如过氧化二碳酸二异丙酯组合使用。

27. 发明授权

US4492656A Dicyanomethyl ethyl peroxy dicarbonate polymerization initiators 失效
标题翻译：二氰甲基乙基过氧化二碳酸酯聚合引发剂
公开(公告)号：US4492656A
公开(公告)日：1985-01-08
申请号：US430167
申请日：1982-09-30
申请人： Robert H. Tang
发明人： Robert H. Tang
IPC分类号： C07C409/40 , C08F299/04 , C07C179/20
CPC分类号： C07C255/00 , C07C409/40 , C08F299/0457 , C07C2101/14
摘要： Organic peroxydicarbonates represented by the following graphic formula are described. ##STR1## In the formula, R and R' are each selected from an alkyl group containing from 1 to 4 carbon atoms, a cycloalkyl group of from 5 to 7 carbon atoms, a C.sub.1 -C.sub.4 alkyl substituted cycloalkyl group, or participate in a cycloalkyl group having from 5 to 7 carbon atoms, provided that when one of R and R' is cycloalkyl, the other is alkyl. The peroxydicarbonates are useful as initiators for the polymerization or copolymerization of ethylenically unsaturated monomers or the cross-linking of unsaturated polyester resins. The organic peroxydicarbonates can be used in combination with commercially available peroxydicarbonates, particularly those having a shorter half-life.
摘要翻译：描述由以下图形公式表示的有机过氧化二碳酸酯。在该式中，R和R'各自选自含有1至4个碳原子的烷基，5至7个碳原子的环烷基，C 1 -C 4烷基取代的环烷基，或者参与具有5至7个碳原子的环烷基，条件是当R和R'中的一个是环烷基时，另一个是烷基。过氧二碳酸酯可用作烯属不饱和单体的聚合或共聚的引发剂或不饱和聚酯树脂的交联。有机过氧碳酸氢盐可以与市售的过氧化二碳酸酯组合使用，特别是半衰期较短的那些。

28. 发明申请

US20130215489A1 OPTICAL ELEMENT HAVING AN ELECTROCHROMIC APODIZED APERTURE AND AN APERTURE BODY FORMING AN ELECTROCHROMIC APODIZED APERTURE 审中-公开
标题翻译：具有电致变色光孔的光学元件和形成电致变色光孔的光孔体
公开(公告)号：US20130215489A1
公开(公告)日：2013-08-22
申请号：US13587218
申请日：2012-08-16
申请人： Forrest R. Blackburn , Jonathan Bork , John A. Charny , Stefan C. Dehaseth , Peter C. Foller , Andrew J. Lamb , Kevin W. Seybert , Michael A. Steimle , Robert H. Tang , Robert W. Walters
发明人： Forrest R. Blackburn , Jonathan Bork , John A. Charny , Stefan C. Dehaseth , Peter C. Foller , Andrew J. Lamb , Kevin W. Seybert , Michael A. Steimle , Robert H. Tang , Robert W. Walters
IPC分类号： G02F1/153
CPC分类号： G02F1/153 , B29D11/0074 , G02B5/005 , G02B27/58 , G03B9/02
摘要： An optical element includes an electrochromic apodized aperture having variable light transmittance through a clear aperture area in response to an applied electrical current. The apodized aperture includes an aperture body including an area defining the clear aperture area, the body having a fluid containment area substantially overlapping the clear aperture area, and includes at least one fill passage extending from the fluid containment area to at least one fill port outside of the clear aperture area; an electrochromic fluid within the fluid containment area substantially overlapping the clear aperture area and having variable light transmittance in response to an applied electrical current; a cover attached with the electrochromic fluid between the cover and body; electrical contacts electrically coupled to the electrochromic fluid for supplying electrical current thereto; and at least one passage seal in each said fill passage positioned outside of the clear aperture area.
摘要翻译：光学元件包括电致变色孔径，其响应于施加的电流通过透明孔径区域具有可变的透光率。变迹孔包括孔体，该孔体包括限定清洁孔径区域的区域，该主体具有基本上与透明孔径区域重叠的流体容纳区域，并且包括从流体容纳区域延伸至至少一个填充口外部的至少一个填充通道的清晰开口面积; 所述液体容纳区域内的电致变色液体基本上与所述透明孔径区域重叠并且响应于施加的电流具有可变的透光率; 盖子和主体之间附着有电致变色流体的盖子; 电接触电耦合到电致变色流体以供应电流的电接触; 并且每个所述填充通道中的至少一个通道密封件位于透光孔区域的外部。

29. 发明授权

US5904829A Method of converting amine hydrohalide into free amine 失效
标题翻译：将胺氢卤化物转化为游离胺的方法
公开(公告)号：US5904829A
公开(公告)日：1999-05-18
申请号：US914601
申请日：1997-08-18
申请人： Peter C. Foller , David G. Roberts , Robert H. Tang
发明人： Peter C. Foller , David G. Roberts , Robert H. Tang
IPC分类号： B01D61/44 , C07C209/68 , C25B3/00 , C25B1/00 , C25B7/00 , C25B9/00
CPC分类号： B01D61/445 , C07C209/68 , C25B3/00
摘要： Describes a method of electreochemically converting amine hydrohalide, e.g., amine hydrochloride, into free amine, e.g., free ethyleneamine. An electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and a bipolar ion exchange membrane, (2) an anode compartment containing an anode assembly comprising either (a) a hydrogen consuming gas diffusion anode and a current collecting electrode or (b) a hydrogen consuming gas diffusion anode which is fixedly held between a hydraulic barrier and a current collecting electrode, and (3) at least one pair of intermediate compartments separating the catholyte and anode compartments and separated from each other by an anion exchange membrane. The following are introduced into the cell: a first aqueous conductive electrolyte solution into the catholyte compartment; hydrogen gas into the anode compartment; an aqueous solution of amine hydrohalide into the first compartment of the pair of intermediate compartments; and a second aqueous conductive electrolyte solution into the second compartment of the pair of intermediate compartments. Direct current is passed through the electrolytic cell, and an aqueous solution comprising free amine is removed from the first compartment.
摘要翻译：描述了将胺氢卤化物（例如胺盐酸盐）电化学转化成游离胺，例如游离亚乙基胺的方法。提供一种电解池，其具有（1）阴极电解液室，其包含阴极组件，阴极组件包括阴极和双极离子交换膜，（2）阳极室，其包含阳极组件，阳极组件包括（a）消耗氢的气体扩散阳极和电流收集电极或（b）固定保持在液压屏障和集电电极之间的消耗氢的气体扩散阳极，以及（3）至少一对隔离阴极电解液室和阳极室的中间隔室，阴离子交换膜。将以下物质引入电池中：将第一水性导电电解质溶液引入到阴极电解液室中; 氢气进入阳极室; 胺氢卤酸盐的水溶液进入该对中间隔室的第一隔室; 以及第二水性导电电解质溶液进入所述一对中间隔室中的第二隔室。直流电流通过电解槽，从第一隔室除去包含游离胺的水溶液。

30. 发明授权

US5496476A Non-formaldehyde durable press finishing for cellulosic textiles with phosphonoalkylpolycarboxylic acid 失效
标题翻译：纤维素纺织品与膦酰基烷基多羧酸的非甲醛耐久压机加工
公开(公告)号：US5496476A
公开(公告)日：1996-03-05
申请号：US247943
申请日：1994-05-24
申请人： Robert H. Tang , William A. Williams, Jr.
发明人： Robert H. Tang , William A. Williams, Jr.
IPC分类号： D06M13/192 , D06M13/203 , D06M13/288 , D06M14/04 , D06M15/263 , D06M13/282
CPC分类号： D06M13/203 , D06M13/192 , D06M13/288 , D06M14/04 , D06M15/263 , D06M2101/06
摘要： A composition and method for providing a non-formaldehyde durable press finish to cellulosic fabrics by employing phosphonoalkylpolycarboxylic acids are disclosed. The phosphonoalkylpolycarboxylic acid is optimally used in combination with another polycarboxylic acid, such as polyacrylic acid, and/or, for cost effectiveness, a low-cost polycarboxylic acid such as citric acid. The catalyst for the curing reaction is optimally a phosphorus-containing acid or alkali metal salt thereof, such as a mixture of sodium monophosphate and sodium hypophosphite.
摘要翻译：公开了一种通过使用膦酰基烷基多羧酸向纤维素织物提供非甲醛耐久的压光加工的组合物和方法。膦酰基烷基多羧酸与另一种多元羧酸（如聚丙烯酸）组合使用，和/或为了成本效益，优选使用低成本多元羧酸如柠檬酸。用于固化反应的催化剂最好是含磷酸或其碱金属盐，例如单磷酸钠和次磷酸钠的混合物。

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