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21. 发明授权

US06339182B1 Separation of olefins from paraffins using ionic liquid solutions 有权
标题翻译：使用离子液体溶液从石蜡中分离烯烃
公开(公告)号：US06339182B1
公开(公告)日：2002-01-15
申请号：US09735176
申请日：2000-12-12
申请人： Curtis L. Munson , Laura C. Boudreau , Michael S. Driver , William L. Schinski
发明人： Curtis L. Munson , Laura C. Boudreau , Michael S. Driver , William L. Schinski
IPC分类号： C07C700
CPC分类号： C10G70/002 , B01J2219/00047 , B01J2219/00306 , B01J2219/00599 , B01J2219/00702 , B01J2219/0072 , B01J2219/00759 , C07B63/00 , C07C1/0485 , C07C7/152 , C07C11/02 , C10G29/00 , C40B50/08 , C40B60/14 , G01N30/02 , Y02P30/42
摘要： Methods for separating olefins from non-olefins, such as parafins, including cycloparaffins, oxygenates and aromatics, are provided. The methods use metal salts to complex olefins, allowing the non-olefins to be separated by a variety of methods, including decantation and distillation. The metal salts are dissolved in ionic liquids, which tend to have virtually no vapor pressure, and which poorly solubilize the non-olefins. Accordingly, the non-olefins phase separate well, and can be distilled without carrying over any of the ionic liquid into the distillate. Preferred salts are Group IB salts, more preferably silver salts. A preferred silver salt is silver tetrafluoroborate. Preferred ionic liquids are those which form stable solutions or dispersions of the metal salts, and which do not dissolve the non-olefins. Further, if the olefins are subject to isomerization, the ionic liquid is preferably relatively non-acidic. The methods involve forming a solution of a suitable olefin-complexing salt in an appropriate ionic liquid. An olefin-containing mixture is contacted with the ionic liquid/salt solution, and the olefins are adsorbed. After the paraffins are removed, the olefins can be isolated by desorption. The olefin-containing mixture can be in the gas phase, or in the liquid phase. The flow of olefin-containing mixtures over/through the ionic liquid can be, for example, co-current, counter-current, or staged in stirred tanks. Countcrcurrent is preferred as it is the most efficient. The methods can be optimized using combinatorial chemistry.
摘要翻译：提供了从非烯烃分离烯烃的方法，如石蜡包括环烷烃，含氧化合物和芳族化合物。该方法使用金属盐来络合烯烃，允许通过各种方法分离非烯烃，包括倾析和蒸馏。金属盐溶解在离子液体中，其倾向于几乎不具有蒸气压，并且使非烯烃的溶解性差。因此，非烯烃相分离井，并且可以蒸馏而不将任何离子液体输送到馏出物中。优选的盐是IB族盐，更优选银盐。优选的银盐是四氟硼酸银。优选的离子液体是形成金属盐的稳定溶液或分散体并且不溶解非烯烃的离子液体。此外，如果烯烃经历异构化，离子液体优选是相对非酸性的。所述方法包括在合适的离子液体中形成合适的烯烃络合盐的溶液。使含烯烃的混合物与离子液体/盐溶液接触，并且吸附烯烃。在除去石蜡之后，可以通过解吸分离烯烃。含烯烃的混合物可以处于气相或液相中。通过离子液体的/通过离子液体的含烯烃混合物的流动可以是例如在搅拌釜中的并流，逆流或分段。 Countcrcurrent是首选，因为它是最有效的。该方法可以使用组合化学方法进行优化。

22. 发明授权

US09205371B2 Method for improving total energy demand in a post-combustion carbon capture process with ionic absorbent 有权
标题翻译：用离子吸收剂改善后燃碳捕获过程中总能量需求的方法
公开(公告)号：US09205371B2
公开(公告)日：2015-12-08
申请号：US13336597
申请日：2011-12-23
申请人： Russell Evan Cooper , Daniel Chinn , Zunqing He , Hye Hyung Timken , Michael S. Driver , James H. Davis, Jr. , Kevin N. West
发明人： Russell Evan Cooper , Daniel Chinn , Zunqing He , Hye Hyung Timken , Michael S. Driver , James H. Davis, Jr. , Kevin N. West
IPC分类号： B01D53/62 , B01J31/02 , C07C309/69 , C07C323/25 , B01D53/78 , B01D53/96 , B01D53/14
CPC分类号： B01D53/1493 , B01D53/1475 , B01D53/62 , B01D2252/20405 , B01D2252/20426 , B01D2252/2056 , B01D2252/30 , B01D2258/0283 , Y02C10/04 , Y02C10/06 , Y02C10/08
摘要： Disclosed herein is a method for improving the total energy demand required to separate carbon dioxide (CO2) from an aqueous ionic absorbent solution in a post-combustion carbon capture process. The method involves (a) contacting a flue gas stream containing CO2 with an aqueous ionic absorbent solution under absorption conditions to absorb at least a portion of the CO2 from the flue gas stream and form a CO2-aqueous ionic absorbent solution stream, wherein the aqueous ionic absorbent solution comprises one or more diluents and an ionic absorbent containing a cation and an anion comprising an amine moiety; and (b) subjecting at least a portion of the CO2-aqueous ionic absorbent solution stream to desorption conditions to form a CO2-rich stream and an aqueous ionic absorbent solution stream having a reduced CO2 content.
摘要翻译：本文公开了一种改进在后燃烧碳捕获过程中从含水离子吸收剂溶液中分离二氧化碳（CO 2）所需的总能量需求的方法。该方法包括（a）在吸收条件下使含有CO 2的烟道气流与含水离子吸收剂溶液接触，以从烟道气流吸收至少一部分CO 2并形成CO 2 - 水离子吸收剂溶液流，其中水离子吸收剂溶液包含一种或多种稀释剂和含有阳离子和含有胺部分的阴离子的离子吸收剂; 和（b）使至少一部分CO 2水溶性离子吸收剂溶液流进行解吸条件以形成富二氧化物流和具有降低的CO 2含量的水性离子吸收剂溶液流。

23. 发明申请

US20120167766A1 Process for the separation of carbon dioxide from flue gas 有权
标题翻译：从烟道气中分离二氧化碳的方法
公开(公告)号：US20120167766A1
公开(公告)日：2012-07-05
申请号：US12930207
申请日：2010-12-30
申请人： Daniel Chinn , Russell Evan Cooper , Zunqing He , James H. Davis, JR. , Kevin N. West , Hye Kyung Timken , Michael S. Driver
发明人： Daniel Chinn , Russell Evan Cooper , Zunqing He , James H. Davis, JR. , Kevin N. West , Hye Kyung Timken , Michael S. Driver
IPC分类号： B01D53/18 , B01D53/14
CPC分类号： B01D53/1493 , B01D53/1425 , B01D53/1456 , B01D53/1475 , B01D53/1481 , B01D2252/103 , B01D2252/30 , B01D2258/0233 , B01D2258/025 , B01D2258/0283 , Y02A50/2342 , Y02C10/04 , Y02C10/06
摘要： A process and system for separating CO2 from a flue gas stream is disclosed. The process involves (a) contacting a flue gas stream containing water vapor and CO2 with an ionic absorbent under absorption conditions to absorb at least a portion of the CO2 from the flue gas stream and form a CO2-absorbent complex; wherein the ionic absorbent comprises a cation and an anion comprising an amine moiety; and (b) recovering a gaseous product having a reduced CO2 content.
摘要翻译：公开了一种用于从烟道气流中分离CO 2的方法和系统。该方法包括（a）在吸收条件下使含有水蒸气和CO 2的烟道气与离子吸收剂接触，以从烟道气流吸收至少一部分CO 2并形成CO 2吸收复合物; 其中所述离子吸收剂包含阳离子和包含胺部分的阴离子; 和（b）回收具有降低的CO 2含量的气态产物。

24. 发明授权

US07902419B2 Reduction of organic halides in alkylate gasoline 有权
标题翻译：烷基化汽油中有机卤化物的还原
公开(公告)号：US07902419B2
公开(公告)日：2011-03-08
申请号：US12415652
申请日：2009-03-31
申请人： Michael S. Driver , Gunther H. Dieckmann
发明人： Michael S. Driver , Gunther H. Dieckmann
IPC分类号： C07C2/60 , C07C2/58
CPC分类号： C10G69/123 , C07C2/58 , C07C7/163 , C07C2527/125 , C07C2531/02 , C10G45/10 , C10G50/00
摘要： An alkylation process comprising contacting a first hydrocarbon feed comprising at least one olefin having from 2 to 6 carbon atoms and a second hydrocarbon feed comprising at least one isoparaffin having from 3 to 6 carbon atoms with a halide-based acidic ionic liquid catalyst under alkylation conditions to produce an alkylate containing an organic halide and contacting at least a portion of the alkylate with a hydrotreating catalyst in the presence of hydrogen under hydrotreating conditions to reduce the concentration of the organic halide in the alkylate is disclosed.
摘要翻译：一种烷基化方法，包括在烷基化条件下使包含至少一种具有2至6个碳原子的烯烃的第一烃进料和包含至少一个具有3至6个碳原子的异链烷烃的第二烃进料与卤化物基酸性离子液体催化剂接触以产生含有机卤化物的烷基化物，并且在加氢处理条件下在氢气存在下使烷基化物的至少一部分与加氢处理催化剂接触以降低烷基化物中有机卤化物的浓度。

25. 发明申请

US20100147746A1 REDUCTION OF ORGANIC HALIDE CONTAMINATION IN HYDROCARBON PRODUCTS 有权
标题翻译：减少碳氢化合物产品中的有机卤化物污染
公开(公告)号：US20100147746A1
公开(公告)日：2010-06-17
申请号：US12336240
申请日：2008-12-16
申请人： Michael S. Driver , Saleh A. Elomari , Hye-Kyung C. Timken
发明人： Michael S. Driver , Saleh A. Elomari , Hye-Kyung C. Timken
IPC分类号： C10G21/08
CPC分类号： C10G29/205 , C10G19/02 , C10G2300/1081 , C10G2300/1088 , C10G2300/201 , C10G2400/02
摘要： A method for reducing halide concentration in a hydrocarbon product having an organic halide content which is made by a hydrocarbon conversion process using a halogen-containing acidic ionic liquid catalyst comprising contacting at least a portion of the hydrocarbon product with an aqueous caustic solution under conditions to reduce the halide concentration in the hydrocarbon product is disclosed.
摘要翻译：一种通过使用含卤素的酸性离子液体催化剂的烃转化方法制备的具有有机卤化物含量的烃产物中的卤化物浓度的方法，包括使至少一部分烃产物与苛性碱水溶液接触，公开了减少烃产物中的卤化物浓度。

26. 发明申请

US20090163759A1 REDUCTION OF ORGANIC HALIDE CONTAMINATION IN HYDROCARBON PRODUCTS 有权
标题翻译：减少碳氢化合物产品中的有机卤化物污染
公开(公告)号：US20090163759A1
公开(公告)日：2009-06-25
申请号：US11960506
申请日：2007-12-19
申请人： Michael S. Driver , Howard S. Lacheen , Mitra A. Hosseini
发明人： Michael S. Driver , Howard S. Lacheen , Mitra A. Hosseini
IPC分类号： C07C7/12
CPC分类号： C07C7/13 , C07C2/60 , C07C2531/02 , C10G21/08 , C10G53/04 , C10G57/005 , C10G57/02 , C10G67/04 , C10G2300/1081 , C10G2300/1088 , C10G2300/1092 , C10G2300/201 , C10G2400/02 , C07C9/16
摘要： A method for reducing halide concentration in a hydrocarbon product having an organic halide content from 50 to 4000 ppm which is made by a hydrocarbon conversion process using an ionic liquid catalyst comprising a halogen-containing acidic ionic liquid comprising contacting at least a portion of the hydrocarbon product with at least one molecular sieve having pore size from 4 to 16 Angstrom under organic halide absorption conditions to reduce the halogen concentration in the hydrocarbon product to less than 40 ppm is disclosed.
摘要翻译：一种通过使用包含含卤素的酸性离子液体的离子液体催化剂的烃转化方法制备的有机卤化物含量为50至4000ppm的烃产物中的卤化物浓度的方法，包括使至少一部分烃在有机卤化物吸收条件下具有至少一个具有4至16埃孔径的分子筛的产物，以将烃产物中的卤素浓度降低至小于40ppm。

27. 发明授权

US06623659B2 Separation of olefins from paraffins using ionic liquid solutions 有权
公开(公告)号：US06623659B2
公开(公告)日：2003-09-23
申请号：US09998138
申请日：2001-12-03
申请人： Curtis L. Munson , Laura C. Boudreau , Michael S. Driver , William L. Schinski
发明人： Curtis L. Munson , Laura C. Boudreau , Michael S. Driver , William L. Schinski
IPC分类号： C09K300
CPC分类号： C10G70/002 , B01J2219/00047 , B01J2219/00306 , B01J2219/00599 , B01J2219/00702 , B01J2219/0072 , B01J2219/00759 , C07B63/00 , C07C1/0485 , C07C7/152 , C07C11/02 , C10G29/00 , C40B50/08 , C40B60/14 , G01N30/02 , Y02P30/42
摘要： Methods for separating olefins from non-olefins, such as paraffins, including cycloparaffins, oxygenates and aromatics, are provided. The methods use metal salts to complex olefins, allowing the non-olefins to be separated by a variety of methods, including decantation and distillation. The metal salts are dissolved in ionic liquids, which tend to have virtually no vapor pressure, and which poorly solubilize the non-olefins. Accordingly, the non-olefins phase separate well, and can be distilled without carrying over any of the ionic liquid into the distillate. Preferred salts are Group IB salts, more preferably silver salts. A preferred silver salt is silver tetrafluoroborate. Preferred ionic liquids are those which form stable solutions or dispersions of the metal salts, and which do not dissolve the non-olefins. Further, if the olefins are subject to isomerization, the ionic liquid is preferably relatively non-acidic. The methods involve forming a solution of a suitable olefin-complexing salt in an appropriate ionic liquid. An olefin-containing mixture is contacted with the ionic liquid/salt solution, and the olefins are adsorbed. After the paraffins are removed, the olefins can be isolated by desorption. The olefin-containing mixture can be in the gas phase, or in the liquid phase. The flow of olefin-containing mixtures over/through the ionic liquid can be, for example, co-current, counter-current, or staged in stirred tanks. Countercurrent is preferred as it is the most efficient. The methods can be optimized using combinatorial chemistry.

28. 发明授权

US5817877A Metal-catalyzed amination of organic sulfonates to organic amines 失效
标题翻译：将有机磺酸盐金属催化胺化成有机胺
公开(公告)号：US5817877A
公开(公告)日：1998-10-06
申请号：US933658
申请日：1997-09-19
申请人： John F. Hartwig , Michael S. Driver , Janis Louie , Blake Hamann
发明人： John F. Hartwig , Michael S. Driver , Janis Louie , Blake Hamann
IPC分类号： C07C209/18 , C07D295/023 , C07C209/22
CPC分类号： C07D295/023 , C07C209/18
摘要： A process of preparing an organic amine having at least one unsaturated group, such as an arylamine, involving contacting an unsaturated organic sulfonate, such as an aryl sulfonate, with a reactant amine, such as an alkyl or aryl amine, in the presence of a base and a transition metal catalyst under reaction conditions. The transition metal catalyst contains a Group 8 metal and a chelating ligand, for example a Group 15-substituted arylene or Group 15-substituted metallocene, such as 1,1'-bis(diphenylphosphino)-2,2'-binaphthyl or 1,1'-bis(diphenylphosphino)-ferrocene, respectively. The aryl sulfonate can be prepared from a phenol and sulfonating agent.
摘要翻译：制备具有至少一个不饱和基团的有机胺的方法，例如芳基胺，包括使不饱和有机磺酸酯如芳基磺酸酯与反应物胺如烷基或芳基胺在存在下进行接触碱和过渡金属催化剂。过渡金属催化剂含有第8族金属和螯合配体，例如第15族取代的亚芳基或第15族取代的茂金属，例如1,1'-双（二苯基膦基）-2,2'-联萘或1,1-二 1'-双（二苯基膦基） - 二茂铁。芳基磺酸盐可以由苯酚和磺化剂制备。

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