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21. 发明授权

US4760100A Terephthalic ester polyols modified with ethoxylated amines and amides and rigid foams therefrom 失效
标题翻译：用乙氧基化胺和酰胺改性的对苯二甲酸酯多元醇及其刚性泡沫
公开(公告)号：US4760100A
公开(公告)日：1988-07-26
申请号：US113642
申请日：1987-10-26
申请人： Kenneth G. McDaniel
发明人： Kenneth G. McDaniel
IPC分类号： C08G18/50 , C08G18/42 , C08G18/46 , C08G63/68 , C08G63/685 , C08G18/14
CPC分类号： C08G18/4247 , C08G18/4615 , C08G63/6856 , C08G2105/02
摘要： The preparation of isocyanurate foams from a recycled polyethylene terephthalate polyol modified with alkoxylated amines and alkoxylated amides is disclosed. These modified foams exhibit improved fluorocarbon solubility, and do not cause the resultant polyols to be monofunctional, but rather difunctional. The foams may be used for building, roofing and sheathing applications.

22. 发明授权

US4442237A Novel aromatic amide polyols from the reaction of phthalic acid residues, alkylene glycols and amino alcohols 失效
标题翻译：来自邻苯二甲酸残基，亚烷基二醇和氨基醇反应的新型芳香族酰胺多元醇
公开(公告)号：US4442237A
公开(公告)日：1984-04-10
申请号：US443726
申请日：1982-11-22
申请人： Robert L. Zimmerman , Kenneth G. McDaniel
发明人： Robert L. Zimmerman , Kenneth G. McDaniel
IPC分类号： C08G69/00 , C08G18/00 , C08G18/02 , C08G18/42 , C08G18/46 , C08G18/60 , C08G69/44 , C08G18/14
CPC分类号： C08G18/4615 , C08G18/4213 , C08G18/4225 , C08G2105/02
摘要： Mixtures of aromatic polyols containing tertiary amine and ester functionalities suitable for use in rigid foams prepared by reacting a phthalic acid residue with an alkylene glycol and an amino alcohol are described. These novel polyols may be blended with conventional polyols to yield rigid polyurethane foams with better flammability resistance as compared with foams made from conventional polyols alone.
摘要翻译：描述了含有叔胺和适用于通过邻苯二甲酸残基与亚烷基二醇和氨基醇反应制备的硬质泡沫中的酯官能团的芳族多元醇的混合物。与常规多元醇单独制成的泡沫相比，这些新型多元醇可与常规多元醇共混以产生具有更好的耐燃性的硬质聚氨酯泡沫。

23. 发明申请

US20130023599A1 POLYURETHANE FOAMS MADE WITH ALKOXYLATED VEGETABLE OIL HYDROXYLATE 审中-公开
标题翻译：用烷氧基化的油酸羟丙酯制成聚氨酯泡沫
公开(公告)号：US20130023599A1
公开(公告)日：2013-01-24
申请号：US13627127
申请日：2012-09-26
申请人： Yu-Ling Hsiao , Richard G. Skorpenske , Bryan D. Kaushiva , Kenneth G. McDaniel , Jose F. Pazos , Stanley L. Hager , Karl W. Haider
发明人： Yu-Ling Hsiao , Richard G. Skorpenske , Bryan D. Kaushiva , Kenneth G. McDaniel , Jose F. Pazos , Stanley L. Hager , Karl W. Haider
IPC分类号： C07C51/367 , C08G18/68
CPC分类号： C08G18/4891 , C08G18/4866 , C08G2101/0008 , C08G2101/005
摘要： The present invention provides polyurethane foams and elastomers made with an alkoxylated vegetable oil hydroxylate replacing at least a portion of the typically used petroleum-based polyol(s). Also provided are processes for making the inventive foams and elastomers and for making alkoxylated vegetable oil hydroxylates. The alkoxylated vegetable oil hydroxylates are environmentally-friendly, bio-based polyols which advantageously also offer the potential of improved hydrophobicity in polyurethane foams and elastomers. The inventive polyurethane foams and elastomers may find use in a wide variety of products such as automobile interior parts, polyurethane structural foams, floor coatings and athletic running tracks.
摘要翻译：本发明提供用烷氧基化植物油羟基化物制备的聚氨酯泡沫和弹性体，代替至少一部分通常使用的石油基多元醇。还提供了制备本发明的泡沫和弹性体以及用于制备烷氧基化植物油羟基化物的方法。烷氧基化植物油羟基化物是环境友好的基于生物的多元醇，其有利地还提供聚氨酯泡沫和弹性体中改善的疏水性的潜力。本发明的聚氨酯泡沫和弹性体可以用于各种各样的产品，例如汽车内部部件，聚氨酯结构泡沫，地板涂料和运动跑道。

24. 发明申请

US20100331517A1 POLYETHER CARBONATE POLYOLS MADE VIA DOUBLE METAL CYANDIE (DMC) CATALYSIS 有权
标题翻译：聚碳酸酯多元醇通过双金属氰化物（DMC）催化
公开(公告)号：US20100331517A1
公开(公告)日：2010-12-30
申请号：US12880231
申请日：2010-09-13
申请人： Karl W. Haider , Kenneth G. McDaniel , John E. Hayes , Jianzhong Shen
发明人： Karl W. Haider , Kenneth G. McDaniel , John E. Hayes , Jianzhong Shen
IPC分类号： C08G64/02
CPC分类号： C08G64/183 , C08G64/32 , C08G65/2663
摘要： The present invention relates to a polyether carbonate polyol made by copolymerizing a starter molecule with carbon dioxide, at a pressure ranging from about 10 psia to about 2,000 psia, and an alkylene oxide, at a temperature ranging from about 50° C. to about 190° C. and in the presence of from about 0.001 Wt. % to about 0.2 wt. % of a substantially non-crystalline double metal cyanide (DMC) catalyst, wherein the polyol has an incorporated carbon dioxide content of from about 1 wt. % to about 40 wt. %, wherein the ratio of cyclic carbonate by-product to total carbonate is less than about 0.3 and wherein the weight percentages are based on the weight of the polyol. The inventive polyether carbonate polyols may find use in producing polyurethane foams, elastomers, coatings, sealants and adhesives with improved properties.
摘要翻译：本发明涉及一种聚醚碳酸酯多元醇，其通过将起始分子与二氧化碳在约10psia至约2,000psia的压力和烯化氧的温度范围内共聚而制备，温度为约50℃至约190℃ 在约0.001Wt的存在下。％至约0.2wt。％的基本上非结晶的双金属氰化物（DMC）催化剂，其中所述多元醇具有约1wt。％至约40wt。％，其中环状碳酸酯副产物与总碳酸盐的比例小于约0.3，并且其中重量百分比基于多元醇的重量。本发明的聚醚碳酸酯多元醇可用于生产具有改进性能的聚氨酯泡沫，弹性体，涂料，密封剂和粘合剂。

25. 发明授权

US6077978A Direct polyoxyalkylation of glycerine with double metal cyanide catalysis 失效
标题翻译：甘油双金属氰化物催化直接聚氧化烷基化
公开(公告)号：US6077978A
公开(公告)日：2000-06-20
申请号：US932613
申请日：1997-09-17
申请人： Kenneth G. McDaniel , Mark J. Perry , John E. Hayes
发明人： Kenneth G. McDaniel , Mark J. Perry , John E. Hayes
IPC分类号： C08G65/26 , C08G65/10 , C07C43/11
CPC分类号： C08G65/2663 , C08G65/2696
摘要： Acidification, neutralization, or removal of basic impurities from acid sensitive low molecular weight starter or acidification of a reactor heel prior to addition of acid sensitive low molecular weight starter allows direct oxyalkylation of continuously added acid sensitive low molecular weight starter to produce polyoxyalkylene acid sensitive low molecular weight starter-initiated or co-initiated polyols in the presence of a double metal cyanide catalyst. The preferred acid sensitive low molecular weight starter is glycerine.
摘要翻译：在加入酸敏感低分子量起始剂之前，酸化，中和或从酸敏感低分子量起始剂中除去碱性杂质或反应器脚跟的酸化使得连续加入的酸敏感低分子量起始物的直接烷氧基化产生聚氧化烯酸敏感性低分子量起始物起始或共引发的多元醇在双金属氰化物催化剂存在下进行。优选的酸敏低分子量起动剂是甘油。

26. 发明授权

US5990232A Stabilizers for polymer polyols 失效
标题翻译：聚合物多元醇的稳定剂
公开(公告)号：US5990232A
公开(公告)日：1999-11-23
申请号：US918207
申请日：1997-08-25
申请人： Jianzhong Shen , Kenneth G. McDaniel , John E. Hayes , Uli B. Holeschovsky , Harry R. Hinney
发明人： Jianzhong Shen , Kenneth G. McDaniel , John E. Hayes , Uli B. Holeschovsky , Harry R. Hinney
IPC分类号： C08G18/48 , C08G18/63 , C08G65/26 , C08L71/02 , C08K5/06
CPC分类号： C08G65/2663 , C08G18/4866 , C08G18/633 , C08G18/636 , C08G65/2615 , C08G65/2642 , C08L71/02
摘要： Unique, well defined polyethers containing both hydroxyl-functionality and unsaturation-functionality are prepared by oxyalkylating an unsaturated monomer having at least two free carboxylic acid groups in the presence of an effective amount of a double metal cyanide complex catalyst, optionally, when necessary, in the presence of a free radical polymerization inhibitor. The resulting polyethers are eminently suitable for such uses as polymer polyol stabilizers or stabilizer precursors, and both in situ and ex situ impact modifiers for thermoplastics.
摘要翻译：含有羟基官能度和不饱和官能度的独特的，明确定义的聚醚通过在有效量的双金属氰化物配合物催化剂存在下，任选地，必要时，在至少两个游离羧酸基团的存在下，在存在自由基聚合抑制剂。所得聚醚特别适用于聚合物多元醇稳定剂或稳定剂前体以及热塑性塑料的原位和非原位冲击改性剂。

27. 发明授权

US4902816A Polyols from phthalic compounds 失效
标题翻译：来自邻苯二甲酸酯的多元醇
公开(公告)号：US4902816A
公开(公告)日：1990-02-20
申请号：US173788
申请日：1988-03-28
申请人： Kenneth G. McDaniel
发明人： Kenneth G. McDaniel
IPC分类号： C07C67/03 , C07C69/80
CPC分类号： C07C67/03 , C07C69/80
摘要： Polyols containing polyether and polyester moieties, based on phthalic acid are described. A phthalic acid derivative is reacted with a polyether polyol to give the novel polyols which are useful not only in polyisocyanurate foams, but also polyurethane foams as well. The phthalic acid derivative may be phthalic acid, phthalic anhydride and an ester of phthalic acid, for example. The polyester polyol is made from an initiator selected from the group consisting of alkanolamines, alkyleneamines, arylamines, sucrose, glycerin, sorbitol, .alpha.-methylglucoside, .beta.-methylglucoside, and mixtures thereof. The polyester polyol may be made by alkoxylating the initiators.
摘要翻译：描述了含有基于邻苯二甲酸的聚醚和聚酯部分的多元醇。使邻苯二甲酸衍生物与聚醚多元醇反应，得到不仅可用于聚异氰脲酸酯泡沫，而且可用于聚氨酯泡沫的新型多元醇。邻苯二甲酸衍生物可以是例如邻苯二甲酸，邻苯二甲酸酐和邻苯二甲酸的酯。聚酯多元醇由选自链烷醇胺，亚烷基胺，芳基胺，蔗糖，甘油，山梨糖醇，α-甲基葡糖苷，β-甲基葡糖苷及其混合物的引发剂制成。聚酯多元醇可以通过使引发剂烷氧基化来制备。

28. 发明授权

US4644019A Modified terephthalic ester polyols and rigid foams therefrom 失效
标题翻译：改性对苯二甲酸酯多元醇及其刚性泡沫
公开(公告)号：US4644019A
公开(公告)日：1987-02-17
申请号：US791679
申请日：1985-10-28
申请人： Kenneth G. McDaniel
发明人： Kenneth G. McDaniel
IPC分类号： C08G18/42 , C08G18/14 , C08G18/16 , C08G18/32 , C08G18/34
CPC分类号： C08G18/4213 , C08G18/4247 , C08G2105/02 , Y10S521/902
摘要： The preparation of isocyanurate foams from a recycled polyethylene terephthalate polyol modified with a polyethoxylated nonylphenol is disclosed. These modified foams exhibit improved fluorocarbon solubility. The foams may be used for building roofing and sheathing applications.
摘要翻译：公开了用聚乙氧基化壬基酚改性的再循环的聚对苯二甲酸乙二醇酯多元醇制备异氰脲酸酯泡沫。这些改性泡沫表现出改善的氟碳溶解度。泡沫可用于建筑屋顶和护套应用。

29. 发明授权

US4383102A Method for producing a low viscosity spray polyol by reacting an alkylene oxide with the reaction product of a phenol, an amine and a smaller formaldehyde portion 失效
标题翻译：通过使环氧烷与苯酚，胺和较小甲醛部分的反应产物反应来生产低粘度喷雾多元醇的方法
公开(公告)号：US4383102A
公开(公告)日：1983-05-10
申请号：US344127
申请日：1982-01-29
申请人： Kenneth G. McDaniel , George P. Speranza
发明人： Kenneth G. McDaniel , George P. Speranza
IPC分类号： C07D295/08 , C07C67/00 , C07C213/00 , C07C213/02 , C07C217/08 , C07C217/58 , C08G14/12 , C08G18/00 , C08G18/32 , C08G18/50 , C08G18/54 , C08G67/00
CPC分类号： C08G14/12 , C08G18/5033 , C08G18/546 , C08G2101/0025 , C08G2101/005 , C08G2150/60
摘要： An improved method for the production of polyols useful in the application of sprayed high density polyurethane foams is described. The improvement involves varying the formaldehyde to phenol mole ratio to range between 1.25:1 to 1.75:1 to produce a polyol with the desired viscosity. Ordinarily such polyols are prepared by reacting 4.65 to 5 moles of propylene oxide with 1 mole of the Mannich reaction product of a mole of phenol or nonylphenol with 1 or 2 moles of diethanolamine and 1 or 2 moles of formaldehyde. It is particularly surprising that such changes in the formulation may be made without adversely affecting the resultant properties of the spray foam.
摘要翻译：描述了用于生产用于喷涂高密度聚氨酯泡沫塑料的多元醇的改进方法。改进之处在于将甲醛与苯酚的摩尔比变化到1.25:1至1.75:1之间，以产生具有所需粘度的多元醇。通常这样的多元醇通过使4.65-5摩尔环氧丙烷与1摩尔苯酚或壬基酚与1摩尔或2摩尔二乙醇胺和1或2摩尔甲醛的曼尼希反应产物反应来制备。特别令人惊讶的是，制剂中的这种变化可以在不影响喷雾泡沫的所得性质的情况下进行。

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