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21. 发明授权

US5977292A Process for the preparation of polyesters in carbon dioxide 失效
标题翻译：在二氧化碳中制备聚酯的方法
公开(公告)号：US5977292A
公开(公告)日：1999-11-02
申请号：US903269
申请日：1997-07-25
申请人： Joseph M. DeSimone , Gerhard Maier
发明人： Joseph M. DeSimone , Gerhard Maier
IPC分类号： C08G63/06 , C08G63/08 , C08G63/18 , C08G63/183 , C08G63/78 , C08G63/80 , C08G63/81
CPC分类号： C08G63/80 , C08G63/06 , C08G63/78 , C08G63/81 , C08G63/18 , C08G63/183
摘要： The present invention provides processes for preparing polyesters. The processes include (a) providing a polymerization medium comprising carbon dioxide, (b) contacting a monomer capable of forming a polyester polymer with the polymerization medium, and (c) polymerizing the monomer in the polymerization medium. The processes of the present invention include preparing polyesters by direct esterification polymerization, transesterification polymerization, melt acidolysis polymerization and acid halide polymerization. As a further aspect, the present invention provides a method of separating the polyester produced from the polymerization medium. Polyester polymers prepared according to the methods of the present invention are also provided.
摘要翻译：本发明提供了制备聚酯的方法。这些方法包括（a）提供包含二氧化碳的聚合介质，（b）使能够形成聚酯聚合物的单体与聚合介质接触，和（c）在聚合介质中聚合单体。本发明的方法包括通过直接酯化聚合，酯交换聚合，熔融酸解聚合和酰卤聚合来制备聚酯。另外，本发明提供了从聚合介质中分离聚酯的方法。还提供了根据本发明的方法制备的聚酯聚合物。

22. 发明授权

US5939501A Nonaqueous polymerization of fluoromonomers 失效
标题翻译：氟单体的非水聚合
公开(公告)号：US5939501A
公开(公告)日：1999-08-17
申请号：US680701
申请日：1996-07-17
申请人： Joseph M. DeSimone , Timothy Romack
发明人： Joseph M. DeSimone , Timothy Romack
IPC分类号： C08F2/00 , C08F4/04 , C08F4/34 , C08F14/18 , C08F16/24
CPC分类号： C08F16/24 , C08F14/18 , Y02P20/544 , Y10S526/942
摘要： The present invention provides a process for making fluorinated polymers and copolymers having stable end groups. The process includes (1) contacting a fluoromonomer, an initiator capable of producing stable end groups on the polymer chain, and a polymerization medium comprising carbon dioxide, and (2) polymerizing the fluoromonomer. The polymerization medium preferably comprises liquid or supercritical carbon dioxide. Advantageously, the process may also include the step of separating the fluoropolymer from the polymerization medium.The present invention also provides polymerization reaction mixtures useful in the processes of the present invention.
摘要翻译：本发明提供一种制备具有稳定端基的氟化聚合物和共聚物的方法。该方法包括（1）使含氟单体，能够在聚合物链上产生稳定端基的引发剂和包含二氧化碳的聚合介质接触，和（2）使该含氟单体聚合。聚合介质优选包含液体或超临界二氧化碳。有利地，该方法还可以包括从聚合介质中分离含氟聚合物的步骤。本发明还提供了可用于本发明方法的聚合反应混合物。

23. 发明授权

US5739223A Method of making fluoropolymers 失效
公开(公告)号：US5739223A
公开(公告)日：1998-04-14
申请号：US529873
申请日：1995-09-18
申请人： Joseph M. DeSimone
发明人： Joseph M. DeSimone
IPC分类号： B05D1/02 , B05D5/08 , C08F2/00 , C08F2/02 , C08F2/04 , C08F2/06 , C08F12/00 , C08F12/14 , C08F12/20 , C08F14/18 , C08F16/14 , C08F16/22 , C08F16/24 , C08F20/22 , C08J3/02
CPC分类号： C08J3/02 , B05D1/025 , B05D5/083 , C08F12/20 , C08F14/18 , C08F16/22 , C08F16/24 , C08F20/22 , C08J2327/12 , Y02P20/544 , Y10S526/942
摘要： A process for making a fluoropolymer is disclosed. The process comprises solubilizing a fluoromonomer in solvent comprising a carbon dioxide fluid, and then polymerizing the fluoromonomer to produce a the fluoropolymer. A preferred solvent for carrying out the process is supercritical carbon dioxide; preferred fluoromonomers for carrying out the process are fluoroacrylate monomers such as 1,1-dihydroperfluorooctyl acrylate. The polymerization step is preferably carried out in the presence of an initiator such as azobisisobutyronitrile.

24. 发明授权

US5420224A Thiophene-based polymers 失效
标题翻译：基于噻吩的聚合物
公开(公告)号：US5420224A
公开(公告)日：1995-05-30
申请号：US212345
申请日：1994-03-11
申请人： Edward T. Samulski , Joseph M. DeSimone
发明人： Edward T. Samulski , Joseph M. DeSimone
IPC分类号： C08G65/40 , C08G69/32 , C08G69/42 , C08G8/02 , C08G73/08 , C08G73/22
CPC分类号： C08G69/42 , C08G65/4062 , C08G69/32 , Y10T428/2913 , Y10T428/2967 , Y10T428/31504 , Y10T428/31725 , Y10T428/31855
摘要： Poly(arylene ether)ketones, polyamides, and poly(benzoxazoles) that contain thiophene rings within the aromatic polymer backbone are disclosed, along with fibers, films, and other articles of manufacture formed therefrom.
摘要翻译：公开了在芳族聚合物主链中含有噻吩环的聚（亚芳基醚）酮，聚酰胺和聚（苯并恶唑）以及由其形成的纤维，薄膜和其它制品。

25. 发明授权

US5312882A Heterogeneous polymerization in carbon dioxide 失效
标题翻译：二氧化碳中的非均相聚合
公开(公告)号：US5312882A
公开(公告)日：1994-05-17
申请号：US99905
申请日：1993-07-30
申请人： Joseph M. DeSimone , Elise E. Maury , James R. Combes , Yusuf Z. Menceloglu
发明人： Joseph M. DeSimone , Elise E. Maury , James R. Combes , Yusuf Z. Menceloglu
IPC分类号： C08F2/18 , C08F2/00 , C08F2/04 , C08F2/08 , C08F2/24 , C08F4/04 , C08F290/00 , C08F290/04 , C08F290/06 , C08F290/14 , C08F293/00 , C08F297/00
CPC分类号： C08F2/04 , C08F2/08 , C08F290/148 , Y10S516/01 , Y10S526/942 , Y10T428/12569 , Y10T428/1369
摘要： The heterogeneous polymerization of water-soluble polymer in CO.sub.2 is disclosed. The method comprises providing a heterogeneous reaction mixture comprising CO.sub.2, a monomer, and a surfactant, then polymerizing the monomer to form a water-soluble polymer.
摘要翻译：公开了水溶性聚合物在二氧化碳中的非均相聚合。该方法包括提供包含CO 2，单体和表面活性剂的非均相反应混合物，然后聚合单体以形成水溶性聚合物。

26. 发明授权

US07919162B2 Intraluminal prostheses having polymeric material with selectively modified crystallinity and methods of making same 有权
标题翻译：具有选择性改性结晶度的聚合材料的管腔内假体及其制备方法
公开(公告)号：US07919162B2
公开(公告)日：2011-04-05
申请号：US11146455
申请日：2005-06-07
申请人： Joseph M. DeSimone , Michael S. Williams
发明人： Joseph M. DeSimone , Michael S. Williams
IPC分类号： B29D22/00 , A61F2/06
CPC分类号： A61F2/07 , A61L27/44 , A61L27/54 , A61L27/58 , A61L31/04 , A61L31/14 , A61L2300/20 , Y10T428/1352 , Y10T428/139
摘要： Methods of manufacturing polymeric intraluminal prostheses include annealing the polymeric material to selectively modify the crystallinity thereof. Annealing may be utilized to selectively modify various properties of the polymeric material of an intraluminal prosthesis, including: selectively increasing the modulus of the polymeric material; selectively increasing the hoop strength of the intraluminal prosthesis; selectively modifying the elution rate (increase or decrease) of a pharmacological agent subsequently disposed on or within the annealed polymeric material; selectively increasing/decreasing stress in the intraluminal prosthesis; and selectively modifying the polymeric material such that it erodes at a different rate.
摘要翻译：制造聚合物腔内假体的方法包括退火聚合物材料以选择性地改变其结晶度。可以使用退火来选择性地修改管腔内假体的聚合材料的各种性质，包括：选择性地增加聚合材料的模量; 选择性地增加腔内假体的环箍强度; 选择性地改变随后设置在退火的聚合材料上或其内的药剂的洗脱速率（增加或减少）; 在腔内假体中选择性增加/减少应力; 并且选择性地改性聚合材料，使得其以不同的速率腐蚀。

27. 发明授权

US07658989B2 Nano-and micro-cellular foamed thin-walled material, and processes and apparatuses for making the same 失效
标题翻译：纳米和微孔泡沫薄壁材料，以及其制造方法和装置
公开(公告)号：US07658989B2
公开(公告)日：2010-02-09
申请号：US10109174
申请日：2002-03-27
申请人： Joseph M. DeSimone , Srinivas Siripurapu , Saad A. Khan , Richard J. Spontak , Joseph Royer
发明人： Joseph M. DeSimone , Srinivas Siripurapu , Saad A. Khan , Richard J. Spontak , Joseph Royer
IPC分类号： B32B3/26 , B32B9/00
CPC分类号： B32B5/18 , B29C44/3453 , B29C44/348 , B32B5/32 , B32B27/065 , B32B27/08 , C08J9/122 , C08J9/34 , C08J2201/032 , C08J2203/06 , Y10T428/249953 , Y10T428/249961 , Y10T428/249978 , Y10T428/249979 , Y10T428/249981 , Y10T428/249986 , Y10T428/249987 , Y10T428/249988 , Y10T428/265
摘要： Polymeric materials having a plurality of cells formed therein are described. The polymeric materials include a foamed layer comprising a plurality of uniform microcells, nanocells or combinations thereof in a closed cell network, a transition layer positioned adjacent to the foamed layer, and at least one unfoamed outer layer positioned adjacent to the transition layer. The foamed layer may be present in a volume ranging from about 80 to about 99 percent based on the volume of the polymeric material, the transition layer may present in a volume ranging from about 0 to about 10 percent based on the volume of the polymeric material, and the at least one outer layer may be present in a volume ranging from about 0.01 to about 10 percent based on the volume of the polymeric material. Methods of making such polymeric materials are also described, as are apparatus for providing foamed polymeric materials.
摘要翻译：对其中形成有多个电池的聚合材料进行了描述。聚合物材料包括泡沫层，其包含多个均匀的微孔，纳米孔或其在闭孔网络中的组合，邻近发泡层定位的过渡层，以及与过渡层相邻定位的至少一个未发泡的外层。基于聚合物材料的体积，发泡层可以以约80至约99％的体积存在，基于聚合物材料的体积，过渡层可以以约0至约10％的体积存在，并且所述至少一个外层可以以基于聚合物材料的体积的约0.01至约10％的体积存在。还描述了制备这种聚合材料的方法，以及用于提供泡沫聚合材料的设备。

28. 发明申请

US20080248438A1 ORTHODONTIC APPLIANCES AND MATERIALS FOR MAKING SAME 审中-公开
标题翻译：正交设备和制造材料
公开(公告)号：US20080248438A1
公开(公告)日：2008-10-09
申请号：US11947172
申请日：2007-11-29
申请人： Joseph M. DeSimone , Robert E. Tricca
发明人： Joseph M. DeSimone , Robert E. Tricca
IPC分类号： A61C3/00
CPC分类号： A61C7/08 , A61C7/002
摘要： The polymeric shell of a removable dental positioning appliance is formed from transparent polymeric materials having a tensile strength at yield of greater than 6,000 pounds per square inch (psi), an elongation at yield of greater than 4%, an elongation at break of greater than 80%, a tensile modulus greater than 200,000 psi, a flexural modulus greater than 200,000 psi, stress relaxation over time of not more than 50%, and a transmissivity of light between 400 nm and 800 nm greater than 75%.
摘要翻译：可拆卸牙科定位器具的聚合物外壳由透明聚合物材料形成，该材料的屈服强度大于6,000磅/平方英寸（psi），伸长率大于4％，断裂伸长率大于 80％，拉伸模量大于200,000psi，挠曲模量大于200,000psi，应力松弛随时间不超过50％，光的透射率在400nm和800nm之间大于75％。

29. 发明授权

US07410620B2 Apparatus for continuous production of polymers in carbon dioxide 失效
标题翻译：用于在二氧化碳中连续生产聚合物的装置
公开(公告)号：US07410620B2
公开(公告)日：2008-08-12
申请号：US11112420
申请日：2005-04-22
申请人： Paul A. Charpentier , Joseph M. DeSimone , George W. Roberts
发明人： Paul A. Charpentier , Joseph M. DeSimone , George W. Roberts
IPC分类号： B01J19/00 , C08F6/00 , C08F2/12
CPC分类号： B01J19/1881 , B01J3/008 , B01J8/0055 , B01J8/006 , B01J19/2435 , B01J19/2465 , B01J19/2475 , B01J2219/00006 , B01J2219/00015 , B01J2219/00033 , B01J2219/00114 , B01J2219/00135 , B01J2219/00166 , C08F2/04 , C08F14/22 , Y02P20/544 , Y10S526/942
摘要： A method for carrying out the continuous polymerization of a monomer in a carbon dioxide reaction medium comprises the steps of: (a) providing an apparatus including a continuous reaction vessel and a separator; (b) carrying out a polymerization reaction in the reaction vessel by combining a monomer and a carbon dioxide reaction medium therein (and preferably by also combining an initiator therein), wherein the reaction medium is a liquid or supercritical fluid, and wherein the reaction produces a solid polymer product in the reaction vessel; then (c) withdrawing a continuous effluent stream from the reaction vessel during the polymerization reaction, wherein the effluent stream is maintained as a liquid or supercritical fluid; then (d) passing the continuous effluent stream through the separator and separating the solid polymer therefrom while maintaining at least a portion of the effluent stream as a liquid or supercritical fluid; and then (e) returning at least a portion of the continuous effluent stream to the reaction vessel while maintaining the effluent stream as a liquid or supercritical fluid. The need for significant recompression of the continuous effluent stream prior to return to the reaction vessel is thereby minimized. Apparatus for carrying out such methods is also disclosed.
摘要翻译：在二氧化碳反应介质中进行单体的连续聚合的方法包括以下步骤：（a）提供包括连续反应容器和分离器的装置; （b）通过在其中组合单体和二氧化碳反应介质（优选通过将其中的引发剂结合在其中）来在反应容器中进行聚合反应，其中反应介质是液体或超临界流体，其中反应产生反应容器中的固体聚合物产物; 然后（c）在聚合反应期间从反应容器中取出连续的流出物流，其中流出物流被保持为液体或超临界流体; 然后（d）使连续的流出物流通过分离器并从其中分离固体聚合物，同时将至少一部分流出物流保持为液体或超临界流体; 然后（e）将至少一部分连续流出物流返回到反应容器中，同时将流出物流保持为液体或超临界流体。因此，在返回到反应容器之前对连续流出物流进行显着再压缩的需要被最小化。还公开了用于执行这种方法的装置。

30. 发明授权

US07141061B2 Photocurable endoprosthesis system 有权
标题翻译：光固化假体内系统
公开(公告)号：US07141061B2
公开(公告)日：2006-11-28
申请号：US10342771
申请日：2003-01-15
申请人： Michael S. Williams , Kevin D. Holbrook , Richard A. Glenn , Jeffrey A. Smith , Joseph M. DeSimone
发明人： Michael S. Williams , Kevin D. Holbrook , Richard A. Glenn , Jeffrey A. Smith , Joseph M. DeSimone
IPC分类号： A61F2/006
CPC分类号： A61F2/90 , A61F2/848 , A61F2002/825 , A61F2220/005 , A61F2220/0058 , A61F2250/0014 , A61L27/34 , A61L27/54 , A61L29/085 , A61L29/16 , A61L31/10 , A61L31/16 , A61L2300/00
摘要： Novel endoprostheses comprising one or more photocurable materials are disclosed. Said endoprostheses may comprise regions wherein said photocurable materials are selectively disposed about said endoprosthesis and are cured according to desired parameters to achieve varying desired properties. Said properties may include but are not limited to cross-linking density, material density, modulus of elasticity, rate of erosion, extensibility, compressibility, mechanical strength, tensile strength, crystallinity, diffusion coefficient, and permeability.
摘要翻译：公开了包含一种或多种光固化材料的新型内用假体。所述内假体可以包括其中所述可光固化材料围绕所述内假体选择性地设置并且根据期望的参数固化以实现变化的所需性质的区域。所述性质可以包括但不限于交联密度，材料密度，弹性模量，侵蚀速率，伸长率，压缩性，机械强度，拉伸强度，结晶度，扩散系数和渗透性。

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