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21. 发明申请

US20080128615A1 Real time analyzer and method for analysis 审中-公开
标题翻译：实时分析仪和分析方法
公开(公告)号：US20080128615A1
公开(公告)日：2008-06-05
申请号：US11987085
申请日：2007-11-27
申请人： Masuyoshi Yamada , Masako Ishimaru
发明人： Masuyoshi Yamada , Masako Ishimaru
IPC分类号： H01J49/04
CPC分类号： H01J49/0422
摘要： An analyzer carrying out analysis with a high degree of qualitative accuracy by separating impurities which hinder the analysis while analyzing in real time. An introducing tube is branched with one branched tube directly leading to an ion source for real time analysis. The other branched tube leads to the ion source so as to introduce the sample gas into the ion source at a later time. When a result of the real time analysis shows that a spectrum pattern on a MS spectrum is changed and an increase in the concentration of an impurity is observed, the introducing path for the sample gas is changed so that the sample gas is introduced into the ion source after the impurity is separated at the separation part.
摘要翻译：分析仪通过分析实时分析分析杂质，以高度的定性精度进行分析。引入管被分支，一个分支管直接通向离子源进行实时分析。另一个分支管通向离子源，以便稍后将样品气体引入离子源。当实时分析的结果表明MS谱上的光谱图变化并且观察到杂质浓度增加时，改变样品气体的引入路径，使样品气体被引入离子杂质在分离部分分离出来。

22. 发明授权

US07375316B2 Mass spectrometer and mass spectrometry 有权
标题翻译：质谱仪和质谱仪
公开(公告)号：US07375316B2
公开(公告)日：2008-05-20
申请号：US11712922
申请日：2007-03-02
申请人： Masuyoshi Yamada , Masao Suga , Izumi Waki
发明人： Masuyoshi Yamada , Masao Suga , Izumi Waki
IPC分类号： H01J49/00 , H01J3/07 , B01D59/44
CPC分类号： H01J49/0422 , H01J49/107
摘要： A mass spectrometer capable of measuring under switching two ion sources at different pressure levels in which a sample gas separated by GC column is branched, and separately introduced to a first ion source (for example, APCI ion source) and a second ion source (for example, EI ion source) at a pressure level lower than that of the first ion source respectively. Preferably, the flow rate of the sample gas introduced to the APCI ion source is made more than the flow rate of the sample gas introduced to the EI ion source, so that the pressure for each of the ion sources can be maintained and analysis can be conducted by each ionization at a good balance in view of the sensitivity.
摘要翻译：一种能够在不同压力水平下切换两个离子源的质谱仪，其中由GC柱分离的样品气体被分支，并分别引入第一离子源（例如APCI离子源）和第二离子源（用于例如，EI离子源），其压力水平分别低于第一离子源的压力水平。优选地，引入到APCI离子源的样品气体的流量比引入到EI离子源的样品气体的流量更多，从而可以保持每个离子源的压力并且可以分析鉴于敏感性，通过各种电离进行良好的平衡。

23. 发明申请

US20080092629A1 Gas component collector, gas component collecting device, filter producing method, and gas component analyzing apparatus 有权
标题翻译：气体成分收集器，气体成分收集装置，过滤器制造方法以及气体成分分析装置
公开(公告)号：US20080092629A1
公开(公告)日：2008-04-24
申请号：US11907905
申请日：2007-10-18
申请人： Masao Suga , Masuyoshi Yamada , Izumi Waki
发明人： Masao Suga , Masuyoshi Yamada , Izumi Waki
IPC分类号： G01N1/22
CPC分类号： A61B5/097 , G01N1/2205 , G01N2001/2244
摘要： A gas component collector comprises a filter assembly 3 comprising an adsorbent and an adsorbent holding plate having a first face, a second face and a plurality of holes that are bored through from the first face to the second face and are filled with the adsorbent adsorbing at least one gas component to be analyzed, the filter assembly satisfying (AL−V)2/L3≧0.003 mm3 and V/AL≧0.3, where V is a total volume of the adsorbent, A is a sum of an opening areas of the holes, and L is an average length of the holes, and a holding container 2 housing the filter assembly 3. On at least one of the holding container 2 a first opening portion for introducing gas and a second opening portion for allowing the introduced gas to be discharged are formed.
摘要翻译：气体成分收集器包括一个过滤器组件3，它包括一个吸附剂和一个吸附剂保持板，该吸附剂保持板具有第一面，第二面和多个从第一面到第二面穿透的孔，并填充吸附在要分析的至少一个气体成分，满足（AL-V）2 / L 3 / SUP 3 = 0.003mm 3和V / AL> = 0.3，其中V是吸附剂的总体积，A是孔的开口面积的总和，L是孔的平均长度，以及容纳过滤器组件3的保持容器2。在保持容器2的至少一个上形成用于引入气体的第一开口部分和用于允许引入气体排出的第二开口部分。

24. 发明授权

US07064320B2 Mass chromatograph 有权
标题翻译：质谱仪
公开(公告)号：US07064320B2
公开(公告)日：2006-06-20
申请号：US11071345
申请日：2005-03-04
申请人： Masuyoshi Yamada , Izumi Waki , Hideo Kasima
发明人： Masuyoshi Yamada , Izumi Waki , Hideo Kasima
IPC分类号： H01J49/26 , G01N27/62
CPC分类号： H01J49/0422 , G01N30/7213 , H01J49/145 , H01J49/168
摘要： A mass spectrometer has an atmospheric pressure chemical ionization source that includes a first ionization portion including a needle electrode, for generating a primary ion by discharge of the needle electrode a primary ion introduction aperture, and a second ionization portion including an introduction aperture, for generating a sample ion by the reaction between the primary ion and the sample gas introduced from an end of a column of gas chromatography, a sample ion movement aperture; and a mass analysis portion; wherein the end is arranged at a position satisfying the relation r≦2R where R is a radius of an inner diameter of the aperture and r is a distance between an axis connecting the center of the aperture and the center of the aperture, and the end.
摘要翻译：质谱仪具有大气压化学电离源，其包括第一离子化部分，其包括针状电极，用于通过针状电极排出初级离子引入孔而产生初级离子;以及第二离子化部分，其包括引入孔，用于产生通过从气相色谱柱的端部引入的初级离子和样品气体之间的反应的样品离子，样品离子运动孔; 和质量分析部分; 其中端部被布置在满足关系r <= 2R的位置处，其中R是孔的内径的半径，r是连接孔的中心的轴线与孔的中心之间的距离，结束。

25. 发明授权

US06852970B2 Mass spectrometer 失效
标题翻译：质谱仪
公开(公告)号：US06852970B2
公开(公告)日：2005-02-08
申请号：US10699805
申请日：2003-11-04
申请人： Masuyoshi Yamada , Izumi Waki
发明人： Masuyoshi Yamada , Izumi Waki
IPC分类号： G01N27/62 , G01N33/00 , H01J49/04 , H01J49/10 , H01M8/04 , H01J49/28
CPC分类号： H01J49/04 , G01N33/005 , H01M8/04082
摘要： There will be provided a mass spectrometer for detecting impurity in sample gas of a low flow rate. A mass spectrometer including: an atmospheric pressure chemical ionization source having a primary ionization part 28 for generating a primary ion by means of electric discharge of reagent gas, and a secondary ionization part 23 for generating an ion of the sample by a reaction of the primary ion and the sample; a mass spectrometric part 11 for performing mass spectrometric analysis of the ion generated; a mixing portion 33 for mixing the sample to be introduced into the secondary ionization part with dilution gas; and a mean 30 for controlling a flow rate of the dilution gas for flowing through the mixing portion; and a mean 12-1 or 12-2 or 12-3 for controlling a flow rate of the sample gas, wherein mixed gas obtained by mixing the sample with the dilution gas is introduced into the secondary ionization part and the sample is ionized.
摘要翻译：将提供用于检测低流量的样品气体中的杂质的质谱仪。一种质谱仪，包括：大气压化学电离源，其具有通过反应气体的放电产生一次离子的一次离子化部28;以及二次离子化部23，其通过所述一次反应生成该样品的离子离子和样品; 用于对生成的离子进行质谱分析的质谱部11; 混合部分33，用于将要引入二次电离部分的样品与稀释气体混合; 以及用于控制用于流过混合部分的稀释气体的流量的平均值30; 以及用于控制样品气体的流量的平均值12-1或12-2或12-3，其中通过将样品与稀释气体混合而获得的混合气体被引入二次电离部分，并且样品被离子化。

26. 发明授权

US06677582B2 Ion source and mass spectrometer 有权
标题翻译：离子源和质谱仪
公开(公告)号：US06677582B2
公开(公告)日：2004-01-13
申请号：US09941547
申请日：2001-08-30
申请人： Masuyoshi Yamada , Yasuaki Takada , Masao Suga
发明人： Masuyoshi Yamada , Yasuaki Takada , Masao Suga
IPC分类号： H01J4910
CPC分类号： H01J49/168
摘要： An apparatus for detecting the minor constituents of a sample with high efficiency in positive and negative ion monitoring modes. The directions in which the sample gas is forced to flow in the ionized region within the ion source are properly switched in the positive and negative ion monitoring modes, respectively, thereby enabling both positive ions and negative ions to be detected with high sensitivity.
摘要翻译：一种用于在正离子和负离子监测模式下以高效率检测样品的次要成分的装置。样品气体被迫在离子源内的离子化区域中流动的方向分别适当地在正离子和负离子监测模式中切换，从而能够以高灵敏度检测正离子和负离子。

27. 发明授权

US07420180B2 Mass spectrometer and mass spectrometry 有权
公开(公告)号：US07420180B2
公开(公告)日：2008-09-02
申请号：US11699366
申请日：2007-01-30
申请人： Masuyoshi Yamada , Masao Suga , Izumi Waki
发明人： Masuyoshi Yamada , Masao Suga , Izumi Waki
IPC分类号： H01J49/00 , H01J49/10
CPC分类号： H01J49/0422 , H01J49/107
摘要： A mass spectrometer capable of measuring under switching two ion sources at different pressure levels in which a sample gas separated by GC column is branched, and separately introduced to a first ion source (for example, APCI ion source) and a second ion source (for example, EI ion source) at a pressure level lower than that of the first ion source respectively. Preferably, the flow rate of the sample gas introduced to the APCI ion source is made more than the flow rate of the sample gas introduced to the EI ion source, so that the pressure for each of the ion sources can be maintained and analysis can be conducted by each ionization at a good balance in view of the sensitivity.

28. 发明申请

US20070181802A1 Mass spectrometer and mass spectrometry 有权
标题翻译：质谱仪和质谱仪
公开(公告)号：US20070181802A1
公开(公告)日：2007-08-09
申请号：US11712922
申请日：2007-03-02
申请人： Masuyoshi Yamada , Masao Suga , Izumi Waki
发明人： Masuyoshi Yamada , Masao Suga , Izumi Waki
IPC分类号： H01J49/00
CPC分类号： H01J49/0422 , H01J49/107
摘要： A mass spectrometer capable of measuring under switching two ion sources at different pressure levels in which a sample gas separated by GC column is branched, and separately introduced to a first ion source (for example, APCI ion source) and a second ion source (for example, EI ion source) at a pressure level lower than that of the first ion source respectively. Preferably, the flow rate of the sample gas introduced to the APCI ion source is made more than the flow rate of the sample gas introduced to the EI ion source, so that the pressure for each of the ion sources can be maintained and analysis can be conducted by each ionization at a good balance in view of the sensitivity.
摘要翻译：一种能够在不同压力水平下切换两个离子源的质谱仪，其中由GC柱分离的样品气体被分支，并分别引入第一离子源（例如APCI离子源）和第二离子源（用于例如，EI离子源），其压力水平分别低于第一离子源的压力水平。优选地，引入到APCI离子源的样品气体的流量比引入到EI离子源的样品气体的流量更多，从而可以保持每个离子源的压力并且可以分析鉴于敏感性，通过各种电离进行良好的平衡。

29. 发明授权

US08253097B2 Mass spectrometer and method of mass spectrometry 有权
标题翻译：质谱仪和质谱法
公开(公告)号：US08253097B2
公开(公告)日：2012-08-28
申请号：US12039762
申请日：2008-02-29
申请人： Masako Ishimaru , Masuyoshi Yamada
发明人： Masako Ishimaru , Masuyoshi Yamada
IPC分类号： H01J49/00
CPC分类号： H01J49/168 , G01N30/461 , G01N30/7213 , H01J49/147
摘要： In a mass spectrometer having ion sources capable of switching between atmospheric pressure chemical ionization and electron impact ionization, a first gas chromatography device capable of separating a sample to meet a condition suitable for atmospheric pressure chemical ionization measurement is connected to upstream of an atmospheric pressure chemical ionization ion source. Part of the sample separated by the first gas chromatography device is introduced to a second gas chromatography device by distributing a flow channel. In the second gas chromatography device, a target substance and background ingredients contained in the sample are further separated and are introduced to an electron impact ionization ion source. By separating the target substance from the background ingredients, an electron impact ionization spectrum of the target substance is obtained without an effect of the background ingredients.
摘要翻译：在具有能够在大气压化学电离和电子轰击电离之间切换的离子源的质谱仪中，能够分离样品以满足适于大气压化学电离测量的条件的第一气相色谱装置连接到大气压化学品电离离子源。通过分配流动通道将由第一气相色谱装置分离的样品的一部分引入第二气相色谱装置。在第二气相色谱装置中，将样品中所含的目标物质和背景成分进一步分离并引入电子轰击离子化离子源。通过将目标物质与背景成分分离，可以获得目标物质的电子轰击电离光谱，而不影响背景成分。

30. 发明申请

US20110204221A1 MASS SPECTROMETER AND METHOD OF MASS SPECTROMETRY 审中-公开
标题翻译：质谱仪和质谱法
公开(公告)号：US20110204221A1
公开(公告)日：2011-08-25
申请号：US13122418
申请日：2009-10-08
申请人： Hiroyuki Satake , Masuyoshi Yamada
发明人： Hiroyuki Satake , Masuyoshi Yamada
IPC分类号： H01J49/26 , H01J49/40
CPC分类号： H01J49/063 , H01J49/0031 , H01J49/004 , H01J49/0054 , H01J49/0072
摘要： When a high-speed analyzer such as a quadrupole mass filter is united with an analyzer which requires a reaction time of 10 msec, such as an ion dissociation chamber of the ion trap type, a problem arises that an ion loss occurs due to a difference in analysis speed between the analyzers. A high-throughput analysis is intended to be achieved by eliminating this loss. A pre ion trap (4) is provided between a quadrupole filter (3) and an ion dissociation chamber (5), and ions are accumulated in the pre ion trap (4) while operations such as dissociation, isolation and ejection are being performed in the ion dissociation chamber (5). This configuration solves a problem with the ion dissociation chamber (5), which is a decrease in transmittance of the dissociation chamber (5), i.e., a decrease in throughput, and accordingly enables a high-throughput structural analysis on a measurement sample.
摘要翻译：当将诸如四极质量过滤器的高速分析仪与需要10毫秒的反应时间的分析仪（例如离子阱型离子解离室）结合在一起时，会产生由于差异而产生离子损失的问题在分析仪之间的分析速度。旨在通过消除这种损失来实现高通量分析。在四极过滤器（3）和离子解离室（5）之间提供预离子阱（4），并且离子聚集在预离子阱（4）中，同时在诸如解离，分离和喷射之类的操作中进行离子解离室（5）。这种结构解决了离子解离室（5）的问题，离子解离室（5）是解离室（5）的透射率降低，即通过量的降低，因此能够对测量样品进行高通量结构分析。

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