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21. 发明授权

US06251351B1 Wet-process technique for refining phosphoric acid 有权
标题翻译：湿法精制磷酸技术
公开(公告)号：US06251351B1
公开(公告)日：2001-06-26
申请号：US09155448
申请日：1999-08-20
申请人： Istvan Potencsik , Alexander Maurer
发明人： Istvan Potencsik , Alexander Maurer
IPC分类号： C01B2516
CPC分类号： C01B25/46
摘要： A process for purification by multistage countercurrent extraction of wet-process phosphoric acid includes the steps of (a) preparing an aqueous phosphoric acid by decomposition of crude phosphates with sulfuric acid and prepurification thereof; (b) providing an organic solvent mixture consisting of one of (A) a water immiscible solvent and a fully water-miscible solvent or (B) a partially water-miscible solvent and a fully water-miscible solvent; (c) extracting water from the acid by contacting with the solvent mixture in a volumetric ratio of acid to solvent mixture of 1:1 to 1:10 at a temperature of 5 to 90° C.; (d) recovering the fully water-miscible solvent by distillation and washing; (e) recycling the fully water-miscible solvent to step (b) to provide a recycled solvent mixture; and (f) repeating steps (c), (d) and (e) with the recycled solvent mixture to provide a phosphoric acid having a preselected degree of purity.
摘要翻译：一种通过湿法磷酸的多级逆流提取进行纯化的方法包括以下步骤：（a）通过用硫酸分解粗制磷酸盐并预纯化制备磷酸水溶液; （b）提供由（A）与水不混溶的溶剂和完全与水混溶的溶剂之一组成的有机溶剂混合物或（B）部分水混溶性溶剂和完全与水混溶的溶剂; （c）在5至90℃的温度下，以1:1至1:10的体积比的酸与溶剂混合物与溶剂混合物接触，从酸中提取水; （d）通过蒸馏和洗涤回收完全与水混溶的溶剂; （e）将完全与水混溶的溶剂再循环到步骤（b）以提供循环的溶剂混合物; 和（f）用再循环的溶剂混合物重复步骤（c），（d）和（e），以提供具有预选纯度的磷酸。

22. 发明授权

US5338524A Process for the production of coarse-grained, anhydrous calcium monohydrogen phosphate (dicalcium phosphate anhydride) and a device for carrying out the process 失效
标题翻译：生产粗粒度，无水磷酸氢钙（磷酸二钙酐）的方法和用于进行该方法的装置
公开(公告)号：US5338524A
公开(公告)日：1994-08-16
申请号：US997368
申请日：1992-12-23
申请人： Alexander Maurer , Guenter Raab , Gudrun Raab , Hans-Georg Steinert , Richard Taenzler
发明人： Alexander Maurer , Guenter Raab , Gudrun Raab , Hans-Georg Steinert , Richard Taenzler
IPC分类号： A61K8/00 , A61K8/24 , A61Q11/00 , C01B25/32
CPC分类号： C01B25/322
摘要： The present invention provides a process and apparatus for the production of coarse-grained dicalcium phosphate anhydride, at least 95% of which consists of particles with a grain diameter of >45 .mu.m, wherein, at a temperature of 60.degree. to 100.degree. C., a highly reactive calcium component, for example freshly slaked milk of lime or an aqueous slurry or suspension of calcium hydroxide and/or calcium carbonate, is introduced directly into the stirrer zones of a vessel containing aqueous phosphoric acid and having one or more turbulent stirrer zones. An equivalent amount of aqueous phosphoric acid is introduced into another zone of the vessel, the speed of introduction being so regulated that a pH value of 3.0 to 4.5 is obtained in the stirrer zone and the whole batch or a continuously or semi-continuously removed part thereof is cooled to 40.degree. to 60.degree. C. The removed part then is mixed with an additional calcium component, for example milk of lime, to obtain a pH value of from 5.5 to 6.8, the mixture further stirred for 10 to 60 minutes and the resultant course-grained dicalcium phosphate anhydride is filtered off and dried.
摘要翻译：本发明提供了一种生产粗粒磷酸二钙酸酐的方法和装置，其中至少95％由粒径>45μm的颗粒组成，其中在60℃至100℃的温度下将高活性钙组分，例如石灰的新鲜熟化的牛奶或氢氧化钙和/或碳酸钙的水性浆料或悬浮液直接引入含有磷酸水溶液的容器的搅拌器区域中并具有一个或多个湍流搅拌区。将等量的磷酸水溶液引入到容器的另一区域中，引入速度被调节到在搅拌器区域和整个批料中获得3.0至4.5的pH值，或者连续或半连续地除去部分将其除去与另外的钙成分（例如石灰乳）混合，得到5.5〜6.8的pH值，进一步搅拌10〜60分钟，将所得的过程粒度的磷酸二钙酸酐滤出并干燥。

23. 发明授权

US4399114A Process for the dearsenification of polyphosphoric acid 失效
标题翻译：多磷酸脱砷方法
公开(公告)号：US4399114A
公开(公告)日：1983-08-16
申请号：US402941
申请日：1982-07-29
申请人： Alexander Maurer , Gero Heymer , Markus Erpenbach
发明人： Alexander Maurer , Gero Heymer , Markus Erpenbach
IPC分类号： C01B25/24 , C01B25/16
CPC分类号： C01B25/24
摘要： The disclosure relates to a process for the continuous dearsenification of polyphosphoric acid with the aid of hydrogen sulfide in a gas admission zone. To this end, the disclosure provides for the acid to be dearsenified in a gas admission zone subdivided so as to comprise at least two separate liquid matter-receiving zones, each zone being separated from the other by means of a separate gas zone; for the liquid in each of the liquid matter-receiving zones to be maintained at a level 0.1 up to 10 cm high, without admission of gas; for hydrogen sulfide which remained unreacted in the individual liquid matter-receiving zones to be collected in the respective gas zone and for it to be finely redispersed in the liquid matter-receiving zone directly upstream of the respective gas zone by allowing the hydrogen sulfide to flow through a plurality of openings into the acid, the latter being delivered from the respective liquid-matter-receiving zone into the next downstream liquid-matter-receiving zone, and introduced thereinto directly below the liquid matter level therein; for precipitated arsenic sulfide to be separated from the acid coming from the lower end of the gas admission zone, and for the filtrate obtained to be freed from gaseous hydrogen sulfide in excess.
摘要翻译：本公开涉及在气体入口区借助硫化氢连续脱砷多磷酸的方法。为此，本公开内容提供了在气体进入区域中进行脱砷的酸，其被细分为包括至少两个分离的液体物质接收区域，每个区域通过单独的气体区域与另一个区域分离; 使每个液体物质接收区域中的液体保持在0.1至10厘米高的水平，而不允许气体; 对于在各个液体物质接收区中保持未反应的硫化氢，其被收集在各个气体区中，并且通过允许硫化氢流动直接在各个气体区的上游被精细地再分散在液体物质接收区中通过多个开口进入酸，后者从相应的液体接收区输送到下一个下游液体接收区，并直接在其中引入液体物质的下方; 使沉淀的硫化砷与气体入口区的下端的酸分离，得到的过滤得到的无水硫化氢的滤液。

24. 发明授权

US4394358A Production of granular alkali metal diphosphates or triphosphates 失效
标题翻译：生产颗粒状碱金属二磷酸盐或三磷酸盐
公开(公告)号：US4394358A
公开(公告)日：1983-07-19
申请号：US303100
申请日：1981-09-17
申请人： Alexander Maurer , Renate Adrian , Herbert Panter , Gero Heymer , Dieter Nolker
发明人： Alexander Maurer , Renate Adrian , Herbert Panter , Gero Heymer , Dieter Nolker
IPC分类号： C01B25/41 , C01B25/42 , C11D3/06 , C01B25/30
CPC分类号： C01B25/418 , C01B25/425 , C11D3/062
摘要： The invention relates to a process for making granulated, partially or completely hydrated alkali metal diphosphates or triphosphates. To this end, the invention provides for alkali metal diphosphates or triphosphates which consist to an extent of at least 20% of particles with a size of less than 0.045 mm and are hydrated to an extent of less than 90%, based on the phosphates' theoretical content of water of hydration, to be intensively mixed and granulated in the presence of water and an ammonium polyphosphate, this latter being used in a proportion of about 0.5 to 50 weight %, based on the quantity of water used.
摘要翻译：本发明涉及制备颗粒状，部分或完全水合的碱金属二磷酸盐或三磷酸盐的方法。为此，本发明提供碱金属二磷酸盐或三磷酸盐，其碱度至少为20％，其尺寸小于0.045mm，并且基于磷酸盐的水合物水合至小于90％的程度，在水和多磷酸铵的存在下，水合的水的理论含量将被浓缩混合和造粒，后者基于所用的水量以约0.5至50重量％的比例使用。

25. 发明授权

US4386024A Granulate of alkali metal aluminum silicate and pentasodium tripolyphosphate, and process for making it 失效
标题翻译：碱金属硅酸铝和三聚磷酸三钠的颗粒，以及其制备方法
公开(公告)号：US4386024A
公开(公告)日：1983-05-31
申请号：US358388
申请日：1982-03-15
申请人： Alexander Maurer , Renate Adrian , Horst-Dieter Wasel-Nielen , Gunter Sorbe , Joachim Kandler
发明人： Alexander Maurer , Renate Adrian , Horst-Dieter Wasel-Nielen , Gunter Sorbe , Joachim Kandler
IPC分类号： C11D3/06 , C11D3/12 , B01J39/14 , C02F1/42 , C11D7/16
CPC分类号： C11D3/06 , C11D3/128
摘要： The disclosure relates to a granulate with a particle size essentially of about 0.2 to 2 mm consisting of(a) about 2 to 95 weight % of a partially or completely hydrated pentasodium tripolyphosphate,(b) less than 3 weight % of an ammonium polyphosphate and the balance(c) being in the form of a water-insoluble aluminum silicate ion exchanging material.The granulate can be used in detergents.
摘要翻译：本公开内容涉及粒径基本上为约0.2至2mm的颗粒，其由（a）约2至95重量％的部分或完全水合的三聚磷酸三钠组成，（b）少于3重量％的多磷酸铵和余量（c）为水不溶性硅酸铝离子交换材料的形式。颗粒可用于洗涤剂。

26. 发明授权

US4294808A Production of anticorrosive pigments containing phosphorus 失效
标题翻译：生产含磷的防锈颜料
公开(公告)号：US4294808A
公开(公告)日：1981-10-13
申请号：US76307
申请日：1979-09-17
申请人： Horst-Dieter Wasel-Nielen , Renate Adrian , Herbert Panter , Gero Heymer , Alexander Maurer , Raban von Schenck
发明人： Horst-Dieter Wasel-Nielen , Renate Adrian , Herbert Panter , Gero Heymer , Alexander Maurer , Raban von Schenck
IPC分类号： C23C22/08 , C01B25/163 , C01B25/165 , C01B25/26 , C01B25/32 , C01B25/34 , C01B25/37 , C09D5/08 , C01B25/36
CPC分类号： C09D5/084 , C01B25/163 , C01B25/165 , C01B25/265 , C01B25/325 , C01B25/34 , C01B25/37
摘要： The invention relates to a process for making phosphorus-containing anticorrosive pigments having a size of at most 20 microns by reacting one or more compounds of magnesium, calcium, strontium, barium, zinc, aluminum, iron, chromium or manganese with an oxygen acid of phosphorus or its alkali metal or ammonium salts at temperatures within the range 10.degree. to 100.degree. C. More particularly pigments consisting to an extent of at least 90% of particles with a size between 0.05 and 8 microns are produced by introducing an aqueous suspension or solution of the reactants into a dispersing means rotating at a speed of 3000 to 10,000 rpm, reacting the reactants by intimately mixing them, and separating and drying precipitated pigment.
摘要翻译：本发明涉及一种通过使一种或多种镁，钙，锶，钡，锌，铝，铁，铬或锰的化合物与氧酸的氧酸反应制备尺寸至多为20微米的含磷防腐颜料的方法磷或其碱金属或铵盐。更具体地说，通过将水性悬浮液或水溶性悬浮液引入至少90％的尺寸为0.05至8微米的颗粒的程度，将反应物溶解在以3000至10,000rpm的速度旋转的分散装置中，通过将它们紧密混合使反应物反应，并分离和干燥沉淀的颜料。

27. 发明授权

US4294621A Production of an anticorrosive pigment on phosphate basis 失效
标题翻译：以磷酸盐为基础生产防腐颜料
公开(公告)号：US4294621A
公开(公告)日：1981-10-13
申请号：US141135
申请日：1980-04-16
申请人： Alexander Maurer , Renate Adrian , Klaus Hestermann , Gero Heymer
发明人： Alexander Maurer , Renate Adrian , Klaus Hestermann , Gero Heymer
IPC分类号： C09D5/08 , C01B25/32 , C09C1/00 , C09C1/02 , C08K3/10
CPC分类号： C01B25/322 , C01B25/325 , C09C1/02 , C01P2004/61 , C01P2006/12
摘要： The invention relates to the production of phosphorus-containing anticorrosive pigments with a particle size of at most 20 microns by reacting one or more calcium or magnesium compounds with phosphoric acid or acid alkali metal or ammonium phosphates by intimately mixing an aqueous suspension or solution of the reactants inside a dispersing means rotating at a speed of 3000 to 10,000 rpm. More particularly, fine pulverulent calcium and magnesium compounds are converted, with agitation, together with water and, if desired, a water-soluble alkanol to a homogeneous suspension or solution. The suspension or solution is intimately mixed, inside the dispersing means at 0.degree. to 40.degree. C. and in an approximately stoichiometric ratio, with the phosphoric acid or acid phosphate solution. Resulting and precipitated pigment is separated and dried under mild conditions while maintaining its content of water of crystallization. The anticorrosive pigment is comprised of a homogeneous mixture and/or mixed crystals of which 10 to 95 mol % is calcium hydrogen phosphate dihydrate, the balance being magnesium hydrogen phosphate trihydrate. An at least 55 weight % proportion consists of particles with a size of up to 5 microns with a BET-surface of at least 1 m.sup.2 /g.
摘要翻译：本发明涉及通过使一种或多种钙或镁化合物与磷酸或酸性碱金属或铵磷酸盐反应，通过将下列物质的水性悬浮液或溶液紧密混合，从而生产粒径至多为20微米的含磷防腐颜料分散装置内的反应物以3000至10,000rpm的速度旋转。更具体地，精细的粉末状钙和镁化合物在搅拌下与水一起转化，如果需要，将水溶性链烷醇转化成均匀的悬浮液或溶液。悬浮液或溶液在分散装置内在0℃至40℃下以大约化学计量比与磷酸或酸式磷酸盐溶液紧密混合。将所得沉淀的颜料分离并在温和条件下干燥，同时保持其结晶水含量。防腐颜料由均匀的混合物和/或其中10〜95摩尔％为磷酸氢钙二水合物的混合晶体组成，余量为磷酸氢二氢钙三水合物。至少55重量％的比例由尺寸高达5微米，BET表面至少为1m 2 / g的颗粒组成。

28. 发明申请

US20110137400A1 STENT DEVICE DELIVERY SYSTEM WITH A VARYING RADIAL PROFILE PULL MEMBER 有权
标题翻译：具有变化的径向轮廓牵引构件的STENT设备传送系统
公开(公告)号：US20110137400A1
公开(公告)日：2011-06-09
申请号：US12958123
申请日：2010-12-01
申请人： Jürgen Dorn , Markus Forster , Daniel Dietrich , Alexander Maurer , Erhard Elsasser
发明人： Jürgen Dorn , Markus Forster , Daniel Dietrich , Alexander Maurer , Erhard Elsasser
IPC分类号： A61F2/82 , B65B11/50
CPC分类号： A61F2/95 , A61F2/966 , A61F2210/0076 , A61F2240/001
摘要： A stent device delivery system and method of making. The stent device delivery system includes a stent device, an outer sheath overlaying the stent device in a radially compact, delivery configuration of the stent device, and a pull member. The outer sheath may include a first layer and a reinforcement layer that are laminated together, a portion of the pull member captured radially between the first layer and the reinforcement layer. At least a partial length of the captured portion of the pull member may be formed with a varying radial profile.
摘要翻译：支架装置输送系统及其制造方法。支架装置递送系统包括支架装置，以支架装置的径向紧凑的输送构造覆盖支架装置的外护套和拉构件。外护套可以包括层压在一起的第一层和加强层，拉动构件的一部分径向地捕获在第一层和加强层之间。牵引构件的捕获部分的至少一部分长度可以形成为具有变化的径向轮廓。

29. 发明授权

US5405436A Process for the preparation of hydroxyapatite 失效
标题翻译：制备羟基磷灰石的方法
公开(公告)号：US5405436A
公开(公告)日：1995-04-11
申请号：US126969
申请日：1993-09-27
申请人： Alexander Maurer , Gudrun Raab , Guenter Raab , Reinhold Schmitt , Detlev Schober , Richard Taenzler
发明人： Alexander Maurer , Gudrun Raab , Guenter Raab , Reinhold Schmitt , Detlev Schober , Richard Taenzler
IPC分类号： A61K8/00 , A61K8/24 , A61Q11/00 , C01B25/32 , D06P1/649 , D06P3/52 , D06P3/54 , A61K7/16
CPC分类号： D06P3/54 , A61K8/24 , A61Q11/00 , C01B25/322 , D06P1/6491 , D06P3/523
摘要： A process for the preparation of a hydroxyapatite, which is suitable as a tooth-cleaning substance, by precipitation from aqueous phosphoric acid and calcium hydroxide solution, in which a calcium-doped phosphoric acid solution is fed to an intensive mixer with a suspension of calcium hydroxide/oxide in a molar ratio of Ca:P=1.667 corresponding to the hydroxyapatite of and reacted there at precipitation temperatures of 60.degree.-100.degree. C., preferably 80.degree.-90.degree. C. and a pH of 4-8, preferably of 6.5-7.5. Also disclosed in a tooth-cleaning substance containing the hydroxyapatite.
摘要翻译：通过从磷酸水溶液和氢氧化钙水溶液中沉淀制备适合作为牙齿清洁物质的羟基磷灰石的方法，其中将掺入磷酸的磷酸溶液加入到具有钙悬浮液的浓缩混合器中氢氧化物/氧化物，其摩尔比为：对应于羟基磷灰石的Ca：P = 1.667，在60℃-100℃，优选80-90℃的沉淀温度和4-8℃的pH下反应为6.5-7.5。还公开在含有羟基磷灰石的牙齿清洁物质中。

30. 发明授权

US5198088A Apparatus for the preparation of alkali metal monofluorhosphates 失效
标题翻译：用于制备碱金属单氟磷酸盐的装置
公开(公告)号：US5198088A
公开(公告)日：1993-03-30
申请号：US640797
申请日：1991-01-16
申请人： Armin Etzel , Richard Taenzler , Alexander Maurer , Gerhard Schoenmann , Hans-Georg Steinert
发明人： Armin Etzel , Richard Taenzler , Alexander Maurer , Gerhard Schoenmann , Hans-Georg Steinert
IPC分类号： B01J6/00 , C01B25/455
CPC分类号： C01B25/455 , B01J6/007
摘要： An apparatus for the preparation of alkali metal monofluorophosphates is disclosed. The apparatus includes a melting crucible of a platinum/rhodium alloy, devices for feeding the alkali metal fluoride and alkali metal metaphosphate or alkali metal polyphosphate raw materials into the upper part of the crucible, an outflow orifice for molten alkali metal fluorophosphate in the bottom of the crucible, a corresponding discharge orifice in the furnace, and a cooling arrangement, wherein a direct voltage is applied between the cooling arrangement and the melting crucible which is connected as the anode.
摘要翻译：公开了一种制备碱金属单氟磷酸盐的装置。该装置包括铂/铑合金的熔化坩埚，用于将碱金属氟化物和碱金属偏磷酸盐或碱金属多磷酸盐原料供给到坩埚的上部的装置，在坩埚的上部的熔融碱金属氟磷酸盐的流出孔坩埚，炉内的相应的排放孔以及冷却装置，其中在冷却装置和作为阳极连接的熔化坩埚之间施加直流电压。

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