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11. 发明授权

US3661635A Dual-etched refractory metallizing 失效
$Dual-etched refractory metallizing$
标题翻译：双重烧蚀金属化
公开(公告)号：US3661635A
公开(公告)日：1972-05-09
申请号：US3661635D
申请日：1970-02-20
申请人： AMERICAN LAVA CORP
发明人： HARRISON HENRY F
IPC分类号： C04B41/51 , C04B41/88 , H01L21/70 , H05K1/09 , H05K3/02 , H05K3/06 , H05K3/04
CPC分类号： C04B41/009 , C04B41/5133 , C04B41/5138 , C04B41/88 , H01L21/705 , H05K1/092 , H05K3/02 , H05K3/064 , H05K2203/025 , Y10T428/24802 , Y10T428/24851 , Y10T428/24917 , Y10T428/24926 , C04B41/4505 , C04B41/4572 , C04B41/53 , C04B35/00
摘要： A process for metallizing on ceramic substrates with fine detail patterns of refractory metal which includes a prefiring to effect oxidation of a portion of the metallizing coating, application of a photopolymerizable coating thereover followed by exposure in pattern form using a mask, removal of unpolymerized coating by conventional means, acid etching to remove the oxides formed during pre-firing in exposed portions of the metallizing coating and mechanical removal of unoxidized and unsintered metal remaining in etched portions. This is followed by a final firing which destroys the photoresist and sinters the metal remaining on the substrate.
摘要翻译：一种用于在陶瓷基片上金属化的难熔金属的精细细节图案的方法，其包括预先实现金属化涂层的一部分的氧化，在其上施加可光聚合涂层，然后使用掩模以图案形式曝光，通过使用掩模去除未聚合的涂层常规方法，酸蚀刻以除去在金属化涂层的暴露部分中预焙烧期间形成的氧化物，并机械去除残留在蚀刻部分中的未氧化和未烧结的金属。之后是最终的烧制，其破坏光致抗蚀剂并烧结剩余在基底上的金属。

12. 发明授权

US3661595A Composition for metalizing ceramic 失效
标题翻译：用于金属化陶瓷的组合物
公开(公告)号：US3661595A
公开(公告)日：1972-05-09
申请号：US3661595D
申请日：1970-02-16
申请人： COORS PORCELAIN CO
发明人： BUCK ROBERT W
IPC分类号： C04B41/51 , C09D5/38 , H01C17/065 , H05K1/09 , C09D5/24
CPC分类号： H01C17/0656 , C04B41/5138 , C04B41/5183 , C09D5/38 , H05K1/092
摘要： The subject matter of this invention is a composition and method for metalizing ceramic wherein the composition is a mixture containing manganese, molybdenum and silicon, at least a portion of the latter being present as molybdenum disilicide or tungsten disilicide, molybdenum disilicide being much preferred. The mixture, in powdered form, is suspended in an organic vehicle to provide a slurry which is coated onto the ceramic after which the ceramic is fired in a wet reducing atmosphere to a temperature of about 1150* C to 1450* C, the organic vehicle vaporizing during the initial phase of the firing operation. By inclusion of the disilicide in the mixture an improved metalized surface on the ceramic can be accomplished using relatively a low firing temperature.
摘要翻译：本发明的主题是用于金属化陶瓷的组合物和方法，其中组合物是含有锰，钼和硅的混合物，其中至少一部分作为二硅化钼或二硅化钨存在，二硅化钼是非常优选的。将粉末状混合物悬浮在有机载体中以提供涂覆在陶瓷上的浆料，然后将陶瓷在湿还原气氛中焙烧至约1150℃至1450℃的温度，有机载体在点火操作的初始阶段期间汽化。通过在混合物中包含二硅化物，可以使用相对低的烧制温度来实现陶瓷上改进的金属化表面。

13. 发明授权

US3619233A Method of metallizing a ceramic member 失效
标题翻译：陶瓷成员金属化方法
公开(公告)号：US3619233A
公开(公告)日：1971-11-09
申请号：US3619233D
申请日：1969-03-06
申请人： GLOBE UNION INC
发明人： HIPP JULIUS CARL , SCHMIDT JAMES ARTHUR
IPC分类号： C04B41/51 , C04B41/52 , C04B41/88 , C04B41/89 , H05K1/09 , H05K3/10 , B44D1/16 , C03C17/08
CPC分类号： C04B41/009 , C04B41/5138 , C04B41/52 , C04B41/88 , C04B41/89 , H05K1/092 , H05K3/105 , C04B41/0072 , C04B41/4539 , C04B41/455 , C04B41/5133 , C04B41/5111 , C04B41/4505 , C04B41/5105 , C04B35/00
摘要： A thick, solderable metallic coating is provided on a ceramic member by applying a metallic composition comprised of at least 10 weight percent, preferably at least 30 weight percent, of powdered molybdenum trioxide, or tungsten trioxide, or mixtures thereof, and at least 30 weight percent of powdered gold, or copper, or silver, or alloys thereof, on the surface of the member and then firing the coated member in a wet reducing atmosphere at a temperature above the melting point of the solderable material to substantially reduce the molybdenum trioxide and/or tungsten trioxide to the metallic form. In one embodiment, the molybdenum trioxide and/or tungsten trioxide is applied to the surface of the ceramic member first and gold, copper, silver, or alloys thereof, is then applied over this first coating. In another embodiment, the metallic composition is applied to the ceramic member as an admixture.

14. 发明授权

US3226822A Art of bonding ceramic to metal 失效
标题翻译：将陶瓷与金属结合的艺术
公开(公告)号：US3226822A
公开(公告)日：1966-01-04
申请号：US14110061
申请日：1961-09-27
申请人： EITEL MCCULLOUGH INC
发明人： BUDDE MILTON C , ZUMAQUERO FRANK J
IPC分类号： B23K35/30 , C04B37/02 , C04B41/52 , C04B41/89
CPC分类号： C04B41/009 , B23K35/302 , C04B37/026 , C04B41/52 , C04B41/89 , C04B2235/6567 , C04B2235/6582 , C04B2235/6588 , C04B2237/12 , C04B2237/122 , C04B2237/126 , C04B2237/16 , C04B2237/34 , C04B2237/343 , C04B2237/406 , C04B2237/407 , C04B2237/72 , C04B2237/765 , C04B2237/88 , Y10T428/12611 , Y10T428/12812 , Y10T428/1291 , C04B41/5133 , C04B41/5138 , C04B41/5127 , C04B35/00

15. 发明授权

US2904456A Metalizing ceramics 失效
标题翻译：金属化陶瓷
公开(公告)号：US2904456A
公开(公告)日：1959-09-15
申请号：US58466456
申请日：1956-05-14
申请人： GEN ELECTRIC
发明人： NOLTE HENRY J
IPC分类号： C04B41/51 , C04B41/88 , H01B1/00 , H05K1/09
CPC分类号： C04B41/009 , C04B41/5138 , C04B41/88 , H01B1/00 , H05K1/092 , C04B35/00

17. 发明申请

US20180222807A1 INCREASING THE DENSITY OF A BOND COAT 审中-公开
公开(公告)号：US20180222807A1
公开(公告)日：2018-08-09
申请号：US15878970
申请日：2018-01-24
申请人： Rolls-Royce Corporation , Rolls-Royce High Temperature Composites, Inc.
发明人： Sungbo Shim , Robert Shinavski , Ann Bolcavage
IPC分类号： C04B41/45 , C04B41/00 , C04B41/50 , C04B41/51 , C04B41/52 , C04B41/87 , C04B41/88 , C23C4/134 , C23C4/04 , B05D1/18 , B05D3/02 , C23C4/126
CPC分类号： C04B41/456 , B05D1/18 , B05D3/0254 , C04B41/009 , C04B41/4554 , C04B41/5001 , C04B41/5024 , C04B41/5059 , C04B41/5133 , C04B41/5138 , C04B41/52 , C04B41/87 , C04B41/88 , C04B41/89 , C23C4/04 , C23C4/126 , C23C4/134 , C23C4/18 , F01D5/288 , F05D2230/312 , F05D2230/90 , F05D2300/222 , F05D2300/6033 , C04B35/80 , C04B35/565 , C04B35/806 , C04B35/584 , C04B41/4527 , C04B41/4582 , C04B41/5096 , C04B41/4519 , C04B41/4535 , C04B41/455 , C04B41/4517 , C04B41/4558 , C04B41/522 , C04B41/4537 , C04B41/5031 , C04B41/5035 , C04B41/5023 , C04B41/5037 , C04B41/5045
摘要： An example method may include applying a bond coat comprising silicon or a silicon alloy on a surface of a ceramic or ceramic matrix composite substrate, where the bond coat comprises a plurality of pores; infiltrating a precursor into at least some pores of the plurality of pores; and heat-treating the bond coat and the precursor, where after heat-treating a porosity of the bond coat is less than about 5 vol. %, and where after heat-treating, the bond coat is substantially free of continuous porosity extending through a thickness of the bond coat.

18. 发明申请

US20160137559A1 COMPLIANT LAYER FOR CERAMIC COMPONENTS AND METHODS OF FORMING THE SAME 有权
标题翻译：陶瓷组件的合适层及其形成方法
公开(公告)号：US20160137559A1
公开(公告)日：2016-05-19
申请号：US14205010
申请日：2014-03-11
申请人： Rolls-Royce Corporation
发明人： Adam Lee Chamberlain , Kang N. Lee , Andrew Joseph Lazur
IPC分类号： C04B41/51 , C04B41/00 , F01D5/30 , C04B41/89 , F01D5/28 , C04B41/88 , C04B41/52
CPC分类号： C23C30/00 , C04B35/71 , C04B41/009 , C04B41/5105 , C04B41/5133 , C04B41/5138 , C04B41/5144 , C04B41/5155 , C04B41/52 , C04B41/522 , C04B41/88 , C04B41/89 , C04B41/90 , F01D5/282 , F01D5/284 , F01D5/288 , F01D5/3007 , F05D2220/30 , F05D2220/32 , F05D2230/90 , F05D2240/30 , F05D2300/10 , F05D2300/6033 , C04B35/565 , C04B35/806 , C04B35/584 , C04B35/10 , C04B35/803 , C04B35/18 , C04B41/5096 , C04B41/5094 , C04B41/5161 , C04B41/5116 , C04B41/5122 , C04B41/5127 , C04B41/5024 , C04B41/5037
摘要： An apparatus includes a ceramic matrix composite (CMC) component and an interface coating on the CMC component, wherein the interface coating includes a layer of at least one of the following compositions: 100 wt % Ir; 90-95 wt % Ir, 5-10 wt % Co, 1-2 wt % Al, 1-2 wt % Si; 40-50 wt % Nb, 28-42 wt % Al, 4-15 wt % Cr, 1-2 wt % Si; 90-92 wt % Mo, 4-5 wt % Si, 4-5 wt % B; or 60-80 wt % V, 20-30 wt % Cr, 2-15 wt % Ti.
摘要翻译：一种装置包括陶瓷基质复合材料（CMC）组分和在CMC组分上的界面涂层，其中界面涂层包括以下组合物中的至少一种：100wt％Ir; 90-95wt％Ir，5-10wt％Co，1-2wt％Al，1-2wt％Si; 40-50重量％的Nb，28-42重量％的Al，4-15重量％的Cr，1-2重量％的Si; 90-92wt％Mo，4-5wt％Si，4-5wt％B; 或60-80重量％V，20-30重量％Cr，2-15重量％Ti。

19. 发明授权

US5529852A Aluminum nitride sintered body having a metallized coating layer on its surface 失效
标题翻译：其表面具有金属化涂层的氮化铝烧结体
公开(公告)号：US5529852A
公开(公告)日：1996-06-25
申请号：US206885
申请日：1994-03-07
申请人： Akira Sasame , Hitoyuki Sakanoue
发明人： Akira Sasame , Hitoyuki Sakanoue
IPC分类号： C04B41/51 , C04B41/88 , H01L21/48 , H01L23/15 , H01L23/498 , H01L33/64 , H05K1/09 , C01G41/00 , C22C38/12
CPC分类号： H01L33/641 , C04B41/5133 , C04B41/5138 , C04B41/88 , H01L21/4867 , H01L23/15 , H01L23/49883 , H01L24/29 , H01L24/31 , H01L24/49 , H01L2224/45015 , H01L2224/45144 , H01L2224/48091 , H01L2224/49 , H01L2224/73265 , H01L2224/83805 , H01L24/45 , H01L24/48 , H01L2924/01005 , H01L2924/01006 , H01L2924/01007 , H01L2924/01013 , H01L2924/01014 , H01L2924/01015 , H01L2924/01018 , H01L2924/01019 , H01L2924/0102 , H01L2924/01022 , H01L2924/01025 , H01L2924/01027 , H01L2924/01028 , H01L2924/01029 , H01L2924/01033 , H01L2924/01039 , H01L2924/01042 , H01L2924/01047 , H01L2924/01074 , H01L2924/01077 , H01L2924/01078 , H01L2924/01079 , H01L2924/01082 , H01L2924/0132 , H01L2924/01322 , H01L2924/0133 , H01L2924/014 , H01L2924/12041 , H01L2924/12042 , H01L2924/1306 , H01L2924/14 , H01L2924/15747 , H01L2924/19041 , H01L2924/19043 , H01L2924/19107 , H05K1/092
摘要： An aluminum nitride sintered body has a metallized layer on its surface. The metallized layer contains tungsten, aluminum oxide and calcium oxide. Preferably, the metallized layer contains 40 to 96 percent by weight of a metal, 0.4 to 25 percent by weight of an aluminum oxide and 3 to 35 percent by weight of calcium oxide. In a method of forming a metallized layer on the surface of the aluminum nitride sintered body, such body is first formed by firing. Then, a metal paste of tungsten containing powder of calcium oxide and powder of aluminum oxide is provided. The metal paste is coated on the surface of the aluminum nitride sintered body which is then fired with the metal paste in an inert atmosphere.
摘要翻译：氮化铝烧结体的表面具有金属化层。金属化层包含钨，氧化铝和氧化钙。优选地，金属化层包含40至96重量％的金属，0.4至25重量％的氧化铝和3至35重量％的氧化钙。在氮化铝烧结体的表面上形成金属化层的方法中，首先通过烧成来形成这种体。然后，提供含有氧化钙粉末和氧化铝粉末的钨的金属膏。将金属膏涂覆在氮化铝烧结体的表面上，然后在惰性气氛中用金属膏烧制。

20. 发明授权

US5045400A Composition for and method of metallizing ceramic surface, and surface-metallized ceramic article 失效
标题翻译：金属化陶瓷表面的组成和方法以及表面金属化陶瓷制品
公开(公告)号：US5045400A
公开(公告)日：1991-09-03
申请号：US473326
申请日：1990-02-01
申请人： Kiyoyuki Esashi
发明人： Kiyoyuki Esashi
IPC分类号： C04B41/51 , C04B41/88 , C22C27/04 , H05K1/09
CPC分类号： C04B41/009 , C04B41/5138 , C04B41/88 , C22C27/04 , H05K1/092 , Y10T428/12493 , Y10T428/12576
摘要： Disclosed is a composition for metallizing a ceramic surface which consists essentially of 10.0 to 32.5% by weight of Mn, 45.0 to 67.5% by weight of W, up to 5.0% by weight of at least one member selected from Ti and Zr, and Ag and Ni in a total amount of 15.0 to 35.0% by weight, the amount of Ni being 5.0 to 20.0% by weight of the total amount of Ni and Ag. This composition is applied to the surface of a ceramic body in the form of a metal paste or metal powder and heat-fusion-bonded to the ceramic surface, or the composition is applied to the surface of a ceramic body by the gas-phase deposition method.
摘要翻译：公开了一种用于金属化陶瓷表面的组合物，其基本上由10.0至32.5重量％的Mn，45.0至67.5重量％的W，至多5.0重量％的选自Ti和Zr的至少一种和Ag和和Ni的总量为15.0〜35.0重量％，Ni的量为Ni和Ag的总量的5.0〜20.0重量％。将该组合物以金属糊或金属粉末的形式施加到陶瓷体的表面，并与陶瓷表面热熔接合，或者通过气相沉积将组合物施加到陶瓷体的表面方法。

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