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    • 14. 发明授权
    • Alkyl percarbonates
    • 烷基过碳酸酯
    • US4584142A
    • 1986-04-22
    • US548373
    • 1983-11-03
    • Robert H. TangJames A. Barter
    • Robert H. TangJames A. Barter
    • C07C409/34C08F299/04C07C179/15
    • C08F299/045C07C409/32
    • Organic peroxydicarbonates represented by the following graphic formula are described. ##STR1## In the formula, R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are each independently selected from an alkyl group containing from 1 to 4 carbon atoms. R.sub.1 and R.sub.2 and/or R.sub.3 and R.sub.4 can participate in a cycloalkyl group having from 3 to 6 carbon atoms. The peroxydicarbonates are useful as initiators for the polymerization or copolymerization of ethylenically unsaturated monomers or the cross-linking of unsaturated polyester resins. The organic peroxydicarbonates can be used in combination with commercially available peroxydicarbonates, particularly those having a longer half-life, or with peresters, diacylperoxides and azo compounds.
    • 描述由以下图形公式表示的有机过氧化二碳酸酯。 在该式中,R 1,R 2,R 3和R 4各自独立地选自含有1至4个碳原子的烷基。 R 1和R 2和/或R 3和R 4可以参与具有3至6个碳原子的环烷基。 过氧二碳酸酯可用作烯属不饱和单体的聚合或共聚的引发剂或不饱和聚酯树脂的交联。 有机过氧二碳酸酯可以与市售的过氧化二碳酸酯,特别是具有较长半衰期的过氧碳酸酯,或与过氧化物,二酰基过氧化物和偶氮化合物组合使用。
    • 16. 发明授权
    • Method of converting amine hydrohalide into free amine
    • 将胺氢卤化物转化为游离胺的方法
    • US5906722A
    • 1999-05-25
    • US914603
    • 1997-08-18
    • Peter C. FollerDavid G. RobertsRobert H. Tang
    • Peter C. FollerDavid G. RobertsRobert H. Tang
    • B01D61/44C02F1/469C25B3/00C25B9/08C25B7/00C25B1/00C25B9/00
    • C25B9/08C25B3/00
    • Describes a method of electrochemically converting amine hydrohalide, e.g., ethyleneamine hydrochloride, into free amine, e.g., free ethyleneamine. A three compartment electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and an anion exchange membrane, (2) an anode compartment containing an anode assembly comprising either (a) a hydrogen consuming gas diffusion anode and a current collecting electrode or (b) a hydrogen consuming gas diffusion anode which is fixedly held between a hydraulic barrier and a current collecting electrode, and (3) an intermediate compartment separated from the catholyte and anode compartments by the anion exchange membrane and either (i) the hydrogen consuming gas diffusion anode or (ii) the hydraulic barrier respectively. An aqueous solution of amine hydrohalide is charged to the catholyte compartment, while hydrogen gas is charged to the anode compartment and an aqueous conductive electrolyte solution is charged to the intermediate compartment. Direct current is passed through the electrolytic cell and an aqueous solution comprising free amine is removed from the catholyte compartment.
    • 描述了将胺氢卤化物(例如乙烯胺盐酸盐)电化学转化成游离胺,例如游离亚乙基胺的方法。 提供一种三室电解池,其具有:(1)阴极电解室,其包含阴极组件,阴极组件包括阴极和阴离子交换膜;(2)阳极室,其包含阳极组件,阳极组件包括(a)消耗氢的气体扩散阳极和 电流收集电极或(b)固定保持在液压屏障和集电电极之间的消耗氢的气体扩散阳极,以及(3)通过阴离子交换膜与阴极电解液和阳极隔室分离的中间室和(i )氢消耗气体扩散阳极或(ii)液压屏障。 将胺氢卤化物的水溶液加入到阴极电解液室中,同时将氢气加入到阳极室中,并将水性导电电解质溶液装入中间室。 直流电流通过电解槽,并从阴极电解液隔室除去包含游离胺的水溶液。
    • 19. 发明授权
    • Tertiaryalkyl peroxycarbonates
    • 过碳酸三烷基酯
    • US4526726A
    • 1985-07-02
    • US430051
    • 1982-09-30
    • Robert H. Tang
    • Robert H. Tang
    • C07C409/38C07C409/40C08F299/04C07C179/18
    • C07C409/40C08F299/045
    • Described are organic peroxycarbonates of the graphic formula: ##STR1## in which R.sub.1 is a C.sub.1 -C.sub.14 alkyl, phenyl or benzyl group, R.sub.2 and R.sub.3 are each selected from the group C.sub.1 -C.sub.4 alkyl, C.sub.5 -C.sub.7 cycloalkyl, C.sub.1 -C.sub.4 alkyl substituted C.sub.5 -.sub.7 cycloalkyl or participate in a cycloalkyl group of from 5 to 7 carbon atoms, provided that when one of R.sub.2 and R.sub.3 is a cycloalkyl group, the other is an alkyl group, A is cyano or alkoxycarbonyl, i.e., ##STR2## wherein R is a C.sub.1 -C.sub.8 alkyl or cyclohexyl group. Preferably R.sub.2 and R.sub.3 are each a C.sub.1 -C.sub.2 alkyl group or participate to form a cyclohexyl group, R.sub.1 is a C.sub.1 -C.sub.3 alkyl or phenyl and R is a C.sub.1 -C.sub.4 alkyl.The compounds can be used as initiators for the polymerization and copolymerization of ethylenically unsaturated monomers. The compounds also find application in connection with the curing of polyester resins and the vulcanization of silicone rubbers, e.g., hot air vulcanization.
    • 描述的是下式的有机过碳酸酯:其中R 1是C 1 -C 14烷基,苯基或苄基,R 2和R 3各自选自C 1 -C 4烷基,C 5 -C 7环烷基,C 1 -C 4烷基 取代的C 5-7环烷​​基或参与5至7个碳原子的环烷基,条件是当R 2和R 3之一为环烷基时,另一个为烷基,A为氰基或烷氧基羰基,即, 其中R是C1-C8烷基或环己基。 R2和R3优选为C1-C2烷基或参与形成环己基,R1为C1-C3烷基或苯基,R为C1-C4烷基。 这些化合物可以用作烯属不饱和单体的聚合和共聚的引发剂。 该化合物还可用于聚酯树脂的固化和硅橡胶的硫化,例如热空气硫化。