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11. 发明授权

US07696295B2 Condensation products of silicic acid derivatives and optical waveguide devices using the same 有权
标题翻译：硅酸衍生物和使用其的光波导器件的缩合产物
公开(公告)号：US07696295B2
公开(公告)日：2010-04-13
申请号：US12162618
申请日：2006-02-03
申请人： Naoyuki Kondo , Takao Hayashi , Michael Popall , Lothar Froehlich , Ruth Houbertz , Sebastien Cochet
发明人： Naoyuki Kondo , Takao Hayashi , Michael Popall , Lothar Froehlich , Ruth Houbertz , Sebastien Cochet
IPC分类号： C08G77/20 , C08G77/04 , C08G77/12 , C08G77/00 , G02B6/00
CPC分类号： G02B6/122 , C08G77/20 , C08G77/24 , G02B1/045 , G02B6/1221
摘要： The present invention relates to condensation products of silicic acid derivatives usable especially in optical waveguides and particularly to a condensation product obtained by condensing a silane diol compound (A) of the general formula (1): R12Si(OR2)2 (1) wherein R1 represents a group having at least one aromatic group and having 6 to 20 carbon atoms, and R2 represents hydrogen (H which may also be a heavy hydrogen D), with a modified silane compound (B) of the general formula (2): R3Si(OR4)3 (2) wherein R3 represents an organic group having at least one C═C double bond; and R4 represents a group of CnH2n+1 (n=a number of 1 or 2), in the molar ratio 1.1 to 1.4:1 [(A):(B)], and to a process for producing the same condensation product, as well as to an optical waveguide device fabricated using the same condensation product.
摘要翻译：本发明涉及特别用于光波导的硅酸衍生物的缩合产物，特别涉及将通式（1）的硅烷二醇化合物（A）：R 12 Si（OR 2）2（1）表示具有至少一个芳族基团并且具有6至20个碳原子的基团，并且R 2表示氢（H，其也可以是重氢D）与通式（2）的改性硅烷化合物（B）：R3Si （OR4）3（2）其中R3表示具有至少一个C = C双键的有机基团; R4表示CnH2n + 1（n = 1或2的数），摩尔比为1.1〜1.4:1 [（A）:( B）]，以及制造相同的缩合物的方法，以及使用相同的缩合产物制造的光波导器件。

12. 发明授权

US5668237A Silicon and zirconium based lacquer, its use as a substrate coating and substrates thus obtained 失效
标题翻译：硅和锆基漆，其用作基底涂层和由此获得的底物
公开(公告)号：US5668237A
公开(公告)日：1997-09-16
申请号：US347472
申请日：1995-02-15
申请人： Michael Popall , Jochen Schulz , Birke Olsowski , Monika Pilz
发明人： Michael Popall , Jochen Schulz , Birke Olsowski , Monika Pilz
IPC分类号： B05D7/26 , C08G77/20 , C08G77/22 , C08G77/58 , C08G79/00 , C09D183/04 , C09D183/07 , C09D183/14 , C09D185/00 , H01B3/46 , H01G4/33 , H01L23/29 , H05K3/28
CPC分类号： C09D183/14 , C08G77/58 , H01B3/46 , H01L23/29 , H01L23/296 , H05K3/285 , H01L2924/0002
摘要： The present invention relates to a lacquer obtained by the process comprising the steps of: (i) precondensation of: a) 1 to 10 mol % of at least one zirconium compound of the formula ZrR.sub.4 ; b) 20 to 94 mol % of at least one organic silane of the formula R".sub.m (R'"Y).sub.n SiX.sub.(4-m-n) ; c) 5 to 30 mol % of at least one organic silane of the formula R".sub.p SiX.sub.4-p ; d) optionally 0 to 10 mol % of at least one low-volatility metal oxide; and (ii) hydrolysis condensation of the precondensate of step (i) in the presence of 0 to 50% of the stoichiometric amount of water. The invention also relates to a process for the obtention of a coating on substrate which comprises the steps of applying the lacquer and curing same. The invention also relates to the thus-coated substrates.
摘要翻译： PCT No.PCT / EP93 / 01427 Sec。 371日期1995年2月15日 102（e）日期1995年2月15日PCT提交1993年6月5日PCT公布。出版物WO93 / 25605 日本公开日1993年12月23日本发明涉及通过该方法获得的漆，其包括以下步骤：（i）预缩合：a）1至10mol％的至少一种式ZrR 4的锆化合物; b）20-94摩尔％的至少一种式R''m（R“'）nSiX（4-m-n）的有机硅烷; c）5至30mol％的至少一种式R''pSiX4-p的有机硅烷; d）任选的0至10摩尔％的至少一种低挥发性金属氧化物; 和（ii）步骤（i）的预缩合物在0至50％化学计量的水存在下的水解缩合。本发明还涉及一种用于获得基材上的涂层的方法，该方法包括施加该漆并固化其的步骤。本发明还涉及如此涂覆的基底。

13. 发明授权

US5360834A Process for photoinitiated control of inorganic network formation in the sol-gel process 失效
标题翻译：溶胶 - 凝胶法中无机网络形成的光引发控制方法
公开(公告)号：US5360834A
公开(公告)日：1994-11-01
申请号：US188746
申请日：1994-01-31
申请人： Michael Popall , Jochen Schulz , Helmut Schmidt
发明人： Michael Popall , Jochen Schulz , Helmut Schmidt
IPC分类号： B01J13/00 , B01J19/12 , C03C1/00 , C03C17/02 , C03C17/25 , C08G4/00 , C08G77/02 , C08J3/28 , C08K3/18
CPC分类号： B01J13/0039 , B01J19/123 , C03C1/008 , C03C17/02 , C03C17/25
摘要： A process is described for photoinitiated control of inorganic network fotion in the sol-gel process, which comprises eitherA) subjecting one or more hydrolytically polycondensable compounds of constituent elements of glass or ceramic, excluding silicon compounds containing polymerizable organic groups, to hydrolytic polycondensation in a liquid reaction medium to form a sol and irradiating the resulting sol in a structured or unstructured manner in the presence of a photoinitiator which can change the pH of the reaction medium on irradiation, using radiation of a wavelength range in which the photoinitiator absorbs;orB) liberating water in an anhydrous reaction medium which contains an alcohol, one or more hydrolytically polycondensable compounds of constituent elements of glass or ceramic and a photoinitiator which can liberate water by a photochemical reaction or a secondary reaction when irradiated, by structured or non-structured irradiation using radiation of a wavelength range in which the photoinitiator absorbs, and in this way effecting the hydrolytic polycondensation.
摘要翻译：描述了在溶胶 - 凝胶法中对无机网络形成进行光引发控制的方法，其包括A）将除了含有可聚合有机基团的硅化合物之外的玻璃或陶瓷的一种或多种水解可缩聚化合物的化合物水解缩聚液体反应介质以形成溶胶，并且在光引发剂存在下以结构或非结构化方式照射所得溶胶，所述光引发剂可使用光引发剂吸收的波长范围的辐射在照射时改变反应介质的pH值; 或B）在含有醇，一种或多种水解可缩聚的玻璃或陶瓷组成元素的化合物和光引发剂的无水反应介质中释放水，其可以通过结构化或非结构化的光化学反应或二次反应释放水使用光引发剂吸收的波长范围的辐射的结构化照射，并且以这种方式进行水解缩聚。

14. 发明授权

US5973176A Hydrolyzable, fluorinated silanes, method of their production and their use for producing silicic acid polycondensates and hetero silicic acid polycondensates 失效
标题翻译：可水解氟化硅烷，其制备方法及其用于生产硅酸缩聚物和异硅酸缩聚物的用途
公开(公告)号：US5973176A
公开(公告)日：1999-10-26
申请号：US832283
申请日：1997-04-03
申请人： Christof Roscher , Michael Popall , Birke-E. Olsowski
发明人： Christof Roscher , Michael Popall , Birke-E. Olsowski
IPC分类号： C07F7/04 , C07F7/12 , C07F7/18 , C08G77/24 , C08G77/58 , C08J5/14 , C09C3/12 , C09D183/08 , C09K3/10 , G03F7/00 , C07F7/08 , C07F7/10
CPC分类号： C07F7/04 , C07F7/12 , C07F7/1836 , C07F7/184 , C07F7/1896 , C08G77/24 , C08G77/58 , C09C3/12 , C09D183/08 , C09K3/1018 , G03F7/00
摘要： The invention relates to hydrolyzable fluorinate silanes, methods of theirroduction and of their use for producing silicic acid polycondensates and hetero silicic acid polycondensats The silanes in accordance with the invention are of the general formula: {[R'-(Y).sub.e ].sub.c+1 (C.sub.6 F.sub.4-c) (C.sub.6 F.sub.4).sub.d }.sub.f SiR.sub.a X.sub.b (I) in which the groups and indices are identical or different and have the following meaning:R=alkyl, alkenyl, aryl, alkylaryl or arylalkyl, substituted if required, each with 1 to 15 carbon atoms, whereby the groups may be interrupted by oxygen or sulfur atoms, ester, carbonyl, amide or amino groups;R'=I, Br, Cl (if d.noteq.0), F (if d.noteq.0), H (if X.noteq.H or R.noteq.methyl or e=1) or an organic group with 1 to 50 carbon atoms;X=hydrogen, halogen except fluorine, hydroxy, alkoxy, acyloxy, alkylcarbonyl, alkoxycarbonyl or NR".sub.2, with R"=hydrogen, alkyl or aryl;Y=O, S, NH or NR', where R' is an organic group with 1 to 50 carbon atoms;a=0, 1 or 2;b=1, 2 or 3;c=0 or 1;d=0 to 9;e=0 or 1;f=1, 2 or 3, with a+b+f=4.
摘要翻译：本发明涉及可水解的氟化物硅烷，其制备方法及其用于生产硅酸缩聚物和异硅酸缩合物的用途根据本发明的硅烷具有以下通式：{[R' - （Y）e] c +1（C6F4-c）（C6F4）d} fSiRaXb（I）其中基团和指数相同或不同，具有以下含义：R =烷基，烯基，芳基，烷基芳基或芳烷基，如果需要， 1至15个碳原子，其中基团可被氧或硫原子间隔，酯，羰基，酰胺或氨基; R'= I，Br，Cl（如果d NOTEQUAL 0），F（如果d NOTEQUAL 0），H（如果X NOTEQUAL H或R NOTEQUAL甲基或e = 1）或具有1至50个碳原子的有机基团; X =氢，除氟以外的卤素，羟基，烷氧基，酰氧基，烷基羰基，烷氧基羰基或NR'2，其中R“=氢，烷基或芳基; Y = O，S，NH或NR'，其中R'是具有1至50个碳原子的有机基团; a = 0,1或2; b = 1,2或3; c = 0或1; d = 0〜9; e = 0或1; f = 1,2或3，a + b + f = 4。

15. 发明授权

US07470761B2 Proton-conductive membranes and layers and methods for their production 失效
标题翻译：质子导电膜及其制备方法
公开(公告)号：US07470761B2
公开(公告)日：2008-12-30
申请号：US11208553
申请日：2005-08-23
申请人： Stéphane Jacob , Lothar Fröhlich , Konrad Olma , Michael Popall , Frank Kahlenberg
发明人： Stéphane Jacob , Lothar Fröhlich , Konrad Olma , Michael Popall , Frank Kahlenberg
IPC分类号： C08F30/08
CPC分类号： C08L83/08 , B01D71/70 , C08G77/26 , C08G77/28 , H01M8/1037 , H01M8/1048 , H01M8/1074 , Y02P70/56
摘要： This invention relates to a silane-resin composition that can be obtained by at least partial hydrolytic condensation of at least the following components: (1) one or more sulfonic acid group-containing silane(s) with at least one group that can be cleaved under hydrolytic conditions, (2) one or more styryl-functionalized silane(s) and (3) one or more silane(s) that carry a nitrogen-containing heterocyclic compound, an amine group or a sulfonamide group with at least one group that can be cleaved under hydrolytic conditions, and mixing of the components before, during or after the hydrolytic condensation, as well as a process for the production of this composition. With the silane resin that is obtained, proton-conductive, organically cross-linked heteropolysiloxanes can be produced that are suitable for PEMFC in a layer or membrane form as proton-conductive systems. Their proton conductivity can be further increased by the addition of suitable liquids.
摘要翻译：本发明涉及可以通过至少以下组分至少部分水解缩合获得的硅烷 - 树脂组合物：（1）一种或多种含有磺酸基的硅烷与至少一个可被切割的基团在水解条件下，（2）一种或多种苯乙烯基官能化的硅烷和（3）一种或多种含有至少一个基团的含氮杂环化合物，胺基或磺酰胺基团的硅烷，可以在水解条件下裂解，并且在水解缩合之前，期间或之后混合组分，以及制备该组合物的方法。使用得到的硅烷树脂，可以制备质子传导性有机交联杂多硅氧烷，其适用于作为质子传导系统的层或膜形式的PEMFC。通过加入合适的液体可以进一步提高其质子传导性。

16. 发明申请

US20060058485A1 Proton-conductive membranes and layers and methods for their production 失效
公开(公告)号：US20060058485A1
公开(公告)日：2006-03-16
申请号：US11208553
申请日：2005-08-23
申请人： Stephane Jacob , Lothar Frohlich , Konrad Olma , Michael Popall , Frank Kahlenberg
发明人： Stephane Jacob , Lothar Frohlich , Konrad Olma , Michael Popall , Frank Kahlenberg
IPC分类号： C08G77/04 , C08L83/04
CPC分类号： C08L83/08 , B01D71/70 , C08G77/26 , C08G77/28 , H01M8/1037 , H01M8/1048 , H01M8/1074 , Y02P70/56
摘要： This invention relates to a silane-resin composition that can be obtained by at least partial hydrolytic condensation of at least the following components: (1) one or more sulfonic acid group-containing silane(s) with at least one group that can be cleaved under hydrolytic conditions, (2) one or more styryl-functionalized silane(s) and (3) one or more silane(s) that carry a nitrogen-containing heterocyclic compound, an amine group or a sulfonamide group with at least one group that can be cleaved under hydrolytic conditions, and mixing of the components before, during or after the hydrolytic condensation, as well as a process for the production of this composition. With the silane resin that is obtained, proton-conductive, organically cross-linked heteropolysiloxanes can be produced that are suitable for PEMFC in a layer or membrane form as proton-conductive systems. Their proton conductivity can be further increased by the addition of suitable liquids.

17. 发明授权

US06984747B2 Method for preparing styryl-functionalized silanes 失效
标题翻译：制备苯乙烯基官能化硅烷的方法
公开(公告)号：US06984747B2
公开(公告)日：2006-01-10
申请号：US10313007
申请日：2002-12-06
申请人： Stéphane Jacob , Lothar Fröhlich , Konrad Olma , Michael Popall , Frank Kahlenberg
发明人： Stéphane Jacob , Lothar Fröhlich , Konrad Olma , Michael Popall , Frank Kahlenberg
IPC分类号： C07F7/04
CPC分类号： C07F7/1876
摘要： The invention relates to a method for preparing silanes comprising styryl groups, said silanes being represented by the general formula (I): (St)bSiR′aR4−a−b with improved yields through a reaction with magnesium in a solvent mixture comprising from 30:70 to 70:30 (v/v) of diethyl ether and tetrahydrofuran.
摘要翻译：本发明涉及一种制备包含苯乙烯基的硅烷的方法，所述硅烷由通式（I）表示：<？in-line-formula description =“In-line Formulas”end =“lead”？>（St） α-in-line-formula description =“In-line Formulas”end =“tail”？ >与包含30:70至70:30（v / v）二乙醚和四氢呋喃的溶剂混合物中的镁反应，产率提高。

18. 发明授权

US06312085B1 Ink jet printing head with elements made of organosilicic compounds 失效
标题翻译：喷墨打印头用有机硅化合物制成
公开(公告)号：US06312085B1
公开(公告)日：2001-11-06
申请号：US09029350
申请日：1998-07-13
申请人： J{overscore (u)}rgen Kappel , Michael Popall , Jochen Schulz , Adelheid Martin , Birke-E. Olsowski , Karl Bühler
发明人： J{overscore (u)}rgen Kappel , Michael Popall , Jochen Schulz , Adelheid Martin , Birke-E. Olsowski , Karl Bühler
IPC分类号： B41J2015
CPC分类号： B41J2/164 , B41J2/1604 , B41J2/1631
摘要： The invention provides inkjet print heads, which have one or more components of a polymer material, which is produced, substantially, or with the use of, at least one Compound (I) XaRbSiR1(4−a−b) with X=hydrolyzable group, R=eventually substituted Alkyl, Aryl, Alkenyl, Alkylaryl or Arylalkyl, R1=organic remainder with at least one polymerizable group, a= to 3, b=0 to 2. In addition, the invention provides a process for the manufacture of the heads and for the utilization, for said purpose, of a polymer material.
摘要翻译：本发明提供喷墨打印头，其具有聚合物材料的一种或多种组分，其基本上或使用至少一种具有X =可水解基团的化合物（I）XaRbSiR1（4-ab），R =最终取代的烷基，芳基，烯基，烷基芳基或芳基烷基，R1 =具有至少一个可聚合基团的有机残余物，a = 3，b = 0至2.另外，本发明提供了制造头部的方法，用于所述目的的聚合物材料的利用。

19. 发明授权

US06949616B2 Proton-conductive membranes and layers and methods for their production 失效
标题翻译：质子导电膜及其制备方法
公开(公告)号：US06949616B2
公开(公告)日：2005-09-27
申请号：US10324079
申请日：2002-12-20
申请人： Stéphane Jacob , Lothar Fröhlich , Konrad Olma , Michael Popall , Frank Kahlenberg
发明人： Stéphane Jacob , Lothar Fröhlich , Konrad Olma , Michael Popall , Frank Kahlenberg
IPC分类号： B01D71/70 , H01M8/1037 , H01M8/1048 , H01M8/1072 , C08G77/20
CPC分类号： C08L83/08 , B01D71/70 , C08G77/26 , C08G77/28 , H01M8/1037 , H01M8/1048 , H01M8/1074 , Y02P70/56
摘要： This invention relates to a silane-resin composition that can be obtained by at least partial hydrolytic condensation of at least the following components: (1) one or more sulfonic acid group-containing silane(s) with at least one group that can be cleaved under hydrolytic conditions, (2) one or more styryl-functionalized silane(s) and (3) one or more silane(s) that carry a nitrogen-containing heterocyclic compound, an amine group or a sulfonamide group with at least one group that can be cleaved under hydrolytic conditions, and mixing of the components before, during or after the hydrolytic condensation, as well as a process for the production of this composition. With the silane resin that is obtained, proton-conductive, organically cross-linked heteropolysiloxanes can be produced that are suitable for PEMFC in a layer or membrane form as proton-conductive systems. Their proton conductivity can be further increased by the addition of suitable liquids.
摘要翻译：本发明涉及可以通过至少以下组分至少部分水解缩合获得的硅烷 - 树脂组合物：（1）一种或多种含有磺酸基的硅烷与至少一个可被切割的基团在水解条件下，（2）一种或多种苯乙烯基官能化的硅烷和（3）一种或多种含有至少一个基团的含氮杂环化合物，胺基或磺酰胺基团的硅烷，可以在水解条件下裂解，并且在水解缩合之前，期间或之后混合组分，以及制备该组合物的方法。使用得到的硅烷树脂，可以制备质子传导性有机交联杂多硅氧烷，其适用于作为质子传导系统的层或膜形式的PEMFC。通过加入合适的液体可以进一步提高其质子传导性。

20. 发明授权

US06283578B1 Hydrophobic coating for ink jet printing heads 失效
标题翻译：用于喷墨打印头的疏水涂层
公开(公告)号：US06283578B1
公开(公告)日：2001-09-04
申请号：US09029127
申请日：1998-06-11
申请人： Michael Popall , Jochen Schulz , Birke-E. Olsowski , Adelheid Martin , Karl Bühler
发明人： Michael Popall , Jochen Schulz , Birke-E. Olsowski , Adelheid Martin , Karl Bühler
IPC分类号： B41J2135
CPC分类号： B41J2/1606 , C09D183/04 , C09D183/06
摘要： The invention provides inkjet print head which has an Anti-wetting Coating of a polymer material, which is produced with the utilization of at least one Compound (I) XaRbSiR1(4-a-b) with X=hydrolyzable group, R=possibly substituted Alkyl, Aryl, Alkenyl, Alkylaryl or Arylalkyl, R1=organic remainder with at least one polymerizable group, a=to 3, b=0 to 2. In addition, a Process for the Manufacture of the Print Heads is made available, as well as a Means for the Coating of same.
摘要翻译：本发明提供喷墨打印头，其具有使用至少一种化合物（I）XaRbSiR1（4-ab）与X =可水解基团，R =可能被取代的烷基取代的聚合物材料的抗潮湿涂层，芳基，烯基，烷基芳基或芳基烷基，R1 =具有至少一个可聚合基团的有机残基，a = 3，b = 0至2.此外，制造印刷头的方法可用，以及用于涂层的方法。

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