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11. 发明授权

US08158037B2 Photochromic materials having extended pi-conjugated systems and compositions and articles including the same 有权
标题翻译：具有延伸的π-共轭体系的光致变色材料和包含其的组合物和制品
公开(公告)号：US08158037B2
公开(公告)日：2012-04-17
申请号：US12873793
申请日：2010-09-01
申请人： Anu Chopra , Jun Deng , Beon-Kyu Kim , David B. Knowles , Frank F. Molock, Jr. , Victor A. Montes , Stephen D. Straight , Wenjing Xiao , Huayun Yu
发明人： Anu Chopra , Jun Deng , Beon-Kyu Kim , David B. Knowles , Frank F. Molock, Jr. , Victor A. Montes , Stephen D. Straight , Wenjing Xiao , Huayun Yu
IPC分类号： G02B5/23 , C07D311/78 , C07D311/94
CPC分类号： G02C7/049 , C07D311/94 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1059 , C09K2211/1088 , C09K2211/1096 , G02B1/041 , G02B1/043 , G02C7/102 , Y10T428/31504 , C08L101/14
摘要： The present invention provides ophthalmic devices comprising at least one photochromic material which is an indeno-fused naphthopyran having a pi-conjugation extending group bonded to the 11-position of the indeno-fused naphthopyran, the pi-conjugation extending group having at least one pendent halo-substituted group bonded thereto. The pi-conjugation extending group extends the pi-conjugation system of said indeno-fused naphthopyran. The 13-position of the indeno-fused naphthopyran is substantially free of spiro-substituents. The invention further provides photochromic materials of specified structure, photochromic compositions, photochromic articles and optical elements that include the photochromic materials. Other non-limiting embodiments relate to methods of making the ophthalmic devices comprising photochromic materials.
摘要翻译：本发明提供了包含至少一种光致变色材料的眼科装置，其是茚并稠合萘并吡喃，其具有与茚并稠合萘并吡喃的11位键合的π结合延伸基团，所述π-共轭延伸基团具有至少一个侧链与其键合的卤素取代基。 π-共轭延伸基团扩展所述茚并稠合萘并吡喃的π-共轭体系。茚并稠合萘并吡喃的13位基本上不含螺取代基。本发明还提供了具有特定结构的光致变色材料，光致变色组合物，光致变色制品和包括光致变色材料的光学元件。其它非限制性实施方案涉及制备包含光致变色材料的眼科装置的方法。

12. 发明申请

US20100209697A1 METHODS FOR PRODUCING PHOTOSENSITIVE MICROPARTICLES, NON-AQUEOUS DISPERSIONS THEREOF AND ARTICLES PREPARED THEREWITH 有权
标题翻译：生产感光性微生物的方法及其制备的非水性分散体及其制备方法
公开(公告)号：US20100209697A1
公开(公告)日：2010-08-19
申请号：US12719293
申请日：2010-03-08
申请人： Steven E. Bowles , Anu Chopra , James P. Colton , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
发明人： Steven E. Bowles , Anu Chopra , James P. Colton , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
IPC分类号： G02B1/10 , H01F1/26 , H01B1/12 , G02B5/23 , C09K11/06 , C08K5/057 , C08K5/5419 , C08L75/00 , B32B5/16
CPC分类号： G02B1/10 , C08G18/3275 , C08G18/348 , C08G18/6659 , C08G18/672 , C08G18/755 , C08G18/758 , C09D175/16 , G02B1/11 , G03C1/733 , G03F7/002 , G03F7/038 , G03F7/105 , G11B7/242 , Y10T428/25 , C08G18/0823
摘要： Described are non-aqueous dispersions of photosensitive polymeric microparticles, comprising: a) an organic continuous phase comprising an organic solvent; and b) photosensitive polymeric microparticles dispersed in the organic continuous phase. The microparticles comprise an at least partially polymerized component having integral surface and interior domains, wherein the surface domain comprises a polymeric material that is solubilized by the organic solvent, the interior domain comprises a polymeric material that is insoluble in the organic solvent, and the surface domain and/or interior domain is photosensitive. Also described are methods of producing such non-aqueous dispersions, curable film-forming compositions containing them, and photosensitive coated substrates.
摘要翻译：描述的是光敏聚合物微粒的非水分散体，包括：a）包含有机溶剂的有机连续相; 和b）分散在有机连续相中的光敏聚合物微粒。微粒包括具有整体表面和内部结构域的至少部分聚合的组分，其中表面结构域包含由有机溶剂溶解的聚合材料，内部结构域包含不溶于有机溶剂的聚合材料，表面域和/或内部域是光敏的。还描述了制备这种非水分散体，含有它们的可固化成膜组合物和感光涂布基材的方法。

13. 发明授权

US07465415B2 Photochromic materials derived from ring-opening monomers and photochromic initiators 有权
标题翻译：衍生自开环单体和光致变色引发剂的光致变色材料
公开(公告)号：US07465415B2
公开(公告)日：2008-12-16
申请号：US10903770
申请日：2004-07-30
申请人： Feng Wang , Barry Van Gemert , Kevin J. Stewart , Carol L. Knox , Anu Chopra , Patrick M. Brown
发明人： Feng Wang , Barry Van Gemert , Kevin J. Stewart , Carol L. Knox , Anu Chopra , Patrick M. Brown
IPC分类号： C09K9/02 , C08G63/08 , C08G63/58 , C08G77/60 , C08F24/00
CPC分类号： C07D311/78 , C07D311/92
摘要： Various non-limiting embodiments disclosed herein related to photochromic materials comprising the reaction product of (a) at least one ring-opening cyclic monomer, and (b) a photochromic initiator. Other non-limiting embodiments related to photochromic materials represented by: wherein S′ comprises the at least one ring-opened cyclic monomer as set forth herein. Other non-limiting embodiments related to photochromic compositions, optical elements, and methods of inhibiting migration of a photochromic material in a polymeric material using the photochromic materials disclosed herein. Methods of making such photochromic materials, compositions, and optical elements are also disclosed.
摘要翻译：本文公开的各种非限制性实施方案涉及包含（a）至少一个开环环状单体和（b）光致变色引发剂的反应产物的光致变色材料。与由下式表示的光致变色材料相关的其它非限制性实施方案：其中S'包含如本文所述的至少一种开环环状单体。与光致变色组合物有关的其它非限制性实施方案，光学元件以及使用本文公开的光致变色材料抑制光致变色材料在聚合物材料中迁移的方法。还公开了制备这种光致变色材料，组合物和光学元件的方法。

14. 发明申请

US20070278461A1 PHOTOCHROMIC MATERIALS COMPRISING HALOALKYL GROUPS 审中-公开
标题翻译：包含HALOALKYL组的光致变色材料
公开(公告)号：US20070278461A1
公开(公告)日：2007-12-06
申请号：US11695126
申请日：2007-04-02
申请人： Olga G. Petrovskaia , Anu Chopra , Patrick M. Brown
发明人： Olga G. Petrovskaia , Anu Chopra , Patrick M. Brown
IPC分类号： C08L73/00 , C07D309/00 , C07D413/02
CPC分类号： G03C1/73 , C07D309/32 , C07F7/1804 , C09B57/00 , C09K9/02
摘要： Various non-limiting embodiments of the present invention relate to photochromic materials which include a haloalkyl group. More particularly, various non-limiting embodiments disclosed herein provide photochromic materials including an indeno-fused naphthopyran, such as, an indeno[2′,3′:3,4]naphtho[1,2-b] pyran, and a haloalkyl group bonded at the 13-position thereof, wherein the haloalkyl group is a perhalogenated group or a group represented by —O(CH2)a(CX2)bCT3, wherein T is a halogen, each X is independently hydrogen or halogen, a is an integer ranging from 1 to 10, and b is an integer ranging from 1 to 10. Other non-limiting embodiments disclosed herein provide photochromic composition and photochromic articles, such as, but not limited to ophthalmic lens, which include the disclosed photochromic materials and methods of making the same.
摘要翻译：本发明的各种非限制性实施方案涉及包含卤代烷基的光致变色材料。更具体地，本文公开的各种非限制性实施方案提供光致变色材料，包括茚并稠合的萘并吡喃，例如茚并[2'，3'：3,4]萘并[1,2-b]吡喃和卤代烷基在其13位上键合，其中卤代烷基是全卤代基或由-O（CH 2 CH 2）a表示的基团（CX 2）其中T是卤素，每个X独立地是氢或卤素，a是1到10的整数，并且b是一个整数。本文公开的其它非限制性实施方案提供光致变色组合物和光致变色制品，例如但不限于眼科镜片，其包括所公开的光致变色材料及其制备方法。

15. 发明授权

US08920928B2 Photochromic compounds and compositions 有权
标题翻译：光致变色化合物和组合物
公开(公告)号：US08920928B2
公开(公告)日：2014-12-30
申请号：US13325285
申请日：2011-12-14
申请人： Meng He , Darrin R. Dabideen , Sujit Mondal , Xiao-Man Dai , Ruisong Xu , Wenjing Xiao , Massimiliano Tomasulo , Huayun Yu , Anu Chopra , Anil Kumar
发明人： Meng He , Darrin R. Dabideen , Sujit Mondal , Xiao-Man Dai , Ruisong Xu , Wenjing Xiao , Massimiliano Tomasulo , Huayun Yu , Anu Chopra , Anil Kumar
IPC分类号： G02B1/04 , G02C7/02 , G02C7/10 , G02C7/14 , C07D311/92 , C07D311/94
CPC分类号： C07D311/94 , C07D311/92 , G02B1/04 , G02C7/02 , G02C7/102 , G02C7/14 , Y10T428/31504 , Y10T428/31551 , Y10T428/31663 , Y10T428/31935
摘要： Described herein are compounds generally comprising an indeno[2′,3′:3,4]naptho[1,2-b]pyran structure. Such compounds may be useful for their photochromic properties, and be used in certain photochromic compositions. Such compositions may further comprise other photochromic compositions and/or materials. Additionally, such compounds and/or compositions may be suitable for preparing certain photochromic articles.
摘要翻译：本文描述的是通常包含茚并[2'，3'：3,4]萘酚[1,2-b]吡喃结构的化合物。这些化合物可用于其光致变色性质，并可用于某些光致变色组合物中。这样的组合物还可以包含其它光致变色组合物和/或材料。另外，这样的化合物和/或组合物可适用于制备某些光致变色制品。

16. 发明申请

US20120214992A1 PHOTOCHROMIC MATERIALS THAT INCLUDE 6-AMINO SUBSTITUTED INDENO-FUSED NAPHTHOPYRANS 有权
标题翻译：包含6-氨基取代的茚三酮的光致变色材料
公开(公告)号：US20120214992A1
公开(公告)日：2012-08-23
申请号：US13268089
申请日：2011-10-07
申请人： Anu Chopra , David B. Knowles , Huayun Yu
发明人： Anu Chopra , David B. Knowles , Huayun Yu
IPC分类号： C07D413/14 , C07D405/10 , C07D413/10
CPC分类号： C07D311/92 , C07D311/94 , C07D413/04 , G03C1/73
摘要： The present invention relates to photochromic materials that include certain indeno-fused naphthopyrans. The indeno-fused naphthopyrans have an amino group (e.g., a piperidino or morpholino group) bonded to the 6-position and hydrogen or a halo group (e.g., fluoro) bonded to the 11-position thereof. The photochromic materials of the present invention can have a closed-form electromagnetic radiation absorption spectrum that is shifted to longer wavelengths (e.g., wavelengths of greater than 390 nm), relative to comparable photochromic materials. The present invention also relates to optical elements, such as eyeglasses, that include the photochromic materials of the present invention.
摘要翻译：本发明涉及包含某些茚并稠合萘并吡喃的光致变色材料。茚并稠合的萘并吡喃具有与6-位键合的氨基（例如哌啶子基或吗啉代基）和与其11位键合的氢或卤素（例如氟）。本发明的光致变色材料可以具有相对于可比较的光致变色材料而转移到较长波长（例如，大于390nm的波长）的闭合型电磁辐射吸收光谱。本发明还涉及包括本发明的光致变色材料的光学元件，例如眼镜。

17. 发明申请

US20120157696A1 METHOD OF MAKING INDENO-FUSED NAPHTHOL MATERIALS 有权
标题翻译：制造印花石墨材料的方法
公开(公告)号：US20120157696A1
公开(公告)日：2012-06-21
申请号：US13324345
申请日：2011-12-13
申请人： Anu Chopra , Barry Van Gemert , Wenjing Xiao , Huayun Yu
发明人： Anu Chopra , Barry Van Gemert , Wenjing Xiao , Huayun Yu
IPC分类号： C07C41/30 , C07C37/11 , C07D311/92
CPC分类号： C07C41/30 , C07C37/001 , C07C51/09 , C07C51/285 , C07C51/353 , C07C51/373 , C07C51/377 , C07C51/56 , C07C57/34 , C07C2603/40 , C07D263/10 , C07D263/14 , C07D307/60 , C07D307/93 , C07D311/94 , C07C57/62 , C07C59/86 , C07C59/72
摘要： The present invention relates to a method of making indeno-fused naphthol materials, that involves, with some embodiments, forming an indanone acid intermediate, which can be represented by the following general Formula V, With Formula V, m is from 0 to 4, and R1 for each m, Rg and Rh can each be independently selected from, for example, hydrogen and hydrocarbyl. The present invention also relates to a method of making an indeno-fused naphthopyran that involves an indanone acid intermediate synthetic route.
摘要翻译：本发明涉及一种制备茚并稠合的萘酚材料的方法，其中一些实施方案涉及形成茚酮酸中间体，其可以由以下通式V表示。通式V，m为0至4，并且每个m，R g和R d的R 1各自独立地选自例如氢和烃基。本发明还涉及一种制备涉及茚酮酸中间体合成路线的茚并稠合萘并吡喃的方法。

18. 发明申请

US20120145973A1 Photochromic Materials That Include Indeno-Fused Naphthopyrans 有权
标题翻译：包含茚诺芬萘醌的光致变色材料
公开(公告)号：US20120145973A1
公开(公告)日：2012-06-14
申请号：US13314297
申请日：2011-12-08
申请人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
发明人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
IPC分类号： G02B5/23 , C07D413/10 , C07D405/10 , C07D311/78
CPC分类号： C07D405/04 , C07D311/78 , C07D311/94 , C07D405/10 , C07D407/12 , C07D409/04 , C07D493/04 , C07D495/04 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1022 , C09K2211/1033 , C09K2211/1059 , C09K2211/1088 , G02B5/23 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： The present invention relates to photochromic materials that include one or more indeno-fused naphthopyrans that have particular groups at the 7, 11, and 13 positions thereof, and at the position alpha to the oxygen of the pyran ring thereof. With some embodiments, hydrogen or an alkoxy group is bonded to the 7 position, an optionally substituted phenyl is bonded to the 11 position, two alkyl groups are bonded to the 13 position, and two optionally substituted phenyl groups are bonded to the position alpha to the oxygen of the pyran ring of the indeno-fused naphthopyran compound. The 13 position of the indeno-fused naphthopyrans is free of ether groups in which an ether oxygen is bonded to the 13 position, and hydroxyl. The present invention also relates to photochromic articles and compositions that include such indeno-fused naphthopyrans.
摘要翻译：本发明涉及光致变色材料，其包括一种或多种茚并稠合的萘并吡喃，其在其7,11和13位具有特定基团，并且在其吡喃环的氧的位置。在一些实施方案中，氢或烷氧基键合至7位，任选取代的苯基键合至11位，两个烷基键合至13位，并且两个任选取代的苯基键合至位置α 茚并稠合萘并吡喃化合物的吡喃环的氧。茚并稠合萘并吡喃的13位没有醚基，其中醚氧与13位结合，羟基。本发明还涉及包含这种茚并稠合萘并吡喃的光致变色制品和组合物。

19. 发明申请

US20100221661A1 METHODS FOR PRODUCING PHOTOSENSITIVE MICROPARTICLES 有权
标题翻译：用于生产感光性微生物的方法
公开(公告)号：US20100221661A1
公开(公告)日：2010-09-02
申请号：US12719335
申请日：2010-03-08
申请人： Steven E. Bowles , Anu Chopra , Randy E. Daughenbaugh , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
发明人： Steven E. Bowles , Anu Chopra , Randy E. Daughenbaugh , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
IPC分类号： G03F7/004
CPC分类号： G03F7/002 , C08F290/067 , C08G18/3271 , C08G18/3275 , C08G18/672 , C08G18/751 , C08G18/757 , C08G18/758 , C08G18/792 , C08G18/8116 , C08L25/06 , C09D175/04 , C09D175/16 , C09K9/02 , G03C1/733 , G03F7/038 , G03F7/105 , C08G18/0823 , C08L2666/14 , C08L2666/16
摘要： Described are various methods of producing non-aqueous dispersions of photosensitive polymeric microparticles, comprising: (a) preparing one or more aqueous dispersions of a polymerizable component, at least one of which contains a photosensitive material and, wherein the polymerizable components comprise at least one hydrophilic functional group and/or at least one hydrophobic functional group; (b) subjecting the dispersion of (a) to conditions sufficient to form microparticles; (c) at least partially polymerizing the polymerizable component; (d) combining the dispersion with an organic continuous phase comprising an organic solvent; (e) removing water from the dispersion such that the final water content of the non-aqueous dispersion is less than 30 percent by weight; wherein e) is performed before or after d); and (f) reacting any acid functional groups on the surface of the microparticles with a reactive material having at least one epoxy functional group, at least one thiocarbonylthio functional group, at least one alkoxyamine functional group, or at least one halide functional group.
摘要翻译：描述了生产光敏聚合物微粒非水分散体的各种方法，包括：（a）制备一种或多种可聚合组分的水分散体，其中至少一种含有感光材料，其中可聚合组分包括至少一种亲水官能团和/或至少一个疏水官能团; （b）使（a）的分散体经受足以形成微粒的条件; （c）至少部分聚合可聚合组分; （d）将分散体与包含有机溶剂的有机连续相组合; （e）从分散体中除去水，使得非水分散体的最终含水量小于30重量％; 其中e）在d）之前或之后执行; 和（f）使微粒表面上的任何酸官能团与具有至少一个环氧官能团，至少一个硫代羰硫基官能团，至少一个烷氧基胺官能团或至少一个卤化物官能团的反应性材料反应。

20. 发明授权

US07556751B2 Photochromic materials having electron-withdrawing substituents 有权
标题翻译：具有吸电子取代基的光致变色材料
公开(公告)号：US07556751B2
公开(公告)日：2009-07-07
申请号：US11314141
申请日：2005-12-21
申请人： Anu Chopra , Beon-Kyu Kim , Barry Van Gemert
发明人： Anu Chopra , Beon-Kyu Kim , Barry Van Gemert
IPC分类号： G02B5/23
CPC分类号： G03C1/73 , C07D311/94 , C07D409/04 , C09K9/02 , C09K2211/1011 , C09K2211/1088
摘要： Photochromic materials comprising indeno-fused naphthopyrans having a first electron-withdrawing substituent and, in certain non-limiting embodiments, a second electron-withdrawing substituent are disclosed. The photochromic materials according to the various embodiments may display faster fade rates, bathochromic shift, and higher performance ratings compared to comparable indeno-fused naphthopyrans without the electron-withdrawing substituents. Photochromic compositions and articles, such as optical elements, incorporating the photochromic materials are also disclosed.
摘要翻译：公开了包含具有第一吸电子取代基的茚并稠合萘并吡喃的光致变色材料，在某些非限制性实施方案中为第二吸电子取代基。根据各种实施方案的光致变色材料可以显示比没有吸电子取代基的可比的茚并稠合萘并吡喃更快的褪色速率，红移偏移和更高的性能等级。还公开了掺入光致变色材料的光致变色组合物和制品，例如光学元件。

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