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11. 发明申请

US20070129472A1 METHOD OF MAKING A THERMOPLASTIC COMPOSITION CONTAINING AN ANTISTATIC AGENT 有权
标题翻译：制备含有抗静电剂的热塑性组合物的方法
公开(公告)号：US20070129472A1
公开(公告)日：2007-06-07
申请号：US11674373
申请日：2007-02-13
申请人： Theodorus Hoeks , Chiel Leenders , Robert van de Grampel
发明人： Theodorus Hoeks , Chiel Leenders , Robert van de Grampel
IPC分类号： C07F9/02 , C08G18/77
CPC分类号： C07C303/32 , C08K5/50 , Y10S524/912 , C07C309/06
摘要： A method for preparing a thermoplastic composition containing an antistatic agent is described. The antistatic agent is a phosphonium sulfonate salt of generic formula (1) wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is not zero then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms. The phosphonium sulfonate salt is prepared by a method that includes combining in an aqueous medium a compound of generic formula (2) wherein M is Li or Na, and X, q, p, and r are as defined above, with a stoichiometric excess of a compound of the generic formula (3) (R)4P-Z (3)wherein Z is a halogen and R is as defined above; and separating the product of formula (1) from the medium. The phosphonium sulfonate salt is then combined with a thermoplastic resin.
摘要翻译：描述了制备含有抗静电剂的热塑性组合物的方法。抗静电剂是通式（1）的鏻磺酸盐，其中每个X独立地是卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p不为零，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基。鏻磺酸盐的制备方法包括在水性介质中将通式（2）的化合物（其中M为Li或Na，X，q，p和r如上定义）与化学计量过量的通式（3）的化合物<？in-line-formula description =“In-line Formulas”end =“lead”？（R）4 PZ（3） line-formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上定义; 和将式（1）的产物与介质分离。然后将鏻磺酸盐与热塑性树脂组合。

12. 发明申请

US20080015377A1 METHODS OF MAKING AN ANTISTATIC AGENT 审中-公开
标题翻译：制造抗静电剂的方法
公开(公告)号：US20080015377A1
公开(公告)日：2008-01-17
申请号：US11772309
申请日：2007-07-02
申请人： Theodorus Hoeks , Chiel Leenders , Robert van de Grampel
发明人： Theodorus Hoeks , Chiel Leenders , Robert van de Grampel
IPC分类号： C07C309/64
CPC分类号： C07C303/32 , C07F9/5407 , C07C309/06 , C07C309/10
摘要： Disclosed are methods for making a phosphonium sulfonate salt of generic formula (1): wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than- about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is 1 then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms.
摘要翻译：公开了制备通式（1）的磺酸鏻盐的方法：其中每个X独立地为卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p为1，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基。

13. 发明申请

US20050203237A1 Biocidal compositions and methods of making thereof 审中-公开
标题翻译：杀生物剂组合物及其制备方法
公开(公告)号：US20050203237A1
公开(公告)日：2005-09-15
申请号：US10798183
申请日：2004-03-11
申请人： Josephus Cornelius Maria Dekkers , Johannes Goossens , Robert Grampel , Theodorus Hoeks , Hendrik Jacobus de Nooijer , Cornelis Johannes Maria van Peer , Gary Smith
发明人： Josephus Cornelius Maria Dekkers , Johannes Goossens , Robert Grampel , Theodorus Hoeks , Hendrik Jacobus de Nooijer , Cornelis Johannes Maria van Peer , Gary Smith
IPC分类号： A01N59/00 , A01N59/16 , C08K3/00 , C08K9/00 , C08L1/00
CPC分类号： A01N59/16 , C08K3/015 , A01N25/34 , A01N25/10 , A01N25/08 , A01N2300/00
摘要： Articles having an exterior surface comprising an inorganic biocidal agent and a first thermoplastic resin can provide a good combination of biocidal activity and physical properties. The biocidal activity of an article or multi-layer article can be enhanced by texturizing the exterior surface of the article or multi-layer article. The surface can be texturized by calender with a textured roll, mechanical or chemical abrading, or molding in a textured mold.
摘要翻译：具有包含无机杀生物剂和第一热塑性树脂的外表面的制品可以提供杀生物活性和物理性能的良好组合。制品或多层制品的杀生物活性可以通过对制品或多层制品的外表面进行纹理化来增强。表面可以通过压纹机通过纹理辊，机械或化学研磨或在纹理模具中成型而变形。

14. 发明申请

US20050038274A1 Antistatic and antidust agents, compositions thereof, and methods of manufacture 有权
标题翻译：抗静电和防尘剂，其组合物和制造方法
公开(公告)号：US20050038274A1
公开(公告)日：2005-02-17
申请号：US10952963
申请日：2004-09-29
申请人： Sanjoy Chowdhury , Prakash Wadgaonkar , Theodorus Hoeks , Suresh Rajaraman , Bhimrao Sarwade , Chilukuri Avadhani
发明人： Sanjoy Chowdhury , Prakash Wadgaonkar , Theodorus Hoeks , Suresh Rajaraman , Bhimrao Sarwade , Chilukuri Avadhani
IPC分类号： C09K3/16 , C07B61/00 , C07C303/32 , C07C309/42 , C07F7/18 , C07F9/54 , C08K5/00 , C08K5/42 , C08L101/00 , C09D183/04 , C09D201/00 , D01F1/10 , C07F9/02
CPC分类号： C07C303/32 , C08K5/0075 , C08K5/42 , C08L69/00 , C07C309/42
摘要： A quaternary onium aromatic sulfonate represented by the formula: wherein each R1 independently comprises substituted or unsubstituted, aliphatic or aromatic, hydrocarbyl, carbocyclic or heterocyclic radicals, each X is selected from the group consisting of phosphorus and nitrogen; wherein “a” has a value of 0, 1 or 2, and “b” has a value of 0 or 1 with the proviso that (a+b) is equal to 1 or 2; G1 is an aromatic group; E comprises a bis(carbonyloxyalkyl) polydiorganosiloxane, a bis(carbonyloxyaryl) polydiorganosiloxane, and an ether linkage; each Y1 independently comprises hydrogen, a monovalent hydrocarbon group, alkenyl, allyl, halogen, bromine, chlorine; nitro; and OR, wherein R is a monovalent hydrocarbon group; “q” represents any integer from and including zero through the number of positions on G1 available for substitution; “t” represents an integer equal to at least one; “s” represents an integer equal to either zero or one; and “u” represents any integer including zero; with the proviso that when E is an ether linkage, then X is phosphorus.
摘要翻译：由下式表示的季铵芳族磺酸盐：其中每个R 1独立地包含取代或未取代的脂族或芳族烃基，碳环或杂环基，每个X选自磷和氮; 其中“a”的值为0,1或2，“b”的值为0或1，条件是（a + b）等于1或2; G 1是芳族基团; E包含双（羰氧基烷基）聚二有机硅氧烷，双（羰基氧基芳基）聚二有机硅氧烷和醚键; 每个Y 1独立地包括氢，一价烃基，烯基，烯丙基，卤素，溴，氯; 硝基和OR，其中R是一价烃基; “q”表示可用于取代的G 1上的位置数的任何整数，包括零; “t”表示等于至少一个的整数; “s”表示等于零或一的整数; “u”表示包括零的任何整数; 条件是当E是醚键时，则X是磷。

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