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91. 发明授权

US4617097A Process and electrolyte for electroplating tin, lead or tin-lead alloys 失效
标题翻译：用于电镀锡，铅或锡铅合金的工艺和电解液
公开(公告)号：US4617097A
公开(公告)日：1986-10-14
申请号：US778353
申请日：1985-09-20
申请人： Fred I. Nobel , Barnet D. Ostrow , David N. Schram
发明人： Fred I. Nobel , Barnet D. Ostrow , David N. Schram
IPC分类号： C25D3/32 , C25D3/36 , C25D3/56 , C25D3/60 , H05K3/34
CPC分类号： C25D3/56 , C25D3/32 , C25D3/36 , C25D3/60 , H05K3/3473
摘要： A process and bath for electroplating tin, lead and tin-lead alloys. Improved brightness, solderability and broader current density ranges are achieved by the use in the baths of a soluble alkylene oxide condensate to provide a cloud point of the bath above about 90.degree. F., a soluble bismuth compound, an aromatic aldehyde and acetaldehyde. Tin and lead are supplied to the bath as salts of alkyl or alkylol sulfonic acids with sufficient free alkyl or alkylol sulfonic acid to provide a bath pH of less than 3.
摘要翻译：用于电镀锡，铅和锡铅合金的工艺和浴。通过在可溶性环氧烷缩合物的浴中使用提供高于约90°F的浴的浊点，可溶性铋化合物，芳族醛和乙醛来实现亮度提高，可焊性和更宽的电流密度范围。将锡和铅作为具有足够游离烷基或烷基磺酸的烷基或烷基磺酸的盐提供到浴中以提供小于3的浴pH。

92. 发明授权

US4615773A Chromium-iron alloy plating from a solution containing both hexavalent and trivalent chromium 失效
标题翻译：从含六价铬和三价铬的溶液中镀铬 - 铁合金
公开(公告)号：US4615773A
公开(公告)日：1986-10-07
申请号：US827196
申请日：1986-02-07
申请人： John Dash , Arash S. Kasaaian
发明人： John Dash , Arash S. Kasaaian
IPC分类号： C25D3/56
CPC分类号： C25D3/56
摘要： Electrodeposition of a chromium-iron alloy on a substrate using an electrolyte solution prepared from water, an inorganic hexavalent chromium compound, an inorganic trivalent chromium compound, and an inorganic iron compound, the solution having an adjusted pH lying within the range of 0.5 to 2.0.
摘要翻译：使用由水，无机六价铬化合物，无机三价铬化合物和无机铁化合物制备的电解质溶液将铬铁合金电沉积在基底上，所述溶液的调节pH在0.5至2.0的范围内。

93. 发明授权

US4560446A Method of electroplating, electroplated coating and use of the coating 失效
标题翻译：电镀，电镀涂层和使用涂层的方法
公开(公告)号：US4560446A
公开(公告)日：1985-12-24
申请号：US683006
申请日：1984-12-18
申请人： Thinh Nguyen , Jean-Pol Wiaux , Christopher J. Vance
发明人： Thinh Nguyen , Jean-Pol Wiaux , Christopher J. Vance
IPC分类号： C25B11/06 , C25D3/54 , C25D3/56 , C25D3/44
CPC分类号： C25D3/54 , C25D3/56 , Y10T428/12736 , Y10T428/12743 , Y10T428/1275 , Y10T428/12757 , Y10T428/12806 , Y10T428/12812 , Y10T428/12819 , Y10T428/12826
摘要： Transition metals of the groups IVB, VB and VIB or alloys thereof with Al are electrodeposited in a system of an electrolyte based on an aromatic hydrocarbon. The electrolyte is originally prepared by dissolving 0.02 to 0.2 moles of an inexpensive high oxidation state transition metal halide and 0.2 to 0.5 moles AlBr.sub.3 in 1.00 mole of the aromatic hydrocarbon. Additions of transition metal powders or Mg or Al particles lead to the pre-reduction of the high oxidation state transition metal ions to lower oxidation states. Alkali metal or Mg halides may be used to establish favorable bath conditions. The electrolysis is carried out with dissolvable metal anodes, to maintain the bath composition. The plating current density, bath composition and method of preparation are chosen to obtain the desired composition of the coatings.
摘要翻译：将基团IVB，VB和VIB或其与Al的合金的过渡金属电沉积在基于芳族烃的电解质体系中。电解质最初通过在1.00摩尔芳烃中溶解0.02至0.2摩尔便宜的高氧化态过渡金属卤化物和0.2至0.5摩尔AlBr 3来制备。添加过渡金属粉末或Mg或Al颗粒导致高度氧化态过渡金属离子的预还原以降低氧化态。可以使用碱金属或卤化镁来建立有利的浴条件。电解是用可溶解的金属阳极进行的，以保持浴组成。选择电镀电流密度，浴组成和制备方法以获得所需的涂层组成。

94. 发明授权

US4428802A Palladium-nickel alloy electroplating and solutions therefor 失效
标题翻译：钯 - 镍合金电镀及其解决方案
公开(公告)号：US4428802A
公开(公告)日：1984-01-31
申请号：US303663
申请日：1981-09-18
申请人： Masao Kanai , Hirotomo Koshiro
发明人： Masao Kanai , Hirotomo Koshiro
IPC分类号： C25D3/56 , C25D21/18
CPC分类号： C25D21/18 , C25D3/56 , C25D3/562 , C25D3/567
摘要： A palladium-nickel alloy plating solutions formed from tetramminepalladous chloride is provided. The tetramminepalladous chloride is soluble in aqueous ammonia plating solution and is also water soluble. This permits replenishment of the palladium in a palladium-nickel plating solution during plating operation merely by adding the tetramminepalladous palladius chloride as a solid which is easily dissolved. The palladium-nickel alloy plating solutions contain between about 5 to 30 g/l of palladium and 5 to 30 g/l of nickel.
摘要翻译：提供了由四氯化铵氯化物形成的钯镍合金电镀液。四氯化铵氯化物可溶于氨水溶液，也是水溶性的。这样可以在电镀操作期间仅在钯 - 镍电镀溶液中补充钯，只需加入容易溶解的固体的四聚氯化钯。钯 - 镍合金电镀溶液含有约5至30g / l的钯和5至30g / l的镍。

95. 发明授权

US4187166A Method of removing copper ions from a bath containing same 失效
标题翻译：从含有它们的浴中除去铜离子的方法
公开(公告)号：US4187166A
公开(公告)日：1980-02-05
申请号：US5602
申请日：1979-01-22
申请人： Wayne A. Kruper
发明人： Wayne A. Kruper
IPC分类号： F16C33/04 , C25D3/56 , C25D3/60 , C25D5/10 , C25D7/10 , C25D21/18 , C25D21/20 , C25C1/12
CPC分类号： C25D7/10 , C25D21/20 , C25D3/56
摘要： A process is provided for electrodepositing a covering layer of lead-tin on the surface of a bearing structure formed by co-electrodepositing lead, copper and tin which process comprises providing a metallic substrate; placing said metallic substrate in an electroplating bath containing lead ions, tin ions and copper ions; passing electrical current through said bath to deposit a layer of lead-tin-copper on the surface of said substrate; removing said so-plated substrate from said bath; subjecting said so-plated substrate to an aqueous rinsing media to remove electrolyte drag-out from said plating bath from the said plated substrate; bring said aqueous rinse media into contact with a metal selected from the group consisting of lead, tin and alloys thereof for a period of time sufficient to cause copper ions in said media to be replaced by ions of said metal and said copper ions to deposit as copper metal on the remainder of said metal; placing said rinsed substrate in an electroplating bath which is essentially devoid of copper ion and which contains both lead ions and tin ions; and passing electrical current through said electroplating bath to deposit a layer of lead-tin on the surface of said substrate.
摘要翻译：提供了一种用于在通过共电沉积铅，铜和锡形成的轴承结构的表面上电沉积铅锡的覆盖层的方法，该方法包括提供金属基材; 将所述金属基板放置在含有铅离子，锡离子和铜离子的电镀浴中; 使电流通过所述浴以在所述衬底的表面上沉积铅 - 锡 - 铜层; 从所述浴中去除所述镀覆的基底; 使所述镀覆的基底经受水性漂洗介质以从所述镀覆的基底去除从所述电镀液中脱出的电解质; 使所述含水漂洗介质与选自铅，锡及其合金的金属接触足够长的时间以使所述介质中的铜离子被所述金属和所述铜离子的离子代替以沉积为在所述金属的剩余部分上的铜金属; 将所述漂洗的基材置于基本上不含铜离子并且含有铅离子和锡离子的电镀浴中; 并使电流通过所述电镀浴以在所述衬底的表面上沉积铅锡层。

96. 发明授权

US4177129A Plated metallic cathode 失效
标题翻译：镀金属阴极
公开(公告)号：US4177129A
公开(公告)日：1979-12-04
申请号：US956557
申请日：1978-11-01
申请人： Han C. Kuo
发明人： Han C. Kuo
IPC分类号： C25B11/04 , C25D3/56 , C25D5/10 , C25D5/16 , C25D5/34
CPC分类号： C25D5/10 , C25B11/0478 , C25D3/56 , C25D5/16 , C25D5/34
摘要： A highly conductive and corrosion resistant low hydrogen overvoltage cathode. The cathode comprises a copper substrate plated with an alloy of nickel and molybdenum.
摘要翻译：高导电和耐腐蚀的低氢过电压阴极。阴极包括镀镍和钼合金的铜基板。

97. 发明授权

US4142948A Chromium deposition solution 失效
标题翻译：铬沉积溶液
公开(公告)号：US4142948A
公开(公告)日：1979-03-06
申请号：US881845
申请日：1978-02-27
申请人： Sakae Tajima , Takashi Mouri , Shigeyoshi Morisaki
发明人： Sakae Tajima , Takashi Mouri , Shigeyoshi Morisaki
IPC分类号： C25D3/06 , C25D3/10 , C25D3/56
CPC分类号： C25D3/06 , C25D3/56
摘要： Disclosed is an aqueous chromium deposition solution containing chromium in the trivalent state, from which a bright decorative chromium plate can be advantageously formed. The chromium deposition solution contains (a) a water-soluble trivalent chromium salt; (b) at least one compound selected from unsubstituted and amino- or hydroxy-substituted carboxylic acids and salts thereof; (c) a water-soluble aluminum salt, and; (d) ammonium ion.

98. 发明授权

US4003804A Method of electroplating of aluminum and plating baths therefor 失效
标题翻译：铝电镀方法及电镀槽
公开(公告)号：US4003804A
公开(公告)日：1977-01-18
申请号：US645552
申请日：1975-12-31
申请人： Jack Yea Wong
发明人： Jack Yea Wong
IPC分类号： C25D3/44 , C25D3/56 , C25D21/14 , C25D21/18
CPC分类号： C25D3/56 , C25D21/18 , C25D3/44
摘要： Two improved methods are described for the electrodeposition of aluminum or an alloy thereof onto an electrically conducting, preferably metallic, substrate which methods comprise:A. reacting aluminum with hydrogen halide (preferably hydrogen bromide) in the absence of water, and in an aromatic hydrocarbon solvent (toluene) to form a plating hydro aluminum halide cation in solution, the concentration of the plating aluminum cation and the concentration of hydrogen ion, in solution being, respectively, below 7.5M and 1.1M and preferably below 4.2M and 0.5M. Various bromine getters are bubbled or passed through the region of the anode, to react with bromine produced, and to prevent attack of the plated aluminum by the bromine produced, or, alternatively.B. reacting aluminum with hydrogen halide (preferably hydrogen bromide) in an aromatic hydrocarbon solvent to form an anhydrous plating, hydro aluminum bromide cation, in solution, of the type set forth in (a) above, and then adding an alkyl halide to form a different plating species, the amount of alkyl halide added being preferably a small percentage of the amount of aromatic solvent employed.Also, the method of directing the said solutions to a separate electroplating zone and depositing aluminum on a cathode using an inert anode is described.
摘要翻译：描述了两种改进的方法，用于将铝或其合金电沉积到导电的，优选金属的基底上，所述方法包括：

99. 发明授权

US3888744A Method for electrodeposition of nickel-chromium alloys and coating of uranium 失效
标题翻译：镍铬合金的电沉积方法和铀涂层的方法
公开(公告)号：US3888744A
公开(公告)日：1975-06-10
申请号：US51766374
申请日：1974-10-24
申请人： US ENERGY
发明人： STROMATT ROBERT W , LUNDQUIST JERRY R
IPC分类号： C25D3/56 , C23B5/32 , C23B5/50
CPC分类号： C25D3/56 , C25D3/562
摘要： High-quality electrodeposits of nickel-chromium binary alloys in which the percentage of chromium is controlled can be obtained by the addition of a complexing agent such as ethylenediaminetetraacetic disodium salt to the plating solution. The nickel-chromium alloys were found to provide an excellent hydrogen barrier for the protection of uranium fuel elements.

100. 发明授权

US3785939A Tin/lead plating bath and method 失效
标题翻译： TIN / LEAD镀锌浴和方法
公开(公告)号：US3785939A
公开(公告)日：1974-01-15
申请号：US3785939D
申请日：1970-10-22
申请人： CONVERSION CHEM CORP
发明人： HSU G
IPC分类号： C25D3/32 , C25D3/36 , C25D3/56 , C25D3/60 , C23B5/38 , C23B5/40 , C23B5/46
CPC分类号： C25D3/56 , C25D3/32 , C25D3/36 , C25D3/60
摘要： A PLATING BATH FOR ELECTRODEPOSITION OF TIN/LEAD ALLOYS CONTAINS STANNOUS ION, LEAD ION, A FLUOBORATE, FLUOSILICATE OR SULFAMATE RADICAL AND, AS A BRIGHTENER SYSTEM, A NON IONIC POLYOXALKYLATED SURFACTANT, A LOWER ALIPHATIC ALDEHYDE, AN ALIPHATIC OR AROMATIC AMINE AND AN AROMATIC ALDEHYDE, THE PH OF THE BATH BEING LESS THAN ABOUT 3.0.

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