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1. 发明授权

US06569366B1 Process for producing meta-type wholly aromatic polyamide filaments 有权
标题翻译：制备间位型全芳族聚酰胺长丝的方法
公开(公告)号：US06569366B1
公开(公告)日：2003-05-27
申请号：US09958900
申请日：2001-10-15
申请人： Kiyotsuna Toyohara , Jiro Sadanobu , Tsutomu Nakamura
发明人： Kiyotsuna Toyohara , Jiro Sadanobu , Tsutomu Nakamura
IPC分类号： D01D506
CPC分类号： D01F6/605
摘要： A meta-type wholly aromatic polyamide containing, as principal repeating units, meta-phenylenediamineisophthalamide units is dissolved in an amide compound solvent; the resultant polymer solution is subjected to a wet-spinning procedure wherein the polymer solution is extruded in the form of filamentary streams into a coagulation bath containing an amide compound-containing solvent and water but substantially not containing salts, through spinning orifices of a spinneret, to coagulate the extruded filamentary polymer solution streams in the coagulation bath; the coagulated porous undrawn filaments are subjected to a drawing procedure wherein the porous undrawn filaments are drawn in a plasticizing drawing bath containing an aqueous solution of an amide compound solvent; the resultant drawn filaments are washed with water, and then heat-treated (for example, further drawn at a draw ratio of 0.7 to 4.0 while being heated at a temperature of 250 to 400° C.), to provide uniform and dense meta-type wholly aromatic polyamide fibers.
摘要翻译：将作为主要重复单元的间苯二甲酰胺间苯二酰胺单元的间位型全芳香族聚酰胺溶解在酰胺化合物溶剂中; 所得聚合物溶液经受湿纺丝程序，其中聚合物溶液以丝状流的形式挤出到含有含酰胺化合物的溶剂和水但基本上不含盐的凝固浴中，通过喷丝头的纺丝孔，使凝固浴中挤出的丝状聚合物溶液流凝结; 对凝固的多孔未拉伸丝进行拉伸处理，其中将多孔未拉伸丝在含有酰胺化合物溶剂的水溶液的增塑拉伸浴中拉伸; 将得到的拉伸长丝用水洗涤，然后进行热处理（例如，在250〜400℃的温度下加热的同时以拉伸比为0.7〜4.0进一步拉伸），得到均匀且致密的间 - 型全芳族聚酰胺纤维。

2. 发明授权

US4840762A Process for preparation of high-performance grade carbon fibers 失效
标题翻译：制备高性能级碳纤维的工艺
公开(公告)号：US4840762A
公开(公告)日：1989-06-20
申请号：US790102
申请日：1985-10-22
申请人： Toru Sawaki , Hideharu Sasaki , Tsutomu Nakamura , Jiro Sadanobu
发明人： Toru Sawaki , Hideharu Sasaki , Tsutomu Nakamura , Jiro Sadanobu
IPC分类号： D01F9/15 , D01F9/155
CPC分类号： D01F9/155 , D01F9/15
摘要： A process for the preparation of high-performance grade carbon fibers, which comprises attaching a fine powder of at least one member selected from oxides and carbides of silicon, aluminum, titanium, and boron to a precursor fiber bundle of as spun pitch fibers, subjecting the fiber bundle to an infusibilization treatment, and subjecting the fiber bundle to a carbonization treatment.
摘要翻译：一种制备高性能级碳纤维的方法，其包括将选自硅，铝，钛和硼的氧化物和碳化物中的至少一种的细粉末附着到作为纺丝沥青纤维的前体纤维束上，纤维束进行输注处理，对纤维束进行碳化处理。

3. 发明授权

US5047292A Pitch-based carbon fiber and process for preparation thereof 失效
标题翻译：沥青基碳纤维及其制备方法
公开(公告)号：US5047292A
公开(公告)日：1991-09-10
申请号：US281245
申请日：1988-12-07
申请人： Jiro Sadanobu , Akihiro Ohba , Tsutomu Nakamura
发明人： Jiro Sadanobu , Akihiro Ohba , Tsutomu Nakamura
IPC分类号： D01F9/14 , D01D4/02 , D01F9/145 , D01F9/15 , D01F9/32
CPC分类号： D01F9/145 , Y10T428/2913 , Y10T428/2918 , Y10T428/2973 , Y10T428/2976
摘要： A pitch-based carbon fiber having a microstructure consisting of strip-like structural units extended in the longitudinal direction of the fiber, wherein the fractal dimension D of the arrangement of the strip-like structural units in the cross-section of the fiber has a fractal structure satisfying the requirement of the following formula (2) relatively to the observation scale r satisfying the requirement of the following formula (1) with respect to the cross-section of the fiber:E/2.5>r>E/25 (1)2.0>D>1.05 (2)wherein E in the formula (1) stands for a smallest principal radius of gyration of cross-sectional area of the cross-section of the fiber.

4. 发明授权

US07407702B2 Polymetaphenylene isophthalamide-based polymer porous film, process for its production and battery separator 失效
标题翻译：聚邻苯二甲酰间苯二胺基聚合物多孔膜，其生产工艺及电池隔膜
公开(公告)号：US07407702B2
公开(公告)日：2008-08-05
申请号：US10776184
申请日：2004-02-12
申请人： Takao Ohno , Jiro Sadanobu , Tsutomu Nakamura , Susumu Honda , Toyoaki Ishiwata
发明人： Takao Ohno , Jiro Sadanobu , Tsutomu Nakamura , Susumu Honda , Toyoaki Ishiwata
IPC分类号： B32B5/22 , B01D39/14 , B05D1/22
CPC分类号： B32B27/08 , B01D67/0011 , B01D67/0016 , B01D69/02 , B01D69/141 , B01D71/56 , B01D2323/08 , B01D2323/12 , B01D2325/22 , B01D2325/24 , B32B27/18 , B32B27/304 , B32B27/34 , B32B27/36 , B32B38/0036 , B32B2305/026 , B32B2307/306 , B32B2307/724 , B32B2309/025 , B32B2377/00 , B32B2457/10 , C08J5/18 , C08J9/28 , C08J2201/0542 , C08J2377/10 , H01M2/1646 , H01M2/1653 , H01M2/166 , Y10T428/249978 , Y10T428/249979 , Y10T428/24998 , Y10T428/249981 , Y10T428/249986 , Y10T428/249991 , Y10T428/249992 , Y10T428/249993 , Y10T428/31725
摘要： A polymetaphenylene isophthalamide-based polymer porous film having a satisfactory porous structure that exhibits excellent gas permeability and heat resistance. It is produced by a process which comprises casting a dope of the polymetaphenylene isophthalamide-based polymer and coagulating it in a coagulating bath. The porous film may also contain inorganic whiskers, and a composite porous film may be formed in combination with a separate thermoplastic polymer film.
摘要翻译：具有令人满意的多孔结构的聚邻苯二甲酰间苯二胺系聚合物多孔膜具有优异的透气性和耐热性。它是通过一种方法生产的，该方法包括将聚邻苯二甲酰间苯二胺基聚合物的掺杂物浇铸并在凝固浴中凝结。多孔膜也可以含有无机晶须，并且复合多孔膜可以与单独的热塑性聚合物膜组合形成。

5. 发明授权

US06428644B1 Process and apparatus for producing a laminate for electronic parts 失效
标题翻译：电子部件用层叠体的制造方法和装置
公开(公告)号：US06428644B1
公开(公告)日：2002-08-06
申请号：US09403169
申请日：1999-10-18
申请人： Takao Ohno , Nobuaki Kido , Tsutomu Nakamura , Michio Yoshino , Masatoshi Ozono , Jiro Sadanobu
发明人： Takao Ohno , Nobuaki Kido , Tsutomu Nakamura , Michio Yoshino , Masatoshi Ozono , Jiro Sadanobu
IPC分类号： B32B3118
CPC分类号： H01G4/30 , H05K1/0306 , H05K3/4629 , H05K3/4638 , Y10T29/435 , Y10T156/1052
摘要： An apparatus and a process for producing a laminate for electronic parts such as ceramic capacitors. After a predetermined pattern for forming an internal conductive layer is formed on a self-supporting green sheet which contains inorganic powder and an organic binder, the self-supporting green sheet is taken up by a columnar roll and laminated. At this point, the position of the same pattern on the green sheet G2 of the next cycle to be laminated adjacently onto the green sheet G1 of the previous cycle as the above pattern with respect to the predetermined pattern on the green sheet G1 taken up by the columnar roll is determined.
摘要翻译：一种用于制造诸如陶瓷电容器的电子部件层压体的装置和方法。在含有无机粉末和有机粘合剂的自支撑生片上形成用于形成内部导电层的预定图案之后，自支撑生片被柱状辊卷绕并层压。此时，将下一个循环的生片G2上的相同图案的位置相对于上一个周期的生片G1相对于上述图案相对于生片G1上的预定图案被摄取，确定柱状辊。

6. 发明授权

US5145616A Process for the preparation of pitch-based carbon fiber 失效
标题翻译：制备沥青基碳纤维的方法
公开(公告)号：US5145616A
公开(公告)日：1992-09-08
申请号：US644983
申请日：1991-01-23
申请人： Jiro Sadanobu , Akihiro Ohba , Tsutomu Nakamura
发明人： Jiro Sadanobu , Akihiro Ohba , Tsutomu Nakamura
IPC分类号： D01F9/145
CPC分类号： D01F9/145
摘要： A process is provided for the preparation of a pitch-based carbon fiber having a microstructure consisting of strip-like structural units extended in the longitudinal direction of the fiber, wherein the fractal dimension D of the arrangement of the strip-like structural units in the cross-section of the fiber has a fractal structure satisfying the requirement of the following formula (2) relatively to the observation scale r satisfying the requirement of the following formula (1) with respect to the cross-section of the fiber:E/2.5>r>E/25 (1)2.0>D>1.05 (2)wherein E in the formula (1) stands for a smallest principal radius of gyration of cross-sectional area of the cross-section of the fiber.
摘要翻译：提供了一种制备具有在纤维的纵向方向上延伸的带状结构单元的微结构的沥青类碳纤维的方法，其中带状结构单元的分布维数D 纤维的横截面相对于满足下列公式（1）对纤维横截面要求的观察比例r，具有满足下式（2）的要求的分形结构：E / 2.5 式（1）中的E表示纤维截面截面积的最小回旋半径。E / 25（1）2.0> D> 1.05（2）

7. 发明授权

US4539393A Dimensionally stable poly-m-phenylene isophthalamide film 失效
标题翻译：尺寸稳定的聚 - 间苯二甲酰间苯二胺薄膜
公开(公告)号：US4539393A
公开(公告)日：1985-09-03
申请号：US482241
申请日：1983-04-05
申请人： Yorikazu Tamura , Jiro Sadanobu , Tsutomu Nakamura
发明人： Yorikazu Tamura , Jiro Sadanobu , Tsutomu Nakamura
IPC分类号： C08J5/18 , C08G69/32
CPC分类号： C08J5/18 , C08J2377/10
摘要： A process for producing an aromatic polyamide film, which comprises drawing an undrawn aromatic polyamide film biaxially at a draw ratio of at least 1.5 in a solvent mixture consisting of (a) 5% to 75% by weight of a good solvent of the aromatic polyamide and (b) 25% to 95% by weight of a non-solvent of the aromatic polyamide, and heat treating the drawn film, which contains at least 1% by weight, based on the weight of the film, of a good solvent of said aromatic polyamide, at a temperature of not lower than 150.degree. C.An m-phenyleneisophthalamide polymer film having extremely excellent dimensional stability under moist conditions, which film has a density d of from 1.35 to 1.41 g/cm.sup.3 and principal refractive indices n.sub..alpha., n.sub..beta. and n.sub..gamma. (n.sub..alpha. >n.sub..beta. >n.sub..gamma.) for D-line of a wavelength of 589 nm satisfying the following formula: ##EQU1##
摘要翻译：一种芳族聚酰胺薄膜的制造方法，其特征在于，在由（a）5重量％〜75重量％的芳香族聚酰胺的良溶剂组成的溶剂混合物中，以拉伸比为1.5以下的双轴拉伸未拉伸芳香族聚酰胺薄膜和（b）25重量％至95重量％的芳族聚酰胺的非溶剂，并且对所述拉伸膜进行热处理，所述拉伸膜基于所述膜的重量，含有至少1重量％的良好溶剂所述芳族聚酰胺在不低于150℃的温度下进行。在湿润条件下具有非常优异的尺寸稳定性的间苯二甲酰间苯二胺聚合物膜，该密度d为1.35至1.41g / cm 3，主折射率为nα ，对于波长为589nm的D线的nβ和nγ（nα> nβ> n伽马）满足以下公式：

8. 发明授权

US06797801B2 Polyimide film and process for producing the same 失效
标题翻译：聚酰亚胺膜及其制造方法
公开(公告)号：US06797801B2
公开(公告)日：2004-09-28
申请号：US10257811
申请日：2002-10-17
申请人： Jiro Sadanobu , Rei Nishio , Susumu Honda , Tsutomu Nakamura
发明人： Jiro Sadanobu , Rei Nishio , Susumu Honda , Tsutomu Nakamura
IPC分类号： C08G7310
CPC分类号： C08J5/18 , B29C41/24 , B29C55/00 , B29C55/12 , B29D7/01 , B29K2079/08 , C08J2379/08 , Y10T428/31678 , Y10T428/31681 , Y10T428/31721
摘要： An oriented polyimide film of high strength and a production process therefor. The process basically comprises stretching a gelled film and then imidating the film. The gelled film is formed by introducing a polyamic acid solution into a condensation agent solution. The gelled film is swollen with a solvent at the time of stretching.
摘要翻译：高强度取向聚酰亚胺薄膜及其制造方法。该方法基本上包括拉伸凝胶膜然后酰亚胺化膜。凝胶膜通过将聚酰胺酸溶液引入缩合剂溶液中而形成。凝胶膜在拉伸时用溶剂溶胀。

9. 发明授权

US09287027B2 Rare earth metal-based permanent magnet 有权
标题翻译：稀土金属永磁体
公开(公告)号：US09287027B2
公开(公告)日：2016-03-15
申请号：US12990341
申请日：2008-05-14
申请人： Yukimitsu Miyao , Tsutomu Nakamura
发明人： Yukimitsu Miyao , Tsutomu Nakamura
IPC分类号： H01F1/057 , B32B15/04 , C22C9/00 , C22C13/00 , H01F41/02
CPC分类号： H01F1/0577 , C22C9/00 , C22C13/00 , H01F41/026 , Y10T428/32 , Y10T428/325
摘要： An objective of the present invention is to provide a rare earth metal-based permanent magnet with improved adhesion properties. A rare earth metal-based permanent magnet of the present invention as a means for achieving the objective has a laminated plating film, and is characterized in that the plating film comprises as an outermost surface layer a SnCu alloy plating film having a film thickness in a range from 0.1 μm to 2 μm, the composition of the SnCu alloy plating film is 35 mass % or more but less than 55 mass % of Sn and the rest being Cu, and a base plating film having two or more layers including at least a Ni plating film and a Cu plating film which are formed as the lower layer under the SnCu alloy plating film, and among the base plating film, the Ni plating film is located just below the SnCu alloy plating film. A joined structure fabricated using the rare earth metal-based permanent magnet of the present invention exhibits favorable initial adhesion strength when combined with a silicone-based adhesive, and is less deteriorated in adhesion strength even after a moisture resistance test.
摘要翻译：本发明的目的是提供一种具有改进的粘合性能的稀土金属基永磁体。本发明的稀土金属类永磁体作为实现目的的手段具有叠层电镀膜，其特征在于，所述镀膜包含作为最外表面层的SnCu合金镀膜，膜厚度为在0.1μm〜2μm的范围内，SnCu合金镀膜的成分为Sn的35质量％以上且小于55质量％，其余为Cu，并且具有两层以上的基底镀膜至少含有 Ni镀覆膜和Cu电镀膜，在SnCu合金镀膜之下形成为下层，并且在底镀膜中，Ni镀膜位于SnCu合金镀膜的正下方。使用本发明的稀土类金属类永磁体制造的接合结构，与硅酮类粘合剂组合时，表现出良好的初期粘合强度，即使在耐湿试验之后，粘合强度也劣化。

10. 发明授权

US08907001B2 Use of a pretreated precipitated silica as a reinforcing filler for silicon elastomer and the curable silicone elastomer compositions thus obtained by cold mixing 有权
标题翻译：使用预处理的沉淀二氧化硅作为硅弹性体的增强填料和通过冷混合获得的可固化的硅氧烷弹性体组合物
公开(公告)号：US08907001B2
公开(公告)日：2014-12-09
申请号：US12461283
申请日：2009-08-06
申请人： Agnès Pottier , Kyu-Min Hwang , Minoru Igarashi , Tsutomu Nakamura , Nahohiko Harada
发明人： Agnès Pottier , Kyu-Min Hwang , Minoru Igarashi , Tsutomu Nakamura , Nahohiko Harada
IPC分类号： C08K9/06
CPC分类号： C08K9/06
摘要： The invention relates to the use of a precipitated silica, pretreated by at least one organosilane hydrophobic compound or one hydrophobic silicone oil, as a reinforcing filler for silicone elastomer, the pretreated silica being incorporated in the silicone elastomer by cold mixing and having the following features: —a BET specific surface ranging from 50 to 450 m2/g, —a water wettability lower than 80, —a sulfur content lower than 0.1% by weight. The invention is directed to the curable silicone elastomer composition thus obtained.
摘要翻译：本发明涉及使用由至少一种有机硅烷疏水化合物或一种疏水性硅油预处理的沉淀二氧化硅作为有机硅弹性体的增强填料，预处理的二氧化硅通过冷混合而结合在有机硅弹性体中，具有以下特征： - BET比表面积为50-450m2 / g， - 水润湿性低于80， - 硫含量低于0.1％（重量）。本发明涉及由此获得的可固化的硅氧烷弹性体组合物。

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