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1. 发明授权

US4892950A Process for the preparation of naphthalene-1,8-dicarboximides 失效
标题翻译：萘-1,8-二羧酰亚胺的制备方法
公开(公告)号：US4892950A
公开(公告)日：1990-01-09
申请号：US204468
申请日：1988-06-09
申请人： Detlef-Ingo Schutze , Klaus Wunderlich , Karl-Heinz Reinhardt , Martin Wienkenhover
发明人： Detlef-Ingo Schutze , Klaus Wunderlich , Karl-Heinz Reinhardt , Martin Wienkenhover
IPC分类号： C07D221/14
CPC分类号： C07D221/14
摘要： Process for the preparation of naphthalene-1,8-dicarboximide which is optionally substituted in the naphthalene ring, characterized in that naphthalene-1,8-dicarboxylic anhydride which is optionally substituted in the naphthalene ring is reacted with an ammonium salt in an aqueous medium at a pH near to the neutral point, the reaction mixture is then acidified to a pH of 1 to 4 and the pH is subsequently adjusted to a value near to the neutral point.
摘要翻译：在萘环中任选取代的萘-1,8-二羧酰亚胺的制备方法，其特征在于在萘环中任选取代的萘-1,8-二羧酸酐与含水介质中的铵盐反应在接近中性点的pH下，将反应混合物酸化至1至4的pH，随后将pH调节至接近中性点的值。

2. 发明授权

US4652660A Process for preparing a thioindigo derivatives comprising cyclizing in a liquid mixture of an aluminium halide an alkali metal halide, and a carboxamide or sulfonamide 失效
标题翻译：制备硫靛衍生物的方法，其包括在卤化铝和碱金属卤化物的液体混合物中环化，以及羧酰胺或磺酰胺
公开(公告)号：US4652660A
公开(公告)日：1987-03-24
申请号：US755048
申请日：1985-07-15
申请人： Detlef-Ingo Schutze , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Klaus Wunderlich
IPC分类号： C09B7/10 , C07D333/64 , C07D409/04
CPC分类号： C09B7/10
摘要： Process for preparing thioindigo compounds of the formula ##STR1## in which A and B denote identical or different, optionally substituted benzene rings or benzene rings to which may be joined further carbocyclic and heterocyclic rings,characterized in that compounds of the formulae ##STR2## in which A and B have the abovementioned meaning andX denotes halogen, such as bromine and preferably chlorine,are reacted in a liquid mixture of an aluminium halide, an alkali metal halide and a carboxamide or sulphonamide, and the resulting intermediate product is subsequently, if desired after prior isolation, oxidized in a manner known per se, and the batch is worked up for the compounds of the formula (I).
摘要翻译：制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其中可以连接有碳环和杂环，其特征在于式其中A和B具有上述含义并且X表示卤素如溴，优选氯，在卤化铝，碱金属卤化物的液体混合物中反应的图像（IIa）和/或

3. 发明授权

US4555580A Process for the preparation of thioindigo compounds 失效
标题翻译：制备硫靛化合物的方法
公开(公告)号：US4555580A
公开(公告)日：1985-11-26
申请号：US535543
申请日：1983-09-26
申请人： Detlef-Ingo Schutze , Reinold Schmitz , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Reinold Schmitz , Klaus Wunderlich
IPC分类号： C09B7/10 , C07D333/24
CPC分类号： C09B7/10
摘要： Process for the preparation of thioindigo compounds of the formula ##STR1## in which A and B designate identical or different, optionally substituted benzene rings or benzene rings to which further carbocyclic and heterocyclic rings can be fused,characterized in that compounds of the formula ##STR2## in which A and B have the abovementioned meaning, are reacted in a mixture of chlorosulphonic acid and a further halide of an inorganic acid and, if appropriate, the resulting reaction product is oxidized in a manner which is in itself known and the batch is worked up to give compounds of the formula (I).
摘要翻译：制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其中可以与其进一步的碳环和杂环稠合，其特征在于，其中A和B具有上述含义的式（IIa）和/或（IIb）在氯磺酸和无机酸的另外的卤化物的混合物中反应，如果合适的话，所得反应产物以本身已知的方式被氧化，并且批处理以得到式（I）的化合物。

4. 发明授权

US4190726A Polycyclic dyestuffs 失效
标题翻译：多环染料
公开(公告)号：US4190726A
公开(公告)日：1980-02-26
申请号：US915020
申请日：1978-06-13
申请人： Detlef-Ingo Schutze , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Klaus Wunderlich
IPC分类号： C09B57/00 , C09B57/08 , C07D471/22
CPC分类号： C09B57/08 , Y10S8/922
摘要： In spite of their pigment character, dyestuffs of the formula ##STR1## are outstandingly suitable for dyeing synthetic fibres, in particular polyester fibres, by customary methods, strong yellow dyeings with good fastness to light and sublimation being obtained. In the abovementioned formula:R.sub.1 and R.sub.3 denote hydrogen, alkyl, aralkyl, alkoxyalkyl, alkoxycarbonyl, alkoxycarbonylalkyl or aryl,R.sub.2 and R.sub.4 denote alkylcarbonyl, arylcarbonyl, alkoxycarbonyl, --CN or --CONX.sub.1 X.sub.2,X.sub.1 denotes hydrogen, alkyl, aralkyl, aryl or cycloalkyl andX.sub.2 denotes hydrogen or alkyl.
摘要翻译：尽管它们具有颜料特性，但是通过常规方法对式（IMAGE）的染料非常适合用于染色合成纤维，特别是聚酯纤维，得到具有良好的耐光牢度和升华性的强黄色染色。在上述式中：R 1和R 3表示氢，烷基，芳烷基，烷氧基烷基，烷氧基羰基，烷氧基羰基烷基或芳基，R 2和R 4表示烷基羰基，芳基羰基，烷氧基羰基，-CN或-CONX 1 X 2，X 1表示氢，烷基，芳烷基，芳基或环烷基 X2表示氢或烷基。

5. 发明授权

US4260778A Process for the preparation of thioindigo compounds 失效
标题翻译：制备硫靛化合物的方法
公开(公告)号：US4260778A
公开(公告)日：1981-04-07
申请号：US40520
申请日：1979-05-21
申请人： Detlef-Ingo Schutze , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Klaus Wunderlich
IPC分类号： C09B7/10
CPC分类号： C09B7/10
摘要： Process for the preparation of thioindigo compounds of the formula ##STR1## in which A and B designate identical or different optionally substituted benzene rings or benzene rings onto which further carbocyclic and heterocyclic rings are fused,characterized in that compounds of the formula ##STR2## in which A and B have the meaning indicated above andX designates halogen, such as bromine and, preferably, chlorine,are reacted in a liquid mixture of an aluminium halide, an alkali metal halide and SO.sub.2 and the resulting intermediate product is then oxidized in a manner which is in itself known, if appropriate after first being isolated, and the mixture is worked up to give the compounds of the formula (I).
摘要翻译：制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其上还有碳环和杂环稠合，其特征在于式（IIa）（IIb）其中A和B具有上述含义，X表示卤素，例如溴，优选氯，在卤化铝，碱金属卤化物的液体混合物中反应然后将所得中间产物以本身已知的方式氧化，如果在首次分离后适当，则将其混合，得到式（I）化合物。

6. 发明授权

US4812568A Process for the preparation of 6,13-dihydroquinacridones and quinacridones 失效
标题翻译：制备6,13-二氢喹吖啶酮和喹吖啶酮的方法
公开(公告)号：US4812568A
公开(公告)日：1989-03-14
申请号：US12921
申请日：1987-02-10
申请人： Helmut Herzog , Detlef-Ingo Schutze , Jurgen Schneider , Reinold Schmitz
发明人： Helmut Herzog , Detlef-Ingo Schutze , Jurgen Schneider , Reinold Schmitz
IPC分类号： C07D471/04 , C09B48/00
CPC分类号： C07D471/04 , C09B48/00
摘要： Process for the preparation of a 6,13-dihydroquinacridone of the general formula (I) ##STR1## in which R.sup.1, R.sup.2, R.sup.3 and R.sup.4 designate hydrogen or substituents customary for quinacridone, characterized in that an optionally substituted dialkyl 2,5-di-(phenylamino)-3,6-dihydroterephthalate is heated to temperatures of 240.degree.-320.degree. C. in an essentially oxygen-free atmosphere in the presence of a dimethyl-diphenyl ether isomer mixture of the formula ##STR2## as the solvent and/or diluent, and a process for the preparation of optionally substituted quinacridone, characterized in that the resulting 6,13-dihydroquinacridone is oxidized in the customary manner.
摘要翻译：用于制备通式（I）的化合物（I）的6,13-二氢喹吖啶酮的方法其中R 1，R 2，R 3和R 4表示氢或通常用于喹吖啶酮的取代基，其特征在于任选取代的二烷基2，将5-二 - （苯基氨基）-3,6-二氢对苯二甲酸酯在基本上不含氧的气氛中在二甲基 - 二苯基醚异构体混合物存在下加热到240-320℃的温度，式 II）和/或作为溶剂和/或稀释剂的（IIa）和/或制备任选取代的喹吖啶酮的方法，其特征在于所得的6,13-二氢喹吖啶酮以常规方式被氧化。

7. 发明授权

US4435589A Process for the preparation of dimethyl succinylosuccinate, the disodium salt thereof, dianilinodihydroterephthalic acids, the dimethyl esters and salts thereof, and dianilinoterephthalic acids, and the dimethyl esters and salts thereof 失效
标题翻译：制备二琥珀酸琥珀酸二甲酯，其二钠盐，二苯胺二氢对苯二甲酸，其二甲酯和盐，以及二苯胺基对苯二甲酸的方法及其二甲酯及其盐
公开(公告)号：US4435589A
公开(公告)日：1984-03-06
申请号：US341047
申请日：1982-01-21
申请人： Meinhard Rolf , Detlef-Ingo Schutze , Rutger Neeff , Hans-Volker Runzheimer
发明人： Meinhard Rolf , Detlef-Ingo Schutze , Rutger Neeff , Hans-Volker Runzheimer
IPC分类号： C07C69/90 , C07C67/00 , C07C69/757 , C07C69/95 , C07C227/00 , C07C227/08 , C07C227/16 , C07C227/18 , C07C229/62 , C07C231/00 , C07C231/12 , C07C237/30 , C07C101/38 , C07C101/68 , C07C103/76
CPC分类号： C07C69/95
摘要： Process for the preparation of dimethyl succinylosuccinate, or the disodium salt thereof, by condensation of dimethyl succinate in a 35-45 percent by weight solution of sodium methylate in methanol, and a process for the preparation of dianilinodihydroterephthalic acids, the dimethyl esters and salts thereof, and of dianilinoterephthalic acids, and the dimethyl esters and salts thereof, starting from the disodium salt of dimethyl succinylosuccinate prepared according to the new process, without intermediate isolation.
摘要翻译：通过琥珀酸二甲酯在35-45重量％甲醇钠的甲醇溶液中缩合制备二甲基琥珀酸琥珀酸酯或其二钠盐的方法，以及制备二苯胺二氢对苯二甲酸的方法，其二甲酯和其盐，以及二苯胺基对苯二甲酸及其二甲酯及其盐，其由根据新方法制备的二甲基琥珀酸二琥珀酸二钠盐开始，无需中间分离。

8. 发明授权

US5738912A Dispersion of post-curable coating compounds 失效
标题翻译：后固化涂料化合物的分散
公开(公告)号：US5738912A
公开(公告)日：1998-04-14
申请号：US760093
申请日：1996-12-11
申请人： Eberhard Konig , Detlef-Ingo Schutze , Josef Pedain
发明人： Eberhard Konig , Detlef-Ingo Schutze , Josef Pedain
IPC分类号： C08G18/08 , C08G18/12 , C08G18/28 , C08G18/44 , C14C11/00 , D06N3/14 , B05D7/12
CPC分类号： D06N3/14 , C08G18/0804 , C08G18/12 , C08G18/283 , C08G18/44 , C14C11/006
摘要： The invention relates to a method for coating textiles and/or leather with an aqueous dispersion comprising (A) a mixture of (i) a urethane-containing blocked NCO prepolymer having a number average molecular weight of 2000 to 10,000, a content of blocked isocyanate groups (calculated as NCO) of 0.5 to 5 wt. %, an ethoxy group content of 2 to 50 wt. %, an ionic group content of 5 to 30 meq per 100 g of the prepolymer, and (ii) a polyamine having (cyclo)aliphatically bonded primary and/or secondary amino groups, wherein the equivalent ratio of blocked NCO groups of component (i) to amino groups of component (ii) is 1:0.9 to 1:1.2, and (B) an aqueous phase.
摘要翻译：本发明涉及一种用水分散体涂布纺织品和/或皮革的方法，其包含（A）（i）数均分子量为2000至10,000的含氨基甲酸酯的封闭NCO预聚物，封端异氰酸酯的含量基团（以NCO计算）为0.5〜5wt。％，乙氧基含量为2〜50wt。％，每100g预聚物的离子基团含量为5至30meq，和（ii）具有（环）脂族键合的伯和/或仲氨基的多胺，其中组分（i）的封闭NCO基团的当量比）至组分（ⅱ）的氨基为1：0.9至1：1.2，和（B）水相。

9. 发明授权

US5252671A Coating compositions for coatings that are permeable to water vapor and a process for their preparation 失效
标题翻译：可渗透水蒸气的涂料涂料组合物及其制备方法
公开(公告)号：US5252671A
公开(公告)日：1993-10-12
申请号：US887213
申请日：1992-05-21
申请人： Josef Pedain , Klaus Noll , Wilhelm Thoma , Detlef-Ingo Schutze
发明人： Josef Pedain , Klaus Noll , Wilhelm Thoma , Detlef-Ingo Schutze
IPC分类号： C14C11/00 , C08L75/00 , C09D133/04 , C09D175/00 , C09D175/04 , D06M15/564 , D06N3/04 , D06N3/14 , C08F8/30
CPC分类号： D06N3/14 , C09D133/04 , C09D175/04 , C08L75/00 , Y10S528/904
摘要： The present invention relates to coating compositions containing(A) 70 to 98% by weight, based on the sum of components (A) and (B), of(a) isocyanate-free polymers of ethylenically unsaturated monomers and/or polyurethanes or blocked isocyanate prepolymers, and(b) optional organic solvents, wherein component (A) contains no significant quantities of groups capable of reacting with component (B) or starting materials thereof and has a viscosity (at 23.degree. C.) of 2000 to 100,000 mPa.s;(B) 2 to 30% by weight, based on the sum of components (A) and (B), of a polyaddition product prepared in and dispersed in component (A), wherein the polyaddition product is a polyurethane, polyurethane urea, polyurea, or mixture thereof, containing ionic groups and/or potentially ionic groups in a quantity corresponding to from 0.5 to 20 milliequivalents per 100 g of component (B) but containing substantially no free isocyanate, hydroxyl, or amino groups: and(C) optional cross-linking agents;in which component (B) is formed in situ in component (A).
摘要翻译：本发明涉及涂料组合物，其包含（A）70至98重量％，基于组分（A）和（B）的总和，（a）烯属不饱和单体和/或聚氨酯或封闭的无异氰酸酯的聚合物异氰酸酯预聚物和（b）任选的有机溶剂，其中组分（A）不含有显着量的能够与组分（B）或其原料反应的基团，并且具有2000至100,000mPa的粘度（在23℃） .s; （B）基于组分（A）和（B）的总和，制备和分散在组分（A）中的加聚产物的2-30重量％，其中所述加聚产物是聚氨酯，聚氨酯脲，聚脲或其混合物，其含有相对于每100g组分（B）0.5至20毫当量但基本上不含游离异氰酸酯，羟基或氨基的量的离子基团和/或潜在的离子基团：和（C）任选的交联剂; 其中组分（B）在组分（A）中原位形成。

10. 发明申请

US20060128885A1 High-solids polyurethane-polyurea dispersions 审中-公开
标题翻译：高固体聚氨酯 - 聚脲分散体
公开(公告)号：US20060128885A1
公开(公告)日：2006-06-15
申请号：US11298345
申请日：2005-12-08
申请人： Thorsten Rische , Gerald Kurek , Holger Casselmann , Thomas Feller , Thomas Munzmay , Detlef-Ingo Schutze , Harald Blum , Hans-Georg Muller
发明人： Thorsten Rische , Gerald Kurek , Holger Casselmann , Thomas Feller , Thomas Munzmay , Detlef-Ingo Schutze , Harald Blum , Hans-Georg Muller
IPC分类号： C08G18/08
CPC分类号： C08G18/6659 , C08G18/0823 , C08G18/0828 , C08G18/10 , C08G18/12 , C08G18/283 , C08G18/4238 , C08G18/44 , C08G18/755 , C09D175/04 , C08G18/3228 , C08G18/3857 , C08G18/3855 , C08G18/3231 , C08G18/305 , C08G18/3225
摘要： The present invention relates to aqueous polyurethane-polyurea dispersions having two discrete maxima in the particle size distribution, wherein the maximum of the fine fraction is between 51 and 150 nm and the maximum of the coarse fraction is between 160 and 700 nm. The present invention also relates to a process for preparing the polyurethane-polyurea dispersions, to coating compositions containing these polyurethane-polyurea dispersions, and to coated substrates prepared from these coating compositions.
摘要翻译：本发明涉及在粒度分布中具有两个离散最大值的水性聚氨酯 - 聚脲分散体，其中细小部分的最大值为51-150nm，粗分数的最大值为160-700nm。本发明还涉及制备聚氨酯 - 聚脲分散体的方法，包含这些聚氨酯 - 聚脲分散体的涂料组合物以及由这些涂料组合物制备的涂布基材。

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