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1. 发明授权

US4555580A Process for the preparation of thioindigo compounds 失效
标题翻译：制备硫靛化合物的方法
公开(公告)号：US4555580A
公开(公告)日：1985-11-26
申请号：US535543
申请日：1983-09-26
申请人： Detlef-Ingo Schutze , Reinold Schmitz , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Reinold Schmitz , Klaus Wunderlich
IPC分类号： C09B7/10 , C07D333/24
CPC分类号： C09B7/10
摘要： Process for the preparation of thioindigo compounds of the formula ##STR1## in which A and B designate identical or different, optionally substituted benzene rings or benzene rings to which further carbocyclic and heterocyclic rings can be fused,characterized in that compounds of the formula ##STR2## in which A and B have the abovementioned meaning, are reacted in a mixture of chlorosulphonic acid and a further halide of an inorganic acid and, if appropriate, the resulting reaction product is oxidized in a manner which is in itself known and the batch is worked up to give compounds of the formula (I).
摘要翻译：制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其中可以与其进一步的碳环和杂环稠合，其特征在于，其中A和B具有上述含义的式（IIa）和/或（IIb）在氯磺酸和无机酸的另外的卤化物的混合物中反应，如果合适的话，所得反应产物以本身已知的方式被氧化，并且批处理以得到式（I）的化合物。

2. 发明授权

US4812568A Process for the preparation of 6,13-dihydroquinacridones and quinacridones 失效
标题翻译：制备6,13-二氢喹吖啶酮和喹吖啶酮的方法
公开(公告)号：US4812568A
公开(公告)日：1989-03-14
申请号：US12921
申请日：1987-02-10
申请人： Helmut Herzog , Detlef-Ingo Schutze , Jurgen Schneider , Reinold Schmitz
发明人： Helmut Herzog , Detlef-Ingo Schutze , Jurgen Schneider , Reinold Schmitz
IPC分类号： C07D471/04 , C09B48/00
CPC分类号： C07D471/04 , C09B48/00
摘要： Process for the preparation of a 6,13-dihydroquinacridone of the general formula (I) ##STR1## in which R.sup.1, R.sup.2, R.sup.3 and R.sup.4 designate hydrogen or substituents customary for quinacridone, characterized in that an optionally substituted dialkyl 2,5-di-(phenylamino)-3,6-dihydroterephthalate is heated to temperatures of 240.degree.-320.degree. C. in an essentially oxygen-free atmosphere in the presence of a dimethyl-diphenyl ether isomer mixture of the formula ##STR2## as the solvent and/or diluent, and a process for the preparation of optionally substituted quinacridone, characterized in that the resulting 6,13-dihydroquinacridone is oxidized in the customary manner.
摘要翻译：用于制备通式（I）的化合物（I）的6,13-二氢喹吖啶酮的方法其中R 1，R 2，R 3和R 4表示氢或通常用于喹吖啶酮的取代基，其特征在于任选取代的二烷基2，将5-二 - （苯基氨基）-3,6-二氢对苯二甲酸酯在基本上不含氧的气氛中在二甲基 - 二苯基醚异构体混合物存在下加热到240-320℃的温度，式 II）和/或作为溶剂和/或稀释剂的（IIa）和/或制备任选取代的喹吖啶酮的方法，其特征在于所得的6,13-二氢喹吖啶酮以常规方式被氧化。

3. 发明授权

US5747582A Aqueous coating compositions and their use for the preparation of coatings that are permeable to water vapor 失效
标题翻译：水性涂料组合物及其用于制备可渗透水蒸气的涂料的用途
公开(公告)号：US5747582A
公开(公告)日：1998-05-05
申请号：US460178
申请日：1995-06-02
申请人： Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp , Josef Pedain , Reinold Schmitz
发明人： Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp , Josef Pedain , Reinold Schmitz
IPC分类号： C08G18/08 , C08G18/28 , C08G18/44 , C08G18/50 , C14C11/00 , D06N3/14 , D21H19/62 , C08J3/00 , C08K3/20 , C08L75/00
CPC分类号： C08G18/0823 , C08G18/0804 , C08G18/0828 , C08G18/283 , C08G18/3228 , C08G18/3231 , C08G18/3855 , C08G18/44 , C08G18/5072 , C08G18/73 , C14C11/006 , D06N3/14 , D21H19/62 , Y10T428/31551 , Y10T428/31558 , Y10T428/31591
摘要： The invention relates to coating compositions used to prepare coatings having water vapor permeabilities of at least 2500 g/m.sup.2 per day (DS 2109 TM1 method) containing (A) a polyurethane containing (1) 0.1 to 75 meq/100 g of ionic groups and (2) 11 to 50% by weight of --(CH.sub.2 CH.sub.2 O).sub.n -- units (wherein n is 2 to 25) incorporated into the main chain prepared from reactive components comprising (I) one or more polyisocyanates, (II) one or more polyols having a number average molecular weight of 350 to 5000, with the proviso that if any such polyol is a sulfonated polyether diol having the formula ##STR1## in which R is hydrogen or an organic group having 1 to 8 carbon atoms, m and n are 1 to 10, p is 0, 1, or 2, and M is ammonium or alkali metal cation, then an additional ethoxy-containing polyether polyol must also be present, and (III) one or more chain lengthening agents having a molecular weight of 32 to 349; and (B) 30 to 80% by weight, based on the sum of components (A) and (B), of an aqueous phase.
摘要翻译：本发明涉及用于制备具有每天至少2500g / m 2的水蒸汽渗透性（DS 2109 TM1方法）的涂层的涂料组合物，其包含（A）含有（1）0.1至75meq / 100g离子基团的聚氨酯和（2）由反应性组分制备的包含（I）一种或多种多异氰酸酯的主链中的 - （CH 2 CH 2 O）n-单元（其中n为2至25）的11至50重量％，（II）一种或多种多元醇数均分子量为350至5000，条件是如果任何这样的多元醇是具有式“IMAGE”的磺化聚醚二醇，其中R是氢或具有1至8个碳原子的有机基团，m和n分别为 1至10，p为0,1或2，M为铵或碱金属阳离子，则还必须含有另外的含乙氧基的聚醚多元醇，和（III）一种或多种链增长剂，其分子量为 32至349; 和（B）基于水相的组分（A）和（B）的总和为30至80重量％。

4. 发明授权

US5716676A Aqueous coating compositions and their use for the preparation of coatings that are permeable to water vapor 失效
标题翻译：水性涂料组合物及其用于制备可渗透水蒸气的涂料的用途
公开(公告)号：US5716676A
公开(公告)日：1998-02-10
申请号：US748743
申请日：1996-11-18
申请人： Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp , Josef Pedain , Reinold Schmitz
发明人： Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp , Josef Pedain , Reinold Schmitz
IPC分类号： C08G18/08 , C08G18/28 , C08G18/44 , C08G18/50 , C14C11/00 , D06N3/14 , D21H19/62 , B05D3/02 , B05D3/00 , C14C5/00 , D06M19/00
CPC分类号： C08G18/0823 , C08G18/0804 , C08G18/0828 , C08G18/283 , C08G18/3228 , C08G18/3231 , C08G18/3855 , C08G18/44 , C08G18/5072 , C08G18/73 , C14C11/006 , D06N3/14 , D21H19/62 , Y10T428/31551 , Y10T428/31558 , Y10T428/31591
摘要： The invention relates to the use of coating compositions to prepare coatings having water vapor permeabilities of at least 2500 g/m.sup.2 per day (DS 2109 TM1 method) containing (A) a polyurethane containing (1) 0.1 to 75 meq/100 g of ionic groups and (2) 11 to 50% by weight of --(CH.sub.2 CH.sub.2 O).sub.n -- units (wherein n is 2 to 25) incorporated into the main chain prepared from reactive components comprising (I) one or more polyisocyanates, (II) one or more polyols having a number average molecular weight of 350 to 5000, with the proviso that if any such polyol is a sulfonated polyether diol having the formula ##STR1## in which R is hydrogen or an organic group having 1 to 8 carbon atoms, m and n are 1 to 10, p is 0, 1, or 2, and M is ammonium or alkali metal cation, then an additional ethoxy-containing polyether polyol must also be present, and (III) one or more chain lengthening agents having a molecular weight of 32 to 349; and (B) 30 to 80% by weight, based on the sum of components (A) and (B), of an aqueous phase.
摘要翻译：本发明涉及涂料组合物用于制备具有每天至少2500g / m 2的水蒸汽渗透性（DS 2109 TM1方法）的涂层的用途，其包含（A）含有（1）0.1至75meq / 100g离子的聚氨酯基团和（2）由反应性组分制备的主链中的 - （CH 2 CH 2 O）n - 单元（其中n为2至25）的11至50重量％，其包含（I）一种或多种多异氰酸酯，（II）一种或多种更多的数均分子量为350〜5000的多元醇，条件是如果任何这样的多元醇是具有1至8个碳原子的式基的磺化聚醚二醇，则m和n为1至10，p为0,1 或2，M是铵或碱金属阳离子，则还必须含有另外的含乙氧基的聚醚多元醇，和（III）一种或多种分子量为32至349的链延长剂; 和（B）基于水相的组分（A）和（B）的总和为30至80重量％。

5. 发明授权

US5093497A Process for the preparation of a substituted or unsubstituted quinacridone 失效
标题翻译：制备取代或未经取代的喹哪啶酮的方法
公开(公告)号：US5093497A
公开(公告)日：1992-03-03
申请号：US597276
申请日：1990-10-12
申请人： Detlef-Ingo Schutze , Reinold Schmitz
发明人： Detlef-Ingo Schutze , Reinold Schmitz
IPC分类号： C09B48/00
CPC分类号： C09B48/00
摘要： Process for the preparation of a substituted or unsubstituted quinacridone by oxidation of a substituted or unsubstituted dihydroquinacridone with oxygen or an oxygen-containing gas in the presence of alkali, a solvent or diluent and an oxygen transfer agent, which is characterized in that the oxidation is carried out in the presence of a quaternary ammonium compound.
摘要翻译：通过在碱，溶剂或稀释剂和氧转移剂存在下用氧或含氧气体氧化取代或未取代的二氢喹吖啶酮来制备取代或未取代的喹吖啶酮的方法，其特征在于氧化为在季铵化合物的存在下进行。

6. 发明授权

US4981997A Process for the preparation of 2,5-diarylaminoterephthalic acids 失效
标题翻译：制备2,5-二芳基氨基对苯二甲酸的方法
公开(公告)号：US4981997A
公开(公告)日：1991-01-01
申请号：US414825
申请日：1989-09-29
申请人： Detlef-Ingo Schutze , Reinold Schmitz
发明人： Detlef-Ingo Schutze , Reinold Schmitz
IPC分类号： C07C227/16 , C07C227/18 , C07C229/62
CPC分类号： C07C229/62 , C07C227/18
摘要： A process for the preparation of 2,5-diarylaminoterephthalic acids by oxidation of 2,5-diarylamino-3,6-dihydroterephthalic acid esters using oxygen or oxygen-containing gases, preferably air, in alcoholic-alkaline or alcoholic-aqueous-alkaline solution or suspension in the presence of an oxygen-transferring agent and working up to give the 2,5-diarylaminoterephthalic acids, characterized in that the oxidation is carried out in the presence of quaternary ammonium compound.
摘要翻译：通过使用含氧气体或含氧气体（优选空气）在醇 - 碱性或醇 - 水 - 碱性溶液中氧化2,5-二芳基氨基-3,6-二氢对苯二甲酸酯来制备2,5-二芳基氨基对苯二甲酸的方法或悬浮液，并进行处理，得到2,5-二芳基氨基对苯二甲酸，其特征在于在季铵化合物的存在下进行氧化。

7. 发明授权

US4652660A Process for preparing a thioindigo derivatives comprising cyclizing in a liquid mixture of an aluminium halide an alkali metal halide, and a carboxamide or sulfonamide 失效
标题翻译：制备硫靛衍生物的方法，其包括在卤化铝和碱金属卤化物的液体混合物中环化，以及羧酰胺或磺酰胺
公开(公告)号：US4652660A
公开(公告)日：1987-03-24
申请号：US755048
申请日：1985-07-15
申请人： Detlef-Ingo Schutze , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Klaus Wunderlich
IPC分类号： C09B7/10 , C07D333/64 , C07D409/04
CPC分类号： C09B7/10
摘要： Process for preparing thioindigo compounds of the formula ##STR1## in which A and B denote identical or different, optionally substituted benzene rings or benzene rings to which may be joined further carbocyclic and heterocyclic rings,characterized in that compounds of the formulae ##STR2## in which A and B have the abovementioned meaning andX denotes halogen, such as bromine and preferably chlorine,are reacted in a liquid mixture of an aluminium halide, an alkali metal halide and a carboxamide or sulphonamide, and the resulting intermediate product is subsequently, if desired after prior isolation, oxidized in a manner known per se, and the batch is worked up for the compounds of the formula (I).
摘要翻译：制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其中可以连接有碳环和杂环，其特征在于式其中A和B具有上述含义并且X表示卤素如溴，优选氯，在卤化铝，碱金属卤化物的液体混合物中反应的图像（IIa）和/或

8. 发明授权

US4892950A Process for the preparation of naphthalene-1,8-dicarboximides 失效
标题翻译：萘-1,8-二羧酰亚胺的制备方法
公开(公告)号：US4892950A
公开(公告)日：1990-01-09
申请号：US204468
申请日：1988-06-09
申请人： Detlef-Ingo Schutze , Klaus Wunderlich , Karl-Heinz Reinhardt , Martin Wienkenhover
发明人： Detlef-Ingo Schutze , Klaus Wunderlich , Karl-Heinz Reinhardt , Martin Wienkenhover
IPC分类号： C07D221/14
CPC分类号： C07D221/14
摘要： Process for the preparation of naphthalene-1,8-dicarboximide which is optionally substituted in the naphthalene ring, characterized in that naphthalene-1,8-dicarboxylic anhydride which is optionally substituted in the naphthalene ring is reacted with an ammonium salt in an aqueous medium at a pH near to the neutral point, the reaction mixture is then acidified to a pH of 1 to 4 and the pH is subsequently adjusted to a value near to the neutral point.
摘要翻译：在萘环中任选取代的萘-1,8-二羧酰亚胺的制备方法，其特征在于在萘环中任选取代的萘-1,8-二羧酸酐与含水介质中的铵盐反应在接近中性点的pH下，将反应混合物酸化至1至4的pH，随后将pH调节至接近中性点的值。

9. 发明授权

US4190726A Polycyclic dyestuffs 失效
标题翻译：多环染料
公开(公告)号：US4190726A
公开(公告)日：1980-02-26
申请号：US915020
申请日：1978-06-13
申请人： Detlef-Ingo Schutze , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Klaus Wunderlich
IPC分类号： C09B57/00 , C09B57/08 , C07D471/22
CPC分类号： C09B57/08 , Y10S8/922
摘要： In spite of their pigment character, dyestuffs of the formula ##STR1## are outstandingly suitable for dyeing synthetic fibres, in particular polyester fibres, by customary methods, strong yellow dyeings with good fastness to light and sublimation being obtained. In the abovementioned formula:R.sub.1 and R.sub.3 denote hydrogen, alkyl, aralkyl, alkoxyalkyl, alkoxycarbonyl, alkoxycarbonylalkyl or aryl,R.sub.2 and R.sub.4 denote alkylcarbonyl, arylcarbonyl, alkoxycarbonyl, --CN or --CONX.sub.1 X.sub.2,X.sub.1 denotes hydrogen, alkyl, aralkyl, aryl or cycloalkyl andX.sub.2 denotes hydrogen or alkyl.
摘要翻译：尽管它们具有颜料特性，但是通过常规方法对式（IMAGE）的染料非常适合用于染色合成纤维，特别是聚酯纤维，得到具有良好的耐光牢度和升华性的强黄色染色。在上述式中：R 1和R 3表示氢，烷基，芳烷基，烷氧基烷基，烷氧基羰基，烷氧基羰基烷基或芳基，R 2和R 4表示烷基羰基，芳基羰基，烷氧基羰基，-CN或-CONX 1 X 2，X 1表示氢，烷基，芳烷基，芳基或环烷基 X2表示氢或烷基。

10. 发明授权

US4260778A Process for the preparation of thioindigo compounds 失效
标题翻译：制备硫靛化合物的方法
公开(公告)号：US4260778A
公开(公告)日：1981-04-07
申请号：US40520
申请日：1979-05-21
申请人： Detlef-Ingo Schutze , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Klaus Wunderlich
IPC分类号： C09B7/10
CPC分类号： C09B7/10
摘要： Process for the preparation of thioindigo compounds of the formula ##STR1## in which A and B designate identical or different optionally substituted benzene rings or benzene rings onto which further carbocyclic and heterocyclic rings are fused,characterized in that compounds of the formula ##STR2## in which A and B have the meaning indicated above andX designates halogen, such as bromine and, preferably, chlorine,are reacted in a liquid mixture of an aluminium halide, an alkali metal halide and SO.sub.2 and the resulting intermediate product is then oxidized in a manner which is in itself known, if appropriate after first being isolated, and the mixture is worked up to give the compounds of the formula (I).
摘要翻译：制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其上还有碳环和杂环稠合，其特征在于式（IIa）（IIb）其中A和B具有上述含义，X表示卤素，例如溴，优选氯，在卤化铝，碱金属卤化物的液体混合物中反应然后将所得中间产物以本身已知的方式氧化，如果在首次分离后适当，则将其混合，得到式（I）化合物。

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