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    • 1. 发明专利
    • 粉体の付着力測定方法及び恒温恒湿空間形成冶具
    • 粉末粘合剂测量方法和热成像室成型
    • JP2016156678A
    • 2016-09-01
    • JP2015033908
    • 2015-02-24
    • 日本ゼオン株式会社
    • 渡辺 香挾間 尚宏細野 優人酒井 幹夫
    • G01Q30/10G01Q30/12G01Q60/28
    • 【課題】粉体の付着力を精度良く測定することができる粉体の付着力測定方法を提供する。 【解決手段】原子間力顕微鏡2を用いて粉体7,13の付着力を測定する粉体の付着力測定方法において、カンチレバー6の探針6aに前記粉体を取り付ける工程と、前記原子間力顕微鏡の測定領域18内に恒温恒湿空間20を形成するための恒温恒湿空間形成冶具12を前記原子間力顕微鏡に取り付ける工程と、前記粉体が固定された基材11を前記恒温恒湿空間内に配置する工程と、少なくとも前記カンチレバー及び前記基材を前記恒温恒湿空間内に収容し、前記恒温恒湿空間を密閉する工程と、前記恒温恒湿空間内の温度と湿度を制御する工程と、前記恒温恒湿空間内において、前記探針に取り付けられた前記粉体を前記基材上に固定された前記粉体に付着させた後に引き離すときの前記探針のたわみ量を検出する工程と、該検出結果に基づいて前記粉体の付着力を求める工程とを含む。 【選択図】図1
    • 要解决的问题:提供一种用于精确测量粉末粘合性的粉末粘合性测量方法。溶解性:用原子力显微镜2测量粉末7和13的粘合性的粉末粘附性测量方法包括:将粉末设置在探针6a上 悬臂6; 设置用于在原子力显微镜的测量区域18中的原子力显微镜上形成恒温恒湿室20的恒温恒湿室形成夹具12; 将其上固定有粉末的基材11设置在恒温恒湿室内; 至少在恒温恒湿室内容纳悬臂和基材,并密封恒温恒湿室; 控制恒温恒湿室的温度和湿度; 在将探针上的粉末与固定在基材上的粉末接触之后,检测在探针上的粉末和基材上的粉末在热恒湿室中分离时探针的挠曲 ; 并根据检测结果确定粉末的粘合性。图1:
    • 2. 发明专利
    • Sample holder for medium and low atomic force microscope
    • 中等和低原子力显微镜样品座
    • JP2013044743A
    • 2013-03-04
    • JP2011199979
    • 2011-08-26
    • Kenjiro Kimura建次郎 木村
    • SAKA TATSUNORIKIMURA KENJIRO
    • G01N1/28G01Q30/10
    • PROBLEM TO BE SOLVED: To provide a sample holder capable of cooling a sample to a medium and low region after attaining the noise level of standard enabling high resolution observation in an atomic force microscope (AFM).SOLUTION: A sample holder includes a heat sink 14 which adheres a measuring object 2 to the cooling side of Peltier elements 1 and is made of a metal material including copper on the heat radiation side. The sample holder includes a DC power supply 8 which controls the temperature of the Peltier elements 1 and the measuring object 2, and a temperature measurement part 10. The temperature measured by the temperature measurement part 10 is controlled so as to become constant.
    • 要解决的问题:提供一种能够在获得原子力显微镜(AFM)中的能够进行高分辨率观察的标准的噪声水平之后,将样品冷却到中等和低压区域的样品保持器。 解决方案:样品架包括将测量对象2粘附到珀耳帖元件1的冷却侧的散热器14,并且由热辐射侧的包含铜的金属材料制成。 样品保持器包括控制珀耳帖元件1和测量对象2的温度的直流电源8和温度测量部件10.由温度测量部件10测量的温度被控制为恒定。 版权所有(C)2013,JPO&INPIT
    • 5. 发明专利
    • Scanning probe microscope
    • 扫描探针显微镜
    • JP2008122326A
    • 2008-05-29
    • JP2006309243
    • 2006-11-15
    • Jeol Ltd日本電子株式会社
    • AOKI SUSUMU
    • G01Q30/08G01Q30/10G01Q30/20G01Q60/24
    • PROBLEM TO BE SOLVED: To prevent deterioration in resolution of an unevenness image of a sample surface caused from temperature changes in a room.
      SOLUTION: A sample scanner 5 with a tube scanner 6 mounts a sample holder 7. The sample scanner 5 is mounted in a sample driving mechanism 3 via a sample stage 4. The stage driving mechanism 3 is supported by a base unit 1. A cantilever 12 mounted to an SPM head 10 right over a sample 8 attached to the sample holder 7 is arranged; a probe 14 attached to the distal end of the cantilever 12 is opposed to the probe 14; physical quantities acting between the probe 14 and the sample 8 is detected by relatively scanning the probe 14 and the sample 8; then, an unevenness image of the sample is obtained based on the physical quantities. The base unit 1 is supported by a chamber 21 made of a thermally insulating material so as to surround a bottom and sides thereof.
      COPYRIGHT: (C)2008,JPO&INPIT
    • 要解决的问题:为了防止由室内温度变化引起的样品表面的不均匀图像的分辨率的劣化。 解决方案:具有管扫描器6的样品扫描器5安装样品架7.样品扫描器5经由样品台4安装在样品驱动机构3中。载物台驱动机构3由基体单元1 安装在安装在样品架7上的样品8上的SPM头10上的悬臂12; 附接到悬臂12的远端的探针14与探针14相对; 通过相对扫描探针14和样品8来检测作用在探针14和样品8之间的物理量; 然后,基于物理量获得样品的不均匀图像。 基座单元1由围绕其底部和侧面的由隔热材料制成的室21支撑。 版权所有(C)2008,JPO&INPIT
    • 7. 发明专利
    • Scanning probe microscope
    • 扫描探针显微镜
    • JP2006284598A
    • 2006-10-19
    • JP2006148810
    • 2006-05-29
    • Sii Nanotechnology Incエスアイアイ・ナノテクノロジー株式会社
    • ANDO KAZUNORI
    • G01Q20/02G01Q30/08G01Q30/10G01Q30/16G01Q30/20G01Q60/24
    • PROBLEM TO BE SOLVED: To adjust a reachable distance of a laser reflection light to an optical position detector, and facilitate measurement, by changing a laser irradiation position and a laser irradiation angle in a vacuum, in a heating or in a cooling state, as is even if a cantilever is bent by a thermal influence, wherein a laser generator and the optical position detector are installed outside a vacuum vessel.
      SOLUTION: The laser generator 61 and the optical position detector 8 are installed outside the vacuum vessel 63, and a sample stage 65 is placed inside the vacuum vessel 63, and mounts, heats or cools a sample 9 so that the irradiation position and irradiation angle to a laser reflection face are changed, on the spot, by the laser generator 61 and the optical position detector 8, which are installed outside the vacuum vessel 63 during a evacuating, heating or cooling state.
      COPYRIGHT: (C)2007,JPO&INPIT
    • 要解决的问题:通过在加热或冷却中改变激光照射位置和激光照射角度来调整激光反射光到光学位置检测器的可达距离,并且便于测量 状态,即使悬臂被热影响弯曲,其中激光发生器和光学位置检测器安装在真空容器的外部。 解决方案:激光发生器61和光学位置检测器8安装在真空容器63的外部,样品台65放置在真空容器63的内部,并安装,加热或冷却样品9,使得照射位置 并且通过在抽真空,加热或冷却状态下安装在真空容器63外部的激光发生器61和光学位置检测器8在现场改变与激光反射面的照射角度。 版权所有(C)2007,JPO&INPIT
    • 10. 发明专利
    • Scanning probe microscope and measuring method using it
    • 扫描探针显微镜和使用它的测量方法
    • JP2005241524A
    • 2005-09-08
    • JP2004053725
    • 2004-02-27
    • Sii Nanotechnology Incエスアイアイ・ナノテクノロジー株式会社
    • ANDO KAZUNORINIHEI AMIKO
    • G01Q30/08G01Q30/10G01Q30/20G01Q60/24G21K7/00G01N13/10
    • G01Q30/18G01Q30/20
    • PROBLEM TO BE SOLVED: To provide a scanning probe microscope capable of measuring the surface shape of a sample and the physical propertes of the sample with high resolving power to keep them even if the evaporative component of an object to be heated is evaporated and capable of measuring a change in physical properties at every heating temperature without causing the heat history of the sample. SOLUTION: The scanning probe microscope is equipped with a cantilever having a probe provided to its leading end, a heating means for heating the sample, a sample moving means for moving the sample and a shield means for shielding the cantilever and the sample. The shield means is interposed between the cantilever and the sample in heating the sample and not interposed between the cantilever and the sample at the time of measurement of the sample. COPYRIGHT: (C)2005,JPO&NCIPI
    • 要解决的问题:提供一种能够以高分辨能力测量样品的表面形状和样品的物理特性的扫描探针显微镜,以便即使被加热物体的蒸发组分蒸发也能保持它们 并且能够在每个加热温度下测量物理性能的变化,而不会引起样品的热历史。 解决方案:扫描探针显微镜配备有悬臂,其具有设置在其前端的探针,用于加热样品的加热装置,用于移动样品的样品移动装置和用于屏蔽悬臂和样品的屏蔽装置 。 在测量样品时,屏蔽装置在加热样品之间插入在悬臂和样品之间,并且不夹在悬臂和样品之间。 版权所有(C)2005,JPO&NCIPI