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    • 2. 发明专利
    • Method for producing exhaust gas catalyst by using coaxial vacuum arc vapor deposition source
    • 使用同轴真空蒸气沉积源生产排气催化剂的方法
    • JP2010142699A
    • 2010-07-01
    • JP2008320327
    • 2008-12-16
    • Kumamoto UnivUlvac Japan Ltd国立大学法人 熊本大学株式会社アルバック
    • MACHIDA MASATOAGAWA YOSHIAKITSUKAHARA NAOKIMURAKAMI HIROHIKO
    • B01J37/02B01D53/94B01J23/63C23C14/14C23C14/24F01N3/10F01N3/28
    • PROBLEM TO BE SOLVED: To provide method for depositing a nanoparticle of an exhaust gas catalyst, and a method for producing the exhaust gas catalyst. SOLUTION: A pulse voltage is impressed between a trigger electrode 13 and a cathode 12 in a vacuum atmosphere by using a coaxial vacuum arc vapor deposition source 1 to generate trigger discharge. A capacitor and a DC power source are connected to each of the cathode 12 and an anode 11, and a DC discharge voltage of 60-100 V is impressed while keeping the capacitance of the capacitor within 360-1,080 μF to induce arc discharge intermittently. Charged particles of a catalytic metal to be produced are supplied to/vapor-deposited on the surface of a carrier being alumina powder or other alumina powder, in which an oxide of a metal consisting of zirconium or lanthanoid is mixed, to obtain the catalyst consisting of the catalytic metal nanoparticle-deposited carrier. COPYRIGHT: (C)2010,JPO&INPIT
    • 待解决的问题:提供沉积废气催化剂的纳米颗粒的方法,以及废气催化剂的制造方法。 解决方案:通过使用同轴真空电弧气相沉积源1在真空气氛中在触发电极13和阴极12之间施加脉冲电压以产生触发放电。 将电容器和直流电源连接到阴极12和阳极11中的每一个,并且施加60-100V的直流放电电压,同时将电容器的电容保持在360-1,080μF内以间歇地引起电弧放电。 将要生产的催化金属的带电粒子供应至/蒸镀在氧化铝粉末或其它氧化铝粉末的载体的表面上,其中由锆或镧系元素组成的金属的氧化物混合,得到催化剂组成 的催化金属纳米颗粒沉积载体。 版权所有(C)2010,JPO&INPIT
    • 4. 发明专利
    • Manufacturing method of graphite nanofiber
    • 石墨纳米纤维的制造方法
    • JP2009084072A
    • 2009-04-23
    • JP2007252172
    • 2007-09-27
    • Ulvac Japan Ltd株式会社アルバック
    • TSUKAHARA NAOKIMURAKAMI HIROHIKO
    • C01B31/04B01J23/745B01J23/889C01B31/02
    • PROBLEM TO BE SOLVED: To provide a manufacturing method of graphite nanofiber which can improve an electron emission property without giving damage to the carbon nanofiber itself. SOLUTION: The manufacturing method of graphite nanofiber has a step (P1) of depositing a membrane of a growing catalyst for graphite nanofiber onto a substrate, a step (P2) of growing the graphite nanofiber by supplying a raw material gas, and a step (P3) of heat-treating the grown graphite nanofiber using a treatment gas containing hydrogen. As the growing catalyst, iron, nickel, copper, cobalt, chromium, or an alloy containing one or more of these metals can be used. COPYRIGHT: (C)2009,JPO&INPIT
    • 要解决的问题:提供可以提高电子发射性能而不损害碳纳米纤维本身的石墨纳米纤维的制造方法。 石墨纳米纤维的制造方法具有将石墨纳米纤维的生长催化剂的膜沉积在基材上的工序(P1),通过供给原料气体来生长石墨纳米纤维的工序(P2),以及 使用含氢处理气体对生长的石墨纳米纤维进行热处理的工序(P3)。 作为生长催化剂,可以使用含有这些金属中的一种或多种的铁,镍,铜,钴,铬或合金。 版权所有(C)2009,JPO&INPIT
    • 5. 发明专利
    • Method for producing fine particle film
    • 生产细颗粒膜的方法
    • JP2008291319A
    • 2008-12-04
    • JP2007138557
    • 2007-05-25
    • Ulvac Japan Ltd株式会社アルバック
    • AGAWA YOSHIAKIYAMAGUCHI KOICHITSUKAHARA NAOKIMURAKAMI HIROHIKO
    • C23C14/24
    • PROBLEM TO BE SOLVED: To provide a method for producing a fine particle film by which a fine particle film uniform in particle size can be formed.
      SOLUTION: When a fine particle film of nano particle size is formed by using a coaxial type vacuum arc vapor deposition source 13, the discharge voltage between an anode electrode 21 and a cathode electrode 22 (a vapor deposition material 22A) is set in 50 to
    • 要解决的问题:提供可以形成颗粒尺寸均匀的细颗粒膜的细颗粒膜的制造方法。 解决方案:通过使用同轴型真空电弧气相沉积源13形成纳米粒径的微粒膜时,设置阳极电极21和阴极电极22(蒸镀材料22A)之间的放电电压 通过限制放电电压并限制放电时产生的电磁力的尺寸,可以避免从阳极电极21的开口21A释放的带电粒子中具有固定或更多粒子的巨大颗粒的共存 ,并且仅释放具有固定或更小粒度的细电荷粒子。 以这种方式,当衬底布置在与阳极21的开口相对的位置时,带电粒子到达衬底W,并且可以在衬底的表面上形成具有高膜质量的致密薄膜。 版权所有(C)2009,JPO&INPIT
    • 8. 发明专利
    • Method of forming electrode active material layer for lithium secondary battery
    • 形成用于锂二次电池的电极活性材料层的方法
    • JP2012054112A
    • 2012-03-15
    • JP2010196135
    • 2010-09-01
    • Ulvac Japan Ltd株式会社アルバック
    • FUKUDA YOSHIROMURAKAMI HIROHIKOTSUKAHARA NAOKI
    • H01M4/139C23C14/08H01M4/13H01M4/48
    • Y02E60/122
    • PROBLEM TO BE SOLVED: To provide a high productivity method of forming an electrode active material layer for a lithium secondary battery capable of forming an electrode active material layer of microcrystal vanadium pentoxide, where an amorphous structure and a layer crystal structure are mixed, in the form of a thin film on the surface of a base material made of an organic material of low heat resistance, and capable of attaining high battery performance when applied to a thin film lithium secondary battery.SOLUTION: A base material W is arranged in a processing chamber 11 with a target 2 containing vanadium, the processing chamber is evacuated to a predetermined pressure, the base material is held at a predetermined temperature equal to or lower than the heatproof temperature of the base material by heating or cooling, rare gas and oxygen gas are introduced into the processing chamber with predetermined partial-pressures, a plasma atmosphere is formed in the processing chamber by charging a predetermined power to the target and the target is sputtered thus forming a vanadium oxide film, i.e. an electrode active material layer.
    • 解决的问题:为了提供形成能够形成微晶五氧化二钒的电极活性物质层的锂二次电池的电极活性物质层的高生产率的方法,其中非晶结构和层状晶体结构被混合 在由耐热性低的有机材料构成的基材的表面上形成薄膜,并且当应用于薄膜锂二次电池时能够获得高的电池性能。 解决方案:将基材W布置在处理室11中,目标物2含有钒,将处理室抽真空至预定压力,基材保持在等于或低于耐热温度的预定温度 通过加热或冷却将稀有气体和氧气以预定的分压引入处理室中,通过向目标物充电预定的功率而在处理室中形成等离子体气氛,从而形成溅射靶 氧化钒膜,即电极活性物质层。 版权所有(C)2012,JPO&INPIT
    • 10. 发明专利
    • Method for embedding metallic material using coaxial vacuum arc vapor deposition source
    • 使用同轴真空蒸镀沉积源嵌入金属材料的方法
    • JP2009242825A
    • 2009-10-22
    • JP2008088134
    • 2008-03-28
    • Ulvac Japan Ltd株式会社アルバック
    • TSUKAHARA NAOKIMURAKAMI HIROHIKO
    • C23C14/14H01L21/285
    • PROBLEM TO BE SOLVED: To provide a method for embedding a metallic material in a trench or a hole having a fine opening and a high aspect ratio.
      SOLUTION: In a coaxial vacuum arc vapor deposition source 1, a cylindrical trigger electrode 13 and a cylindrical cathode electrode 12 having an evaporation material member 12a are arranged in a coaxially adjacently fixed state via a cylindrical electrical porcelain 15, and an anode electrode 11 is coaxially arranged around and apart from the cathode electrode. The coaxial vacuum arc vapor deposition source 1 is used to generate trigger discharge between the trigger electrode and the cathode electrode to intermittently induce arc discharge between the cathode electrode and the anode electrode to allow release of charged particles produced from the evaporation material member in a vacuum chamber to embed a metallic material in a trench or a hole.
      COPYRIGHT: (C)2010,JPO&INPIT
    • 要解决的问题:提供一种将金属材料嵌入沟槽或具有细孔和高纵横比的孔中的方法。 解决方案:在同轴真空电弧气相沉积源1中,具有蒸发材料构件12a的圆柱形触发电极13和圆柱形阴极12经由圆柱形电瓷15以同轴相邻固定的状态布置,阳极 电极11围绕和离开阴极同轴地布置。 同轴真空电弧气相沉积源1用于在触发电极和阴极之间产生触发放电,以间断地在阴极和阳极之间引起电弧放电,以允许在真空中释放由蒸发材料构件产生的带电粒子 将金属材料嵌入沟槽或孔中。 版权所有(C)2010,JPO&INPIT