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1. 发明专利

JP2013202306A Method and apparatus for decomposing dioxin in exhaust gas 有权
标题翻译：在排气中分解二氧化铅的方法和装置
公开(公告)号：JP2013202306A
公开(公告)日：2013-10-07
申请号：JP2012077016
申请日：2012-03-29
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社 , Tokyo Energy & Systems Inc , 株式会社東京エネシス
发明人： SHIMOJO MIKIO , KANAMORI SATORU , ITO KOICHI , KUSUNOKI TOSHIHARU
IPC分类号： A62D3/30 , A62D3/178 , A62D101/22 , B01D53/70 , B01D53/77
摘要： PROBLEM TO BE SOLVED: To provide a method for decomposing dioxin in an exhaust gas discharged from specific facilities such as an incinerator; and a portable apparatus used for the same.SOLUTION: A method for decomposing dioxin in an exhaust gas has: a gas absorbing step of causing a coolant to absorb the exhaust gas containing dioxin; and a decomposing step of decomposing the dioxin in the absorbed liquid by causing the absorbed liquid to circulate in a catalyst-filled device and irradiating the absorbed liquid with a microwave. The decomposing apparatus includes a gas absorbing device 10 for absorbing the dioxin in the exhaust gas; and a decomposing device 20 for decomposing the dioxin absorbed by the gas absorbing device. The gas absorbing device includes an absorbing tank for reserving an exhaust gas absorbing solvent, and a liquid cooler for cooling the absorbing solvent. The decomposing apparatus includes the catalyst-filled device for decomposing the dioxin absorbed by the absorbing solvent, the microwave processing device and the liquid circulation system.
摘要翻译：要解决的问题：提供从诸如焚化炉的特定设施排出的废气中分解二恶英的方法; 和用于其的便携式设备。解决方案：一种用于分解废气中二恶英的方法具有：使吸收含有二恶英的废气的冷却剂吸收气体的气体吸收步骤; 以及通过使吸收的液体在催化剂填充装置中循环并用微波照射被吸收的液体来分解吸收液体中的二恶英的分解步骤。分解装置包括用于吸收废气中的二恶英的气体吸收装置10; 以及用于分解由气体吸收装置吸收的二恶英的分解装置20。气体吸收装置包括用于储存废气吸收溶剂的吸收罐和用于冷却吸收溶剂的液体冷却器。分解装置包括用于分解被吸收溶剂吸收的二恶英的催化剂填充装置，微波处理装置和液体循环系统。

2. 发明专利

JP2013208510A Method for treating large-sized instrument contaminated with pcb and treatment device to be used for the same 有权
标题翻译：用于处理用PCB污染的大尺寸仪器和处理设备的方法
公开(公告)号：JP2013208510A
公开(公告)日：2013-10-10
申请号：JP2012078524
申请日：2012-03-30
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社 , Tokyo Energy & Systems Inc , 株式会社東京エネシス
发明人： SHIMOJO MIKIO , KANAMORI SATORU , FURUHASHI TETSUTARO , OGAWA HITOSHI , ITO KOICHI , OTSUKI SHIGERU , KUSUNOKI TOSHIHARU
IPC分类号： B09B5/00 , A62D3/178 , A62D3/30 , A62D101/22 , B01J19/12 , B08B3/08 , B09B3/00
摘要： PROBLEM TO BE SOLVED: To provide a method for treating a container that can be treated in a storage place in a large-sized high concentration instrument that is not easy to carry and is extremely hard to treat, and to provide a treatment device.SOLUTION: A method for treating a large-sized instrument contaminated with PCB is characterized by performing in parallel: a cleaning step of, while performing the circular cleaning of the inside of the large-sized instrument 1 contaminated with PCB by using a cleaning liquid, suitably extracting a predetermined amount of the cleaning liquid into a first buffer tank 2 from the cleaning liquid in use for cleaning, and newly supplying the cleaning liquid to the large-sized instrument 1 after the cleaning liquid is extracted to perform the circular cleaning; and a decomposition treatment step of transferring a part of the extracted cleaning liquid from the first buffer tank 2 to a feed liquid tank 3 for storing the cleaning liquid, adding an alkali to the cleaning liquid in the feed liquid tank 3, and then, while circulating the cleaning liquid through a catalyst filled device 4 that is filled with a PCB decomposition catalyst, irradiating the cleaning liquid with a microwave by a microwave treatment device 5 to decompose the PCB in the cleaning liquid, and returning the cleaning liquid circulated through the catalyst filled device to a treated liquid tank 6. A treatment device is used for the method for treating the large-sized instrument contaminated with PCB.
摘要翻译：要解决的问题：提供一种处理不易携带并且极难处理的大型高浓度仪器中的储存处所的容器的处理方法以及提供处理装置。用于处理被PCB污染的大型仪器的方法的特征在于并行执行：清洁步骤，在通过使用清洁液体对被PCB污染的大型仪器1的内部进行循环清洁时，适当地从用于清洗的清洗液中将预定量的清洗液提取到第一缓冲罐2中，并且在清洗液体被抽取之后将清洗液重新供给到大型仪器1中以进行循环清洗; 以及分解处理步骤，将一部分提取的清洗液从第一缓冲罐2转移到用于储存清洗液的进料液罐3，向进料液罐3中的清洗液添加碱，使清洗液循环通过填充有PCB分解催化剂的催化剂填充装置4，用微波处理装置5用微波照射清洗液，以分解清洗液中的PCB，并使通过催化剂循环的清洗液返回填充装置到经处理的液体罐6.处理装置用于处理被PCB污染的大型仪器的方法。

3. 发明专利

JP2013202314A Method and apparatus for decomposing organic halogen compound 审中-公开
标题翻译：用于分解有机卤化物的方法和装置
公开(公告)号：JP2013202314A
公开(公告)日：2013-10-07
申请号：JP2012077146
申请日：2012-03-29
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社 , Tokyo Energy & Systems Inc , 株式会社東京エネシス
发明人： SHIMOJO MIKIO , KANAMORI SATORU , FURUHASHI TETSUTARO , OGAWA HITOSHI , ITO KOICHI , OTSUKI SHIGERU , KUSUNOKI TOSHIHARU
IPC分类号： A62D3/30 , A62D3/178 , A62D101/22 , C07B35/06 , C07B37/06 , C07B61/00 , C07C25/18
摘要： PROBLEM TO BE SOLVED: To provide a method for decomposing an organic halogen compound and a decomposing apparatus, capable of decomposing an organic halogen compound remaining in a container of a large transformer in which a large amount of organic halogen compound contained in one batch of treatment liquid should be decomposed without causing fixation of a catalyst.SOLUTION: A method for decomposing an organic halogen compound includes: adding a hydrogen donor and an alkali compound to an organic halogen compound to prepare a mixed liquid; taking out all or some of the mixed liquid; allowing the taken mixed liquid to circulate in a catalyst-filled device; and irradiating the mixed liquid circulating in the catalyst-filled device with a microwave to decompose the organic halogen compound. In this method, the catalyst-filled device is formed by stacking a filling member layer on the top and an organic halogen compound decomposition catalyst layer on the bottom. The mixed liquid is introduced from the upper part of the catalyst layer on the top and discharged through the filling member layer on the bottom. A decomposing device is used for the method.
摘要翻译：要解决的问题：提供一种有机卤素化合物和分解装置的分解方法，其能够分解保留在一次处理中所含的大量有机卤素化合物的大型变压器的容器中的有机卤素化合物分解有机卤素化合物的方法包括：向有机卤素化合物中加入氢供体和碱化合物以制备混合液体; 取出全部或部分混合液体; 使得所采集的混合液体在催化剂填充装置中循环; 并用微波照射在催化剂填充装置中循环的混合液体以分解有机卤素化合物。在该方法中，催化剂填充装置通过在顶部堆叠填充构件层和底部的有机卤素化合物分解催化剂层而形成。混合液从顶部的催化剂层的上部引入，并通过底部的填充构件层排出。该方法使用分解装置。

4. 发明专利

JP2009233654A Cleaning method and cleaning system for contaminated apparatus 审中-公开
标题翻译：污染装置清洁方法和清洁系统
公开(公告)号：JP2009233654A
公开(公告)日：2009-10-15
申请号：JP2009006368
申请日：2009-01-15
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社
发明人： ITO KOICHI , KANAMORI SATORU , SHIMOJO MIKIO , UMEDA YOKO
IPC分类号： B09B3/00 , A62D3/178 , A62D3/34 , A62D101/22 , B01J23/44 , B08B3/02 , B08B3/08 , B08B9/093
摘要： PROBLEM TO BE SOLVED: To provide a cleaning method and cleaning system, capable of easily detoxifying a container and an inner member without using large-scale equipment after removing insulating oil from an apparatus containing the insulating oil containing an organic halogen compound and before separating the inner member such as a coil from the container (case) of a contaminated apparatus from which the organic halogen compound is not completely removed.
SOLUTION: Simultaneous execution of following processes is made possible: a jetting and cleaning process of filling cleaning liquid in the contaminated apparatus until a coil inside the apparatus is completely immersed in it, then jetting the cleaning liquid inside the contaminated apparatus from a cleaning liquid jetting nozzle disposed near the opening surface of the contaminated apparatus, and cleaning the inner surface of the apparatus; and a decomposing and cleaning process of circulating the cleaning liquid inside the contaminated apparatus while distributing it to a catalyst filled device filled with a catalyst capable of decomposing an organic halogen compound and decomposing the organic halogen compound that the cleaning liquid contains.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种清洁方法和清洁系统，其能够在从含有有机卤素化合物的绝缘油的装置中除去绝缘油之后不使用大型设备容易地对容器和内部构件进行解毒，以及在将内部构件（例如线圈）从有机卤素化合物未被完全去除的污染设备的容器（壳体）分离之前。解决方案：同时执行以下过程成为可能：在污染设备中填充清洁液体的喷射和清洁过程，直到设备内部的线圈完全浸入其中，然后将污染设备内的清洁液体从清洁液体喷射喷嘴，设置在污染设备的开口表面附近，并清洁设备的内表面; 以及将污染装置内的清洗液循环，同时将其分配到填充有能够分解有机卤素化合物的催化剂的催化剂填充装置并分解清洗液含有的有机卤素化合物的分解和清洁过程。版权所有（C）2010，JPO＆INPIT

5. 发明专利

JP2008194660A Method for detoxifying instrument containing built-in organic halogen compound 审中-公开
标题翻译：含有机有机卤素化合物的脱氧仪的方法
公开(公告)号：JP2008194660A
公开(公告)日：2008-08-28
申请号：JP2007051679
申请日：2007-03-01
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社
发明人： ITO KOICHI , SHIMOJO MIKIO , FURUHASHI TETSUTARO , ITOI MASAYUKI , UMEDA YOKO
IPC分类号： B09B3/00 , A62D3/30 , A62D3/37 , A62D101/22 , B01J23/44 , C07B35/06
CPC分类号： Y02W30/78
摘要： PROBLEM TO BE SOLVED: To provide a method for detoxifying an instrument containing built-in organic halogen compounds, which makes it possible to wash off organic halogen compounds contained in insulation oil remaining in/on a pole transformer and the like simply within a short time by neither using any special apparatus for decomposition nor producing harmful dioxins as by-products and to detoxify a pole transformer and the like before dismantlement.
SOLUTION: The method for detoxifying an instrument containing built-in organic halogen compounds comprises: the process of filling the instrument from which the insulation oil containing organic halogen oil has been removed with a solution prepared by mixing a hydrogen donor with an alkali compound; and the process of washing by eluting and decomposing organic halogen compounds remaining in the instrument by circulating the solution while flowing the solution throughout the catalytic filling apparatus and then continuing the circulation until the level of organic halogen compounds remaining in/on the instrument and the internal members thereof satisfies the criteria; whereby the solution is removed after the washing process and then the instrument is dismantled.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种使含有内装有机卤素化合物的仪器解毒的方法，其使得可以简单地将残留在极变压器中的/绝缘油中的有机卤素化合物等除去短时间内不得使用任何特殊的分解装置，也不会产生有害的二恶英作为副产品，并在拆除之前对杆式变压器等进行解毒。解决方案：含有内置有机卤素化合物的仪器的解毒方法包括：将含有有机卤素油的绝缘油从其中除去的仪器的填充方法与通过将氢供体与碱混合制备的溶液复合; 以及通过在将溶液流过整个催化填充装置的同时循环溶液洗脱和分解残留在仪器中的有机卤素化合物，然后继续循环直到仪器内部/内部的有机卤素化合物的水平和内部其成员满足标准; 从而在洗涤过程之后除去溶液，然后拆除仪器。版权所有（C）2008，JPO＆INPIT

6. 发明专利

JP2007105063A Method of decomposing organic halogen compound and microwave built-in type decomposition system 审中-公开
标题翻译：分解有机卤化物和微波内置式分解系统的方法
公开(公告)号：JP2007105063A
公开(公告)日：2007-04-26
申请号：JP2005231282
申请日：2005-08-09
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社
发明人： ITO KOICHI , OGAWA HITOSHI , SHIMOJO MIKIO , ITOI MASAYUKI , UMEDA YOKO
IPC分类号： A62D3/178 , A62D3/00 , A62D3/30 , A62D3/36 , A62D3/37 , A62D101/22 , C07B35/06
摘要： PROBLEM TO BE SOLVED: To provide a method and a system for decomposing an organic halogen compound, capable of detoxicating the oil, in which the organic halogen compound such as insulating oil used in a pole transformer is mixed, in a pole transformer container in a short period of time without requiring the labor of separating a catalyst and with a low possibility of generation of a side reaction product. SOLUTION: The method is for decomposing the organic halogen compound included in the oil filled or stored in the container. In the method, a mixture liquid obtained by adding a hydrogen donor and an alkaline compound to the oil including the halogen compound is circulated in the container while letting the mixture liquid into a catalyst filled device attached to a lid body of the container, and microwaves are applied to the mixed liquid inside the container to decompose the organic halogen compound in the oil. The microwave built-in type decomposition system comprises at least the lid body with the catalyst filled device and a microwave oscillator to be set inside the container which is filled with the oil or in which the oil is stored, and a feeding means for feeding the oil, etc. in the container to the catalyst filled device. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种分解有机卤素化合物的方法和系统，该有机卤素化合物能够使极性变压器中使用的诸如绝缘油的有机卤素化合物混合在一起的油分解，容器在短时间内不需要分离催化剂的劳动并且产生副反应产物的可能性低。解决方案：该方法用于分解填充或储存在容器中的油中包含的有机卤素化合物。在该方法中，通过向含有卤素化合物的油中添加氢供体和碱性化合物而得到的混合液在容器内循环，同时使混合液体进入附着于容器的盖体的催化剂填充装置，微波施加到容器内的混合液体中以分解油中的有机卤素化合物。微波内置型分解系统至少包括具有催化剂填充装置的盖体和设置在容器内部的充满油或其中储存油的微波振荡器，以及馈送装置油等容器中的催化剂填充装置。版权所有（C）2007，JPO＆INPIT

7. 发明专利

JP2007105062A Microwave applicator and method for decomposition using the same 审中-公开
标题翻译：微波加热器及其分解方法
公开(公告)号：JP2007105062A
公开(公告)日：2007-04-26
申请号：JP2005231281
申请日：2005-08-09
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社
发明人： ITO KOICHI , OGAWA HITOSHI , SHIMOJO MIKIO , ITOI MASAYUKI , TEZUKA HIROKO , UMEDA YOKO
IPC分类号： A62D3/178 , A62D3/30 , A62D3/36 , A62D101/22 , B01J19/12 , C07B35/06 , C07B37/06 , C07C25/18
摘要： PROBLEM TO BE SOLVED: To provide a microwave applicator capable of improving the efficiency in using microwaves in the chemical reaction using microwaves and reducing the time necessary for the reaction thereby, and a method for decomposition using the same.
SOLUTION: The microwave applicator for chemical reaction is characterized by a reflection plate for reflecting microwaves oscillated or transmitted from a microwave oscillator in a fixed direction. A catalyst layer is disposed inside the microwave applicator with the reflection plate, and an organic halogen compound is decomposed by letting a mixture liquid including the organic halogen compound flow in the catalyst layer and applying microwaves to the mixture liquid via the reflection plate.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种能够提高使用微波的化学反应中使用微波的效率以及由此减少反应所需的时间的微波施加器及其分解方法。解决方案：用于化学反应的微波施加器的特征在于用于反射微波从微波振荡器沿固定方向振荡或发射的反射板。催化剂层设置在具有反射板的微波施加器内部，通过使包含有机卤素化合物的混合液在催化剂层中流动并通过反射板向混合液体施加微波，分解有机卤素化合物。版权所有（C）2007，JPO＆INPIT

8. 发明专利

JP2010259496A Decomposition treatment method for organic halogen compound and decomposition treatment device 审中-公开
标题翻译：有机卤化物化合物和分解处理装置的分解处理方法
公开(公告)号：JP2010259496A
公开(公告)日：2010-11-18
申请号：JP2009110880
申请日：2009-04-30
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社
发明人： ITO KOICHI , SHIMOJO MIKIO , KANAMORI SATORU , UMEDA YOKO
IPC分类号： A62D3/178 , A62D3/34 , A62D3/36 , A62D3/37 , A62D101/22 , B01J23/44 , C07C25/18
摘要： PROBLEM TO BE SOLVED: To provide a decomposition treatment method for organic halogen compounds and a decomposition treatment device for easily detoxifying an oil in which an organic halogen compound such as an insulating oil used in a pole-mounted transformer is mixed in a short time and for showing a low possibility of generating side reaction products.
SOLUTION: In the decomposition treatment method for decomposing the organic halogen compounds contained in the oil filled or kept in a container 1, the organic halogen compound is decomposed by repeating the operation of preparing a mixture liquid 2 by adding a hydrogen donor and an alkali compound to the oil containing the organic halogen compound, of cooling the mixture liquid 2, heated by microwaves applied in circulating in a catalyst filled device 4, in a liquid accumulation in a lower part of the catalyst tank 7 after the mixture liquid 2 is circulated in the catalyst filled device 4 disposed in an upper part of a catalyst tank 7, and of circulating the mixture liquid in the catalyst filled device 4 again.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种有机卤素化合物的分解处理方法和用于容易地将油中有机卤素化合物如极性安装的变压器中使用的绝缘油混合的油的分解处理装置短时间并且产生副反应产物的可能性低。解决方案：在用于分解填充或保存在容器1中的油中的有机卤素化合物的分解处理方法中，有机卤素化合物通过重复制备混合液2的操作而分解，通过加入氢供体和将含有有机卤素化合物的油的碱性化合物冷却，在混合液2之后，在催化剂填充装置4的循环中施加的微波加热的混合液2在催化剂罐7的下部积液在设置在催化剂罐7的上部的催化剂填充装置4中循环，并再次使催化剂填充装置4中的混合液循环。版权所有（C）2011，JPO＆INPIT

9. 发明专利

JP2008194063A Method of degrading highly-concentrated organic chlorine compound 有权
标题翻译：降低高浓度有机氯化合物的方法
公开(公告)号：JP2008194063A
公开(公告)日：2008-08-28
申请号：JP2007003964
申请日：2007-01-12
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社
发明人： ITO KOICHI , SHIMOJO MIKIO , KANAMORI SATORU , OTSUKI SHIGERU , UMEDA YOKO
IPC分类号： A62D3/36 , A62D3/178 , A62D3/30 , A62D101/22 , B01D53/86 , C07B35/06 , C07C25/18
摘要： PROBLEM TO BE SOLVED: To provide a method of degrading a highly-concentrated organic chlorine compound, reusing a reaction solution after the degradation treatment and reducing the treatment cost for further facilitating the degradation treatment of the highly-concentrated organic chlorine compound.
SOLUTION: At least one kind of catalyst selected from a carbon crystal compound and a compound with metal on a carrier is filled in a column, and while letting the reaction solution comprising an organic chlorine compound including polychlorinated biphenyl of at least 50 mass%, a hydrogen feeding solvent and an alkali compound flow through the column filled with the catalyst, the organic chlorine compound is dechlorinated. Then, a new organic chlorine compound and an alkali compound of 0.8-1.5 equivalent to the organic chlorine compound (to chlorine) are added to the solution after the dechlorination reaction, and the highly-concentrated organic chlorine compound is dechlorinated while reusing the reaction solution.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供一种降解高浓度有机氯化合物的方法，在降解处理后重新使用反应溶液，降低处理成本，进一步促进高浓度有机氯化合物的降解处理。解决方案：将选自碳晶体化合物和载体上的金属化合物的至少一种催化剂填充在柱中，并且在使含有至少50质量份的包含多氯联苯的有机氯化合物的反应溶液％，进料溶剂和碱性化合物流过填充有催化剂的柱，有机氯化合物脱氯。然后，在脱氯反应后，向溶液中加入新的有机氯化合物和0.8〜1.5当量的有机氯化合物（至氯）的碱性化合物，高浓度有机氯化合物在再次使用反应溶液的同时脱氯。版权所有（C）2008，JPO＆INPIT

10. 发明专利

JP2007306948A Method of decomposing treatment of low concentration organic halogen compound 审中-公开
标题翻译：分解低浓度有机卤化物化合物的方法
公开(公告)号：JP2007306948A
公开(公告)日：2007-11-29
申请号：JP2006083880
申请日：2006-03-24
申请人： Tokyo Electric Power Co Inc:The , 東京電力株式会社
发明人： ITO KOICHI , SHIMOJO MIKIO , OGAWA HITOSHI , ITOI MASAYUKI , KANAMORI SATORU , UMEDA YOKO
IPC分类号： A62D3/34 , A62D101/22 , C07B35/06
摘要： PROBLEM TO BE SOLVED: To provide a method of decomposing a low concentration organic halogen compound for performing from decomposition to recovery of an oil by recovering a solvent to reuse it after decomposing a small amount of the organic halogen compound in an oil such as an insulating oil and by further recovering the treated oil for the reuse.
SOLUTION: The method of decomposing a low concentration organic halogen compound comprises the following processes: (A) a process 101 of mixing the oil containing the organic halogen compound with an alkaline substance and a hydrogen donor, (B) a process 102 of decomposing the organic halogen compound by bringing the obtained mixed solution into contact with a catalyst, (C) a process 103 of recovering the hydrogen donor and a decomposed product having a low boiling point by distilling the obtained decomposed solution under reduced pressure, and (D) a process 104 of separating the oil from water by neutralizing the residue after the reduced-pressure distillation with an acid and by washing with water.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种低分子有机卤素化合物的分解方法，其通过在分解少量的油中的有机卤素化合物之后，通过回收溶剂进行回收来重新使用，从而分解成油来回收油，例如作为绝缘油，并进一步回收处理过的油以便再利用。解决方案：分解低浓度有机卤素化合物的方法包括以下方法：（A）将含有机卤素化合物的油与碱性物质和氢供体混合的方法101，（B）方法102 通过使所得到的混合溶液与催化剂接触来分解有机卤素化合物，（C）通过在减压下蒸馏得到的分解溶液，回收氢供体和低沸点的分解产物的方法103，和 D）通过用酸中的残余物进行中和，并用水洗涤来分离油与水的方法104。版权所有（C）2008，JPO＆INPIT

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