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1. 发明专利

JP2002254086A METHOD FOR TREATING WASTE WATER CONTAINING FLUORINE 审中-公开
公开(公告)号：JP2002254086A
公开(公告)日：2002-09-10
申请号：JP2001371241
申请日：2001-12-05
申请人： TOSHIBA CORP , OKUTAMA KOGYO CO LTD
发明人： TAKEDA MAKOTO , HAYASHI MASARU , KINOSHITA HIROAKI , HASEGAWA AKIRA , MANNAMI ICHIRO , KUREHA SHOZO , YAMASHITA KAZUO , FURUKAWA TAKAHISA
IPC分类号： C02F1/28 , C02F1/58
摘要： PROBLEM TO BE SOLVED: To provide a method for treating waste water containing fluorine, being capable of reducing the fluorine concentration below the environmental quality standard by removing the fluorine from the waste water containing the fluorine of the low concentration. SOLUTION: The method for treating the waste water containing the fluorine in which the fluorine concentration in the treated waste water is reduced by bringing the waste water containing the fluorine as the treated water into contact with calcium hydroxide as a treatment agent and making the treatment agent adsorb the fluorine in the treated water. The calcium hydroxide as the treatment agent is characterized by having a specific surface area of 20 m /g or more if a carbon dioxide treatment is not carried out as an after-treatment.

2. 发明专利

JP2003024953A Method for treating water containing fluorine 审中-公开
标题翻译：用于处理含水氟的方法
公开(公告)号：JP2003024953A
公开(公告)日：2003-01-28
申请号：JP2001214716
申请日：2001-07-16
申请人： Toshiba Corp , 株式会社東芝
发明人： HAYASHI MASARU , TAKEDA MAKOTO , HASEGAWA AKIRA , KINOSHITA HIROAKI
IPC分类号： C02F1/58
摘要： PROBLEM TO BE SOLVED: To provide an economical method for treating wastewater containing fluorine which can meet severe wastewater standards by a simple process.
SOLUTION: In order to decrease a fluorine concentration in wastewater, a mixture of calcium hydroxide and calcium phosphate is prepared by adding a phosphoric acid raw material into calcium hydroxide slurry. The mixture is used to react with fluorine, to adsorb it, and to remove it at a low running cost. In addition, gas containing carbon dioxide is introduced into the wastewater to generate calcium carbonate to adsorb fluorine so that the concentration of fluorine is decreased.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供一种处理含氟废水的经济方法，通过简单的工艺可以达到严格的废水标准。解决方案：为了降低废水中的氟浓度，通过将磷酸原料加入到氢氧化钙浆料中制备氢氧化钙和磷酸钙的混合物。该混合物用于与氟反应以吸附，并以低运行成本除去。此外，含有二氧化碳的气体被引入废水中以产生碳酸钙以吸附氟，使得氟的浓度降低。

3. 发明专利

JP2001247627A FLUORORESIN MOLDED PRODUCT, FLUORORESIN AND METHOD FOR PRODUCING FLUORORESIN 失效
公开(公告)号：JP2001247627A
公开(公告)日：2001-09-11
申请号：JP2000333918
申请日：2000-10-31
申请人： TOSHIBA CORP
发明人： TAKENAKA MIYUKI , YAMADA YUJI , TATEBE TETSUYA , HAYASHI MASARU , KOZUKA SHOJI , SAKAI KIMITO , OMORI HIROFUMI , MORITA MASAAKI
IPC分类号： C08J5/00 , B29C43/02 , C08F6/00 , C08F14/18
摘要： PROBLEM TO BE SOLVED: To provide a fluororesin molded product prevented from secondarily contaminating surroundings by impurities and the like. SOLUTION: In a fluororesin molded product 10 obtained by integral molding of a plurality of fluororesin particles, the number of unstable terminal groups per unit surface of the particle is in the range of 1 to 10 assuming that the number of unstable terminal groups inside the particle is 1.

4. 发明专利

JPH10255862A VALUABLE MATERIAL SEPARATING METHOD FROM LITHIUM ION SECONDARY BATTERY 失效
公开(公告)号：JPH10255862A
公开(公告)日：1998-09-25
申请号：JP6101397
申请日：1997-03-14
申请人： TOSHIBA CORP
发明人： YABUKI MOTOO , HAYASHI MASARU , KONUMA MASATAKA , TOMIOKA YOSHIKI , OYASATO NAOHIKO , KOMATSU IZURU , KITAMURA HIDEO , GOTANDA TAKESHI , TADAUCHI KIMIHIRO , FURUYA TOMIAKI , MORITA MASAAKI
IPC分类号： B09B5/00 , H01M10/54
摘要： PROBLEM TO BE SOLVED: To recover a valuable material such as rare metal from a used secondary lithium ion battery at a high recovering rate by soaking an electrode of the used secondary lithium ion battery in an acidic solution or the like, and separating the electrode into an electrode material and a current collecting body. SOLUTION: A used secondary lithium ion battery is disassembled, and an electrolyte is completely removed from an electrode, and is soaked in a solvent, and is cleaned. This electrode is soaked in any one of an acidic solution (such as hydrogen halide, sulfuric acid, hydrogen peroxide, nitric acid, etc.), a hydroxide solution of alkaline metal (such as sodium hydroxide or potassium hydroxide), an alcohol solution (such as a lithium alkoxide, sodium alkoxide, etc.) of alkaline metal or an organic solvent (such as ketone and ester), and is separated into an electrode material and a current collecting body. This electrode material is soaked in the acidic solution, and after valuable metal is dissolved, the valuable metal can be inexpensively recovered with high purity by chemical treatment.

5. 发明专利

JPH0885890A DEVICE AND METHOD FOR CLEANING PARTS FOR REFRIGERATOR 失效
公开(公告)号：JPH0885890A
公开(公告)日：1996-04-02
申请号：JP22227294
申请日：1994-09-16
申请人： TOSHIBA CORP
发明人： YABUKI MOTOO , HAYASHI MASARU , TATEBE TETSUYA , YOSHIDA TAKASHI , TAKEMURA MOMOKO
IPC分类号： B08B3/08 , C23G3/00
摘要： PURPOSE: To provide the device and method for cleaning the parts for a HCFC or HFC refrigerator capable of easily and effectively reducing the amts. of the Na, K and amines to be deposited on the parts when the parts are produced. CONSTITUTION: This device is provided with a first cleaning tank 1 to wash the parts cleaned with a degreasing detergent with industrial water and a second cleaning tank 2 to wash the parts washed in the first cleaning tank with pure water. The first cleaning tank is furnished with a feed port 3 to be supplied with industrial water and a discharge port 4 for the industrial water in excess to overflow, and the second cleaning tank is provided with a pure water feed port and a pure water discharge port, a pipeline 5 to make the feed port communicate with the discharge port of the second cleaning tank so that the pure water in the second cleaning tank is circulated and the means 7 and 8 disposed in the pipeline to remove the inorg. ions present in the pipeline.

6. 发明专利

JPH07333116A SAMPLE DECOMPOSING APPARATUS AND SAMPLE DECOMPOSING METHOD 失效
公开(公告)号：JPH07333116A
公开(公告)日：1995-12-22
申请号：JP12740494
申请日：1994-06-09
申请人： TOSHIBA CORP
发明人： MATSUNAGA HIDEKI , TAKENAKA MIYUKI , HAYASHI MASARU
IPC分类号： G01N1/28 , H01L21/66
摘要： PURPOSE:To provide a sample decomposing apparatus and a sample decomposing method which carry out sample decomposition efficiently to prepare a sample solution for analysis which is polluted extremely slightly by a reagent or the environments. CONSTITUTION:A sample decomposing apparatus is provided with a closed container 1, an acidic liquid storage container 2 installed in the inside of the closed container 1, a heating means 7 to heat the acidic liquid storage container 2, a magnetic field generating means 9 to affect an acidic liquid to be stored in the acidic liquid storage container 2 with magnetic force, a cooling tank 8 to cool the acid vapor produced by heating, and a sample storage container 3 installed under the cooling means.

7. 发明专利

JPH04132956A ION CHROMATOGRAPH FOR ANALYZING ANION 失效
公开(公告)号：JPH04132956A
公开(公告)日：1992-05-07
申请号：JP25409890
申请日：1990-09-26
申请人： TOSHIBA CORP
发明人： HASHIMOTO YOSHIMI , OKADA AKIRA , HAYASHI MASARU
IPC分类号： G01N30/02 , G01N30/14
摘要： PURPOSE:To continuously analyze sample solution with high accuracy by providing an alkali and alkaline earth removing means wherein a cation exchange resin film tube is placed inside a hollow housing member on an upper stream of a separation column in an analysis system. CONSTITUTION:Sample solution 1 is made flow in a direction of an arrow A inside a cation exchange resin film tube 2 while acid solution as reproduction solution 3 is made flow outside the tube 2 inside a housing member 4 from a direction indicated by an arrow B1 to a direction indicated by an arrow B2, whereby alkaline metal ions and alkaline earth metal ions in the solution 1 react with the tube 2 and replaced with hydrogen ions, and further by permit ting acid solution outside the tube 2, the tube 2 is reproduced. Thus alkaline metal ions and alkaline earth metal ions can be continuously removed from the solution 1. Therefore, highly accurate and rapid detection and analysis is possible in a background where anions are low in the solution 1 containing highly concentrated alkaline metal ions and alkaline earth metal ions.

8. 发明专利

JPS6432165A QUANTITATIVE ANALYSIS OF COPPER PEROXIDE (CU3+) IN OXIDE SUPERCONDUCTOR 失效
公开(公告)号：JPS6432165A
公开(公告)日：1989-02-02
申请号：JP18763387
申请日：1987-07-29
申请人： TOSHIBA CORP
发明人： HAYASHI MASARU , ENDO HIROSHI , YAMASHITA TSUTOMU , HASHIMOTO YOSHIMI , YABUKI MOTOHISA , SUZUKI ISAO
IPC分类号： G01N31/00 , G01N31/16
摘要： PURPOSE:To easily and rapidly determine copper peroxide (Cu ) by decomposing a sample to be analyzed with an inorg. acid added with an Fe ion soln. and titrating the unreacted Fe ions in the resultant sample soln. with a standard oxidation soln. CONSTITUTION:Gaseous N2 is fed from an inert gas supplying device 3 into a analyzing vessel 1 to replace the air with the gaseous N2. This supply is continued until the titration ends. A prescribed amt. of the ground analysis sample is then weighed into the vessel 1. The standard Fe ion liquid and the inorg. acid are then added thereto and the soln. is heated to at least >=30 deg.C on a hot plate 2 which is a heat source to decompose the oxide superconductor. Then, part of the instantaneously dissolved Cu ions react with the Fe ions to form Cu . The unreacted Fe ion remaining in the resultant sample soln. are thereafter titrated with the standard oxidizing liquid, by which the copper peroxide (Cu ) in the oxide superconductor is determined.

9. 发明专利

JPS646757A SIMULTANEOUS ANALYSIS OF FLUORINE AND SULFUR IN COMPOSITE MATERIAL CONTAINING SOLID LUBRICANT 失效
公开(公告)号：JPS646757A
公开(公告)日：1989-01-11
申请号：JP16091987
申请日：1987-06-30
申请人： TOSHIBA CORP
发明人： YAMASHITA TSUTOMU , HAYASHI MASARU , HASHIMOTO YOSHIMI , YABUKI MOTOHISA
IPC分类号： G01N30/06 , G01N31/00
摘要： PURPOSE:To simultaneously quantity F and S rapidly and precisely by an ion chromatograph, by a method wherein a composite material containing a solid lubricant is subjected to thermal hydrolysis to turn F and S into HF and H2SO4 respectively and these substances are made to be absorbed in an absorbing liquid to prepare a sample solution. CONSTITUTION:Steam and an oxygen gas 4 generated by heating in a mantle heater 3 are sent into a reaction tube 2 made of quartz, which is heated to about 500-1,200 deg.C in an electric furnace 1, and a boat 5 loaded with a prescribed quantity of an analytical sample weighed and put thereon is inserted into the tube. PTFE and molybdenum disulfide are pyrolytically decomposed completely by using a platinum net 6 as a catalyst, and hydrogen sulfide and H2SO4 are produced. These substances are made to be absorbed by NaOH of a prescribed concentration, which is diluted with distilled water to prepare a sample solution for quantifying F and S. F and S in the sample solution for quantifying F and S which is obtained in this way are quantified simultaneously by an ion chromatography.

10. 发明专利

JPH11265737A LITHIUM RECOVERING METHOD 失效
公开(公告)号：JPH11265737A
公开(公告)日：1999-09-28
申请号：JP6728898
申请日：1998-03-17
申请人： TOSHIBA CORP
发明人： HAYASHI MASARU , YABUKI MOTOO , KONUMA MASATAKA , TEZUKA FUMINOBU , TOMIOKA YOSHIKI
IPC分类号： C22B7/00 , C22B26/12 , H01M10/54
摘要： PROBLEM TO BE SOLVED: To inexpensively and easily separate and recover lithium from positive electrode active material of a spent lithium ion secondary battery. SOLUTION: In this lithium recovering method, when alkali used for deposit formation is separated from lithium contained in residual solution by using the residual solution containing alkali obtained after recovering transition metal from positive electrode active material of a spent lithium ion secondary battery, the residual solution is evaporated, dried and hardened, the dried substance is dissolved by alcohol, the solution obtained is then brought into contact with a positive ion exchange resin, and thereby, an alkali ion is separated from a lithium ion by absorbing the alkali ion in the solution by the positive ion exchange resin, in order to recover the separator lithium.

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